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At least 163 records · Page 9

Variable Depth Bragg Peak Method for Single Event Effects Testing

Traditionally, accelerator SEE testing is accomplished by removing the tops of packages so that the IC chips are accessible to heavy ions. However, ICs in some advanced packages cannot be de-lidded so a different approach is used that involves grinding and/or chemically etching away part of the package and the chip from the back side. The parts are then tested from the back side with ions having sufficient range to reach the sensitive volume. More recently, the entire silicon substrate in an SOI/SRAM was removed, making it possible to use low-energy ions with shorter ranges. Where removal of part of the package is not possible, facilities at Michigan State, NASA Space Radiation Laboratory, GANIL (France) and GSI (Germany) offer high-energy heavy ions with long ranges so that the ions can reach the devices' sensitive volumes without much change in the LET. Unfortunately, a run will typically involve only one ion species having a single energy and LET due to the long time it takes to tune a new energy. The Variable Depth Bragg Peak (VDBP) method is similar to the above method in that it involves the use of high-energy heavy ions that are able to pass through the packaging material and reach the device, obviating the need to remove the package. However, the method provides a broad range of LETs from a single ion by inserting degraders in the beam that modify the ion energy and, therefore, the LET. The crux of the method involves establishing a fiduciary point for degrader thickness, i.e., where the Bragg peak is located precisely at the sensitive volume in the device, for which the measured SEU cross-section and the ion LET are both also maxima and can be calculated using a Monte-Carlo program, TRIM. Once the fiduciary point has been established, calibrated high density polyethylene (HDPE) degraders are inserted into or removed from the beam to vary the ion LET at the device in a known manner. After each change of degrader thickness, the SEU cross-section is measured and the corresponding LET calculated from the change in degrader thickness. That information is used to generate a plot of cross-section as a function of ion LET. The advantages of this approach are that the part does not have to be de-lidded and a broad range of LETs is available from a single heavy ion without having to go to non-normal angles of incidence to change the "effective" LET. As we will show, it is possible to obtain an entire curve of cross-section versus LET using just two or three ions. Fig. 1 shows curves of cross-section vs LET for a Freescale 4 Mbit SOI/SRAM measured at the 88" Cyclotron at Berkeley and at NSRL. The open symbols are the data obtained from Berkeley for top-side and back-side irradiation. The solid data points are for the data obtained at NSRL using a device for which the package was intact. The data are for Iron and Gold and cover a range of LETs from 4 MeV.cm2/mg to 84 MeV.cm2/mg. The agreement between the data obtained from Berkeley and from NSRL is excellent, demonstrating that the VDBP method is capable of providing accurate values of cross-section versus LET, at least for the 4 Mbit SRAM. Details of the technique will be included in the final presentation.

Buchner, S.↗

Preliminary Evaluation of Commercial Off the Shelf (COTS) Packing Materials for Flight Medication Dispenser (FMD) Technology Development

This slide presentation reviews preliminary results of the program to evaluate Commercial Off the Shelf (COTS) packaging materials for pharmaceutical stability. The need for improved packaging is due to possible changes in chemical and/or physical properties of the drugs, which cause reported reduced potency and/or altered bioavailability and decreased efficacy.

Du, B.↗

HMPT: Hazardous Waste Transportation Live 27928, Test 27929

HMPT: Hazardous Waste Transportation (Live 27928, suggested one time and associated Test 27929, required initially and every 36 months) addresses the Department of Transportation (DOT) function-specific training requirements of the hazardous materials packagings and transportation (HMPT) Los Alamos National Laboratory (LANL) lab-wide training. This course addresses the requirements of the DOT that are unique to hazardous waste shipments. Appendix B provides the Title 40 Code of Federal Regulations (CFR) reference material needed for this course.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Licensing and Operation of BEA Research Reactor Package for Fuel, Source and Target Payloads - 19198

The Battelle Energy Alliance (BEA) Research Reactor Package (BRR Package) is currently in use for a variety of payload types and operational scenarios. The BRR Package is licensed by the Nuclear Regulatory Commission (NRC), under Certificate of Compliance (CoC) number USA/9341/B(U)F-96. The original packaging design, testing, and safety analysis activities were conducted by Orano Federal Services (Orano FS, formerly AREVA Federal Services) for the Idaho National Laboratory (INL), operated by the Battelle Energy Alliance (BEA) for the U.S. Department of Energy (DOE). One package was built and delivered to the INL in 2009, and has seen routine use since that time, primarily by DOE University Research Reactor programs. This paper will provide a history and description of the original design and licensing of the package and subsequent amended applications for the addition of new payloads. Each additional payload type provided unique design, operational, and licensing challenges - these challenges will be discussed, and the results and lessons learned presented will be beneficial for application in other radioactive material packaging projects. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Development of a New 48 Inch UF6 Cylinder Overpack - 17476

