Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “material identification”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 145 records · Page 8

Tuning magnetic antiskyrmion stability in tetragonal inverse Heusler alloys

The identification of materials supporting complex, tunable magnetic order at ambient temperatures is foundational to the development of new magnetic device architectures. In this work, we report the design of Mn 2 XY tetragonal inverse Heusler alloys that are capable of hosting magnetic antiskyrmions whose stability is sensitive to elastic strain. Here We first construct a universal magnetic Hamiltonian capturing the short- and long-range magnetic order which can be expected in these materials. This model reveals critical combinations of magnetic interactions that are necessary to approach a magnetic phase boundary, where the magnetic structure is highly susceptible to small perturbations such as elastic strain. We then computationally search for quaternary Mn 2 (X 1 , X 2 ) Y alloys where these critical interactions may be realized and which are likely to be synthesizable in the inverse Heusler structure. We identify the Mn 2 Pt 1–z X z Ga family of materials with X = Au, Ir, Ni as an ideal system for accessing all possible magnetic phases, with several critical compositions where magnetic phase transitions may be actuated mechanically.

36 MATERIALS SCIENCE↗

Origins and consequences of asymmetric nano-FTIR interferograms

Infrared scattering-type near-field optical microscopy, IR s-SNOM, and its broadband variant, nano-FTIR, are pioneering, flagship techniques for their ability to provide molecular identification and material optical property information at a spatial resolution well below the far-field diffraction limit, typically less than 25 nm. While s-SNOM and nano-FTIR instrumentation and data analysis have been discussed previously, there is a lack of information regarding experimental parameters for the practitioner, especially in the context of previously developed frameworks. Like conventional FTIR spectroscopy, the critical component of a nano-FTIR instrument is an interferometer. However, unlike FTIR spectroscopy, the resulting interference patterns or interferograms are typically asymmetric. Here, we unambiguously describe the origins of asymmetric interferograms recorded with nano-FTIR instruments, give a detailed analysis of potential artifacts, and recommend optimal instrument settings as well as data analysis parameters.

47 OTHER INSTRUMENTATION↗

Lunar surface - Identification of the dark mantling material in the Apollo 17 soil samples

Evidence indicates that Apollo 17 sample 74001, a soil consisting of very dark spheres, is composed almost entirely of the dark mantling material that covers a large region of the southeastern boundary of Mare Serenitatis. Other Apollo 17 samples contain only a component of this material. The underlying basalt in the Taurus-Littrow valley appears to be an extension of material forming the low-albedo ring around part of Mare Serenitatis and much of the surface of Mare Tranquillitatis. The surface of this basalt region is spectrally distinct from areas with dark mantling material. These results are derived from telescopic and laboratory measurements of the optical properties of lunar soil. Digital vidicon color images are used to map the extent of these material units in the Taurus-Littrow region.

Pieters, C.↗

Oil-pollution detection and monitoring from space using ERTS-1

The author has identified the following significant results. Three reported spills were investigated using four digital computer, compatible techniques on ERTS - 1 data. A spill on the Atlantic Ocean (off Virginia) was studied to develop spectral signatures. Another spill, in Oakland Bay, was studied by ratioing spectral channels (to try to eliminate turbidity effects) and by summing different spectral channels to look for anomolus values caused by oil. The final spill, off Southern California, was investigated by looking for anomolus values in each channel separately. Results indicate that any of these methods might be usable if the spill is large enough to be seen by satellite, if the spill occurs more than a few kilometers off shore, and if the sky and water are relatively clear. In the case of the Atlantic spill, identification of material was not possible; and in the other two cases, the spills could not be detected at all. ERTS-1 was not considered feasible for this type of work because of its 18 day overpass frequency, the few spectral channels, the extended bandwidths, and the long, information retrieval time.

Horvath, R.↗

Biomedical application in space, pilot program in the southern California region

A pilot program is presented which was to promote utilization of the Shuttle/Spacelab for medical and biological research applied to terrestrial needs. The program was limited to the Southern California region and consisted of the following five tasks: (1) preparation of educational materials; (2) identification of principal investigators; (3) initial contact and visit; (4)development of promising applications; and (5) evaluation of regional program methodology.

Kelton, A. A.↗

Rapid data comparison technique development for N-ray/X-ray analysis

An operational N-ray/X-ray computer analysis system for nondestructive testing problems was realized by developing: (1) more efficient data transfer routines for use in existing image processing systems; (2) the capability to store and analyze multiple N-ray/X-ray images; (3) an efficient 2-D Fast Fourier Transform; and (4) transfer functions compensation capability to correct for distortions and nonlinearities of N-rays/X-rays. Applications of the technique are summarized for the following: thermal protection system tile with hydraulic fluid; thermal protection system tile with corrosion; thermal protection system tile debonding; stainless steel tubing corrosion; defective electrical devices; fast film restoration and deblur; corrosion tracking over time; reduction of source vignetting, and identification of materials (0 rings, Teflon parts, soft goods) via table look up.

Butterfield, R. L.↗

Spectroscopic remote sensing for geological applications

Remote sensing is being used with increasing frequency in the development of geologic maps and in the exploration process. Spectral data from airborne and spaceborne multispectral scanners provide information on rock type and vegetation stress, important in geologic applications. Emphasis is now being placed on direct identification of materials rather than discrimination among geologic units. To do this, higher spectral resolution systems with wider spectral coverage than currently available are required. Imaging spectroscopy in the 0.4 - 14 microns region appears to be the answer.

