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Results for “X-ray fluorescence”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

New techniques in geochemical analysis

Thin layer and gas chromatography, Mossbauer and atomic absorption spectrometry, fission track analysis, X-ray fluorescence spectroscopy, and other methods employed in geochemistry

X-RAY FLUORESCENCE SPECTROSCOPY

K/rb ratios in tektites.

Potassium/rubidium ratios and individual K and Rb contents for 54 tektites determined by flame photometry or X-ray fluorescence

TEKTITE

Pattern recognition methods and air pollution source identification

Directional air samplers, used for resolving suspended particulate matter on the basis of time and wind direction were used to assess the feasibility of characterizing and identifying emission source types in urban multisource environments. Filters were evaluated for 16 elements and X-ray fluorescence methods yielded elemental concentrations for direction, day, and the interaction of direction and day. Large numbers of samples are necessary to compensate for large day-to-day variations caused by wind perturbations and/or source changes.

Leibecki, H. F.

X-Ray Absorption Spectroscopy in High Temperature Oxidation of Metals and Alloys

An experimental technique is described that allows for the joint study of the kinetics and of the oxide structure during the high temperature oxidation of metal surfaces. Oxygen is supplied at the metal through an electrochemical oxygen pump and the oxygen pressure, at the metal surface, is measured during oxidation by a YSZ (yttria stabilized zirconia) oxygen sensor. XAS (x-ray absorption spectroscopy) is performed in fluorescence mode at the cation K edge and after each oxidation step. An appropriate analysis of the XAS spectra could provide information on both the oxidation kinetics and oxide structure. Experimental data on the high temperature oxidation of nickel, cobalt, and Fe(64%)Ni(36%) alloy, at low oxygen pressure, are reported and analyzed according to the proposed data reduction. These results indicate the presented technique to be particularly suitable for studying the hot corrosion of oxide film too thick for common surface spectroscopy (AUGER, ESCA) and too thin for conventional thermogravimetric technique.

Daniele Gozzi

On the possible detection of an energetic photon pulse from the recent supernova in NGC 5253

A diffuse atmospheric fluorescence pulse having the proper signatures of an excitation caused by a fast burst of X-ray photons incident from the general direction of the recent supernova in NGC 5253, was recorded on May 3, 1972, at 20 hr 48 min 51 sec UT. Due to excessive background pulses of terrestrial origin, it is concluded that the evidence should at best be regarded as suggestive. It is recommended that the data of satellite-borne X-ray detectors be examined for anomalies at the indicated time.

Ogelman, H.