The Kevil Kougar overpack is new generation USA DOT Specification 7A packaging designed to transport ANSI N14.1 and ISO-7195 compliant 48-inch UF6 cylinders. In December 2016, the USA DOT issued USA/0815/H(U)-96 for the transport of 48X and 48Y cylinders and USA/0819/H(M)-96 for the transport of 48G, 48H, 48HX, 48O, 48OM, 48OM(Allied) and 48T cylinders. The H(U) certificate is for transport of thick-walled cylinders and the H(M) certificate is for transport of thin-walled cylinders. The Kevil Kougar design provides thermal and impact protection for the cylinder under conditions required for a Type A package capable of transporting UF{sub 6} via road, rail, and ocean. The packaging design is a smooth octagonal shape designed to carry one 48-inch UF{sub 6} cylinder. It consists of an upper subassembly and lower subassembly, which are fastened together with ten toggle bolts, five per side. Each subassembly consists of an outer and inner steel shell secured to a frame assembly, with wood and polyurethane foam filling the space between. The protruding components are only for ease of operation and consist of four lifting lugs and fork pockets on the upper body, and the base and fork pockets on the lower body. The design incorporates interior rubber pads for cylinder cushioning, support and alignment, steel stabilizing beams fore and aft to prevent cylinder movement, closure mechanisms, a tamper indicating device and tie-down features. The Kevil Kougar is currently designed to transport contents of depleted uranium and natural uranium. Future activities include licensing the package as Type AF to facilitate transport of historic USA Department of Energy fissile material packages. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Recent Advances in Biological Recycling of Polyethylene Terephthalate (PET) Plastic Wastes

Polyethylene terephthalate (PET) is one of the most commonly used polyester plastics worldwide but is extremely difficult to be hydrolyzed in a natural environment. PET plastic is an inexpensive, lightweight, and durable material, which can readily be molded into an assortment of products that are used in a broad range of applications. Most PET is used for single-use packaging materials, such as disposable consumer items and packaging. Although PET plastics are a valuable resource in many aspects, the proliferation of plastic products in the last several decades have resulted in a negative environmental footprint. The long-term risk of released PET waste in the environment poses a serious threat to ecosystems, food safety, and even human health in modern society. Recycling is one of the most important actions currently available to reduce these impacts. Current clean-up strategies have attempted to alleviate the adverse impacts of PET pollution but are unable to compete with the increasing quantities of PET waste exposed to the environment. In this review paper, current PET recycling methods to improve life cycle and waste management are discussed, which can be further implemented to reduce plastics pollution and its impacts on health and environment. Compared with conventional mechanical and chemical recycling processes, the biotechnological recycling of PET involves enzymatic degradation of the waste PET and the followed bioconversion of degraded PET monomers into value-added chemicals. This approach creates a circular PET economy by recycling waste PET or upcycling it into more valuable products with minimal environmental footprint.

42 ENGINEERING↗

9977 type b packaging internal data collection feasibility testing - magnetic field communications

The objective of this report is to document the findings from proof-of-concept testing performed by the Savannah River National Laboratory (SRNL) R&D Engineering and Visible Assets, Inc. for the DOE Packaging Certification Program (PCP) to determine if RuBee (IEEE 1902.1) tags and readers could be used to provide a communication link from within a drum-style DOE certified Type B radioactive materials packaging. A Model 9977 Type B Packaging was used to test the read/write capability and range performance of a RuBee tag and reader. Testing was performed with the RuBee tags placed in various locations inside the packaging including inside the drum on the outside of the lid of the containment vessel and also inside of the containment vessel. This report documents the test methods and results. A path forward will also be recommended.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Assessing the Success of Shipping High Burn-Up Sister Rods from ORNL to PNNL - 19456