Goetz, A. F. H.↗

Investigation of test methods, material properties, and processes for solar cell encapsulants

A study of potentially useful low cost encapsulation materials for the Flat-Plate Solar Array project is discussed. The goal is to identify, evaluate, test and recommend encapsulant materials and processes for the production of cost-effective, long life solar cell modules. Technical investigations included studies of aging and degradation of candidate encapsulation materials, continued identification of primers for durable bonding of module interfaces, continued evaluation of soil resistant treatments for the sunlit surface of the module and testing of corrosion protective coatings for use low cost mild steel substrates.

Willis, P. B.↗

Improved Spectrometer for Field Use

Proposed portable spectrometer for analyzing minerals in field generates spectral images like camera and process spectral data for real-time identification of materials. To identify unknown mineral, user locates significant peaks in displayed spectrum and matches them to spectrum in portfolio of reference spectra. Alternatively, user calls up display of prerecorded spectra in same wavelength region for comparison or allows spectrometer to determine best match automatically. New instrument makes it unnecessary to return data to laboratory or equipment trailer for processing.

Goetz, A. F. H.↗

Remote sensing of vegetation at regional scales

Relations between spectroscopy and the concept of inferring surface cover type and condition from measurements of reflected or emitted radiation are examined, taking into account the observation of 'spectral signatures'. It has now become evident that the paradigm which had provided the basis for the spectroscopic identification of materials, is incomplete when applied to the inference of type and condition of materials in a natural environment. It was found that one could not collect a remote sensing signature from an unknown ground cover class at a particular time and place and match that signature with an a priori catalog value to infer the properties of the unknown cover class. The spectroscopy paradigm was, therefore, largely abandoned in favor of decision theoretic approaches. Attention is given to the temporal greenness profile feature space, the crop stage of development estimation using a temporal greenness profile, the temporal greenness profile for crop yield, and applications to regional scales.

Hall, F. G.↗

A simplified orthotropic viscoplasticity theory based on overstress

The viscoplasticity theory based on overstress, a simplified version of Sutcu (1985) theory, is presented for the case of orthotropy. The theory permits asymptotic solutions for checking numerical experiments and for identification of material properties. It is applicable to materials with rate(time) dependence, hysteresis, and a permanent set, such as cubic crystals, directionally solidified alloys, and metal matrix composites. Though it is a unified type theory, with effects of creep and plasticity not separated, it allows to identify viscous and plastic contributions to the stress in the asymptotic state.

Sutcu, M.↗

A DTA/GC for the in Situ Identification of the Martian Surface Material

The composition and mineralogy of the Martian surface material remain largely unknown. To determine its composition and mineralogy, several techniques are being considered for in situ analyses of the Martian surface material during missions to Mars. We have successfully developed, constructed, and tested a laboratory DTA/GC. The DTA is a Dupont model 1600 high temperature DTA coupled with a GC equipped with a MID detector. The system is operated by a Sun Sparc 11 workstation. When gas evolves during a thermal chemical event, it is shunted into the GC and the temperature is recorded in association with the specific thermal event. We have used this laboratory instrument to define experimental criteria necessary for determining the composition and mineralogy of the Martian surface in situ (e.g., heating of sample to 1100 C to distinguish clays). Our studies indicate that DTA/GC will provide a broad spectrum of mineralogical and evolved gas data pertinent to exobiology, geochemistry, and geology.

Mancinelli, R. L.↗

Design, Progressive Modeling, Manufacture, and Testing of Composite Shield for Turbine Engine Blade Containment

An effective design methodology was established for composite jet engine containment structures. The methodology included the development of the full and reduced size prototypes, and FEA models of the containment structure, experimental and numerical examination of the modes of failure clue to turbine blade out event, identification of materials and design candidates for future industrial applications, and design and building of prototypes for testing and evaluation purposes.

Binienda, Wieslaw K.↗

Colossal Tooling Design: 3D Simulation for Ergonomic Analysis

The application of high-level 3D simulation software to the design phase of colossal mandrel tooling for composite aerospace fuel tanks was accomplished to discover and resolve safety and human engineering problems. The analyses were conducted to determine safety, ergonomic and human engineering aspects of the disassembly process of the fuel tank composite shell mandrel. Three-dimensional graphics high-level software, incorporating various ergonomic analysis algorithms, was utilized to determine if the process was within safety and health boundaries for the workers carrying out these tasks. In addition, the graphical software was extremely helpful in the identification of material handling equipment and devices for the mandrel tooling assembly/disassembly process.

Hunter, Steve L.↗

Preliminary Examination Process of Apollo Core 73002 - Insights and Lessons Learned From ANGSA for Future Sample Return Missions

Apollo Sample 73002 is part of a 2-foot long “drive tube” (73001/73002) of regolith that was collected from a landslide deposit near Lara Crater at the Apollo 17 site, Station 3. The double drive tube is believed to have penetrated a lunar landslide deposit that was transported from the slope of the South Massif into the TLV [1]. As part of the ANGSA (Apollo Next Generation Sample Analyses) initiative, preparing preliminary examination (PE) catalog of 73002 is a crucial first step for the early identification of material types such as rock fragments, and potential stratigraphy within