The U.S. Department of Energy's (DoE's) Used Fuel Disposition Campaign (UFDC), in collaboration with the U.S. Nuclear Regulatory Commission and the commercial nuclear industry have initiated a group of projects to obtain data to support the enhancement of the technical bases for the extended storage and transportation of high-burnup (HBU) (>45 GWd/MTU) spent nuclear fuel (SNF). Under this overall effort, a U.S. Nuclear Regulatory Commission-licensed storage cask was loaded with Thirty-Two (32) HBU SNF assemblies. The cask was modified to allow radial and axial temperature profiles to be measured using thermocouple lances inserted through the lid. Twenty-five (25) rods from similar assemblies of similar claddings, in-reactor placement, and burnup histories (herein called 'sister rods') have been shipped from the North Anna Nuclear Power Plant and are currently being nondestructively tested at Oak Ridge National Laboratory (ORNL). To meet UFD's research objectives, testing on ten (10) of these rods is required to be performed at Pacific Northwest National Laboratory (PNNL). Although the twenty-five rods were originally received at ORNL in the 10-160B, the PNNL facility that would need to receive the ten (10) rods did not have an active history with using the 10-160B. This paper first identifies and summarizes various criteria and evaluations used in helping to select which package will be used for the shipment of the ten (10) sister rods to PNNL (i.e., Bases on why the NACLWT was chosen). With the shipment scheduled to be complete, identified potential concerns, issues, lessons learned, and transportation summary documents were studied (post-shipment). The adequacy of the criteria and evaluations used to choose the NAC-LWT were accessed to determine their adequacy. The results show the criteria were adequate. However, it was noted that DOE Order 460.2A, DOE M 460.2-1A, and DOE G 460.2-1 have differences in the terminology and scope, resulting in clarity issues and differences in regulatory interpretation. Since one-of-a kind spent fuel shipments are uncommon, the topic will be significant interest to people who work in radioactive material packaging and transportation. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

A new classification scheme of plastic wastes based upon recycling labels

Highlights: • PET, HPDE or PP types of plastics are considered. • An automated classification of plastic bottles based on the feature extraction and classification methods is performed. • The decision mechanism consists of PCA, Kernel PCA, FLDA, SVD and Laplacian Eigenmaps methods. • SVM is selected to achieve the classification task and majority voting technique is used. - Abstract: Since recycling of materials is widely assumed to be environmentally and economically beneficial, reliable sorting and processing of waste packaging materials such as plastics is very important for recycling with high efficiency. An automated system that can quickly categorize these materials is certainly needed for obtaining maximum classification while maintaining high throughput. In this paper, first of all, the photographs of the plastic bottles have been taken and several preprocessing steps were carried out. The first preprocessing step is to extract the plastic area of a bottle from the background. Then, the morphological image operations are implemented. These operations are edge detection, noise removal, hole removing, image enhancement, and image segmentation. These morphological operations can be generally defined in terms of the combinations of erosion and dilation. The effect of bottle color as well as label are eliminated using these operations. Secondly, the pixel-wise intensity values of the plastic bottle images have been used together with the most popular subspace and statistical feature extraction methods to construct the feature vectors in this study. Only three types of plastics are considered due to higher existence ratio of them than the other plastic types in the world. The decision mechanism consists of five different feature extraction methods including as Principal Component Analysis (PCA), Kernel PCA (KPCA), Fisher’s Linear Discriminant Analysis (FLDA), Singular Value Decomposition (SVD) and Laplacian Eigenmaps (LEMAP) and uses a simple experimental setup with a camera and homogenous backlighting. Due to the giving global solution for a classification problem, Support Vector Machine (SVM) is selected to achieve the classification task and majority voting technique is used as the decision mechanism. This technique equally weights each classification result and assigns the given plastic object to the class that the most classification results agree on. The proposed classification scheme provides high accuracy rate, and also it is able to run in real-time applications. It can automatically classify the plastic bottle types with approximately 90% recognition accuracy. Besides this, the proposed methodology yields approximately 96% classification rate for the separation of PET or non-PET plastic types. It also gives 92% accuracy for the categorization of non-PET plastic types into HPDE or PP.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Pressure Relief Valve

"Sputtering" is the process of applying film-like metal coatings onto a surface by bombarding the coating material with electrocharged ions. This causes the material to disintegrate and relocate on the substrate an atom layer at a time. The process allows a variety of coating materials to be deposited on various surfaces. Deposition Technology, Inc. (DTI) uses "sputtering" for window films, packaging materials, etc. Valves installed on two vacuum chambers which are part of DTI's system, were developed by Lewis Research Center and detailed in Tech Briefs. The valve protects the environment and frees the operator from monitoring the chamber venting.

Source record↗

Production and characterization of a composite insulation material from waste polyethylene teraphtalates

The pollution of polyethylene teraphtalate (PET) is in huge amounts due to the most widely usage as a packaging material in several industries. Regional pumice has several desirable characteristics such as porous structure, low-cost and light-weight. Considering the requirements approved by the Ministry of Public Works on isolation, composite insulation material consisting of PET and pumice was studied. Sheets of composites differing both in particle size of pumice and composition of polymer were produced by hot-molding technique. Characterization of new composite material was achieved by measuring its weight, density, flammability, endurance against both to common acids and bases, and to a force applied, heat insulation and water adsorption capacity. The results of the study showed that produced composite material is an alternative building material due to its desirable characteristics; low weight, capability of low heat conduction.

36 MATERIALS SCIENCE↗

Biological toxicity and environmental hazards associated with PLGA nanoparticles

There have been tremendous advances in nanotechnology. More recently, the use of nanoparticles has expanded to applications including materials, packaging, energy, and medical uses such as drug delivery, diagnostics, and therapeutics. The American Society for Testing and Materials (ASTM) and the International Organization for Standardization (ISO) define nanoparticles as particles with at least one dimension measuring between 1 and 100 nm (2), but this view is generally too limited, and recommendations have been made to consider all materials with a dimension measuring under 1,000 nm as nanoparticles. The biomedical uses of nanoparticles are particularly promising because of their ability to reach and target various sites and organs. However, some nanoparticles can be composed of toxic materials or are limited by issues of biodistribution and bioaccumulation, which have hampered their use in biomedicine. The copolymer poly lactic-co-glycolic acid (PLGA) has gained use in biomedical applications as a delivery system because it is considered biocompatible and can be formulated with controlled degradation in physiological environments. PLGA has a history in biomedicine that dates to the 1970s when biodegradable sutures were developed using PLGA. In addition, the United States (US) Food and Drug Administration (FDA) and the European Medicine Agency (EMA) have approved various PLGA particle formulations as therapeutic delivery vehicles. Interest in biocompatible materials to deliver a range of therapeutic drugs, proteins, nucleic acids, and other molecules has risen recently. In addition to drug delivery, sustained drug release can be achieved by tuning the physical properties of PLGA, such as the molecular weight, ratio of lactic to glycolic acid, drug concentration, stabilizing molecules, and particle size. Given the rise of nanoparticles, human and environmental exposure to them is inevitable as more applications use free, unbound, and highly mobile particles. Although PLGA is generally considered safe, a detailed understanding of how PLGA and the other components used to help formulate this copolymer into a nanoparticle delivery vehicle is useful for assessing potential harmful effects. Despite recent advances in PLGA nanoparticle formulations, residual stabilizing molecules, inconsistent preparations, and batch-to-batch variations can lead to toxicity. Poor preparations of PLGA can lead to common mechanisms of toxicity observed with nanoparticles, such as inflammation and oxidative stress. Consistency in PLGA formulations and accurate methods to evaluate nanoparticle toxicity are needed to ensure safety. In order to better assess PLGA nanoparticles as non-toxic delivery systems, it is critical to understand their physical and chemical properties and the formulation protocols that may introduce toxic components into particles.

Biology, nanoparticle, toxicity↗

Comparison of German and American fabrication standards for transportation and storage containments of high level radioactive material type B packages - 15055

As the competent authority for the evaluation of German radioactive material (RAM) transport and storage packages, BAM (the German Federal Institute for Materials Research and Testing) has evaluated various international cask manufacturers regarding compliance with the German Type B(U) licensing requirements. The US NRC has recommended paragraphs in the ASME Boiler and Pressure Vessel (B and PV) Code, Section III, Division 3, as the measure to quantify the safety requirements of the US regulations regarding fabrication of RAM transportation and storage containments. The objective of this study is to compare the fabrication criteria of the German Dangerous Goods Procedural Rules (BAM-GGR) and the German Institute for Standardization (DIN) with the US quantitative measures for fabrication of RAM package containment vessels. This comparison will cover major similarities and differences between the requirements of the German standards and the ASME Code requirements for Type B package containment fabrication QC (quality control). While the material most often used for German RAM containment applications is ductile cast iron (DCI), in the US forged austenitic stainless steel is typically used. This study focuses on fabrication QC measures required to ensure reproducible and acceptable properties for DCI containments. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

High-Performance Power-Semiconductor Packages

A 600-V, 50-A transistor and 1,200-V, 50-A diode in rugged, compact, lightweight packages intended for use in inverter-type power supplies having switching frequencies up to 20 kHz. Packages provide low-inductance connections, low loss, electrical isolation, and long-life hermetic seal. Low inductance achieved by making all electrical connections to each package on same plane. Also reduces high-frequency losses by reducing coupling into inherent shorted turns in packaging material around conductor axes. Stranded internal power conductors aid conduction at high frequencies, where skin effect predominates. Design of packages solves historical problem of separation of electrical interface from thermal interface of high-power semiconductor device.

Renz, David↗

PHASE II VAULT TESTING OF THE ARGONNE RFID SYSTEM

The U.S. Department of Energy (DOE) (Environmental Management [EM], Office of Packaging and Transportation [EM-45]) Packaging and Certification Program (DOE PCP) has developed a Radio Frequency Identification (RFID) tracking and monitoring system, called ARG-US, for the management of nuclear materials packages during transportation and storage. The performance of the ARG-US RFID equipment and system has been fully tested in two demonstration projects in April 2008 and August 2009. With the strong support of DOE-SR and DOE PCP, a field testing program was completed in Savannah River Site's K-Area Material Storage (KAMS) Facility, an active Category I Plutonium Storage Facility, in 2010. As the next step (Phase II) of continued vault testing for the ARG-US system, the Savannah River Site K Area Material Storage facility has placed the ARG-US RFIDs into the 910B storage vault for operational testing. This latest version (Mark III) of the Argonne RFID system now has the capability to measure radiation dose and dose rate. This paper will report field testing progress of the ARG-US RFID equipment in KAMS, the operability and reliability trend results associated with the applications of the system, and discuss the potential benefits in enhancing safety, security and materials accountability. The purpose of this Phase II K Area test is to verify the accuracy of the radiation monitoring and proper functionality of the ARG-US RFID equipment and system under a realistic environment in the KAMS facility. Deploying the ARG-US RFID system leads to a reduced need for manned surveillance and increased inventory periods by providing real-time access to status and event history traceability, including environmental condition monitoring and radiation monitoring. The successful completion of the testing program will provide field data to support a future development and testing. This will increase Operation efficiency and cost effectiveness for vault operation. As the next step (Phase II) of continued vault testing for the ARG-US system, the Savannah River Site K Area Material Storage facility has placed the ARG-US RFIDs into the 910B storage vault. Deploying the ARG-US RFID system lends to a reduced need for manned surveillance and increased inventory periods by providing real-time access to status and event history traceability, including radiation and environmental monitoring. The successful completion of the testing program will provide field data to support future development and testing.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Dual Use of Packaging on the Moon: Logistics-2-Living

This paper describes a modular packaging system for logistics that can be reconfigured into internal outfitting for a lunar outpost, including desks, chairs, partitions, cabinets, and radiation shielding. Logistics include clothes, equipment, food, and other consumables needed to sustain the crew for the duration of the mission. A significant mass penalty is required for the packaging and handling of logistics for re-supply of short to long-term space missions that must be brought out of the gravity well on a launch vehicle. Once the supplies have been exhausted, the packaging material is typically of no further use and is discarded. If a scheme can be developed that reuses the logistics packaging, the mass penalty can be reduced. In this research, a modular packaging system has been devised as a kit-of-parts that can be used for both handling logistics supplies, and then reconfigured into desks, chairs, partitions, cabinets, and radiation shielding. The system is derived from a standard International Space Station (ISS)-type Cargo Transfer Bag (CTB), using soft, unfoldable box-like containers with stiff metal inserts. The empty hydrogen-impregnated CTBs can be used as-is for cabinets, opened up for use as partitions, or draped over the habitat as layers of radiation shielding. Stiff metal inserts can be reconfigured into desks and other useful outfitting.

recycle and reuse↗

Automotive Power Electronics and Electric Machine Thermal Management

The transition to modular and scalable electrified vehicle transportation requires technologies to improve power density within cost and reliability constraints to maximize vehicle platform flexibility. Key research challenges arise due to the limited packaging space, coolant distribution, electrical connections, and ambient temperatures. Challenges include thermal management for compact power-dense electric machines and the associated power electronics for power management within the vehicle. High-temperature silicon and wide-bandgap (WBG) based power electronics systems are of interest to enable compact and efficient electric drive systems. The higher temperatures present packaging challenges for thermal management and reliability. In this work, we provide an overview of research for thermal characteristics of materials, packages and thermal management approaches for enabling compact power dense automotive electric drive systems.

DIRECT ENERGY CONVERSION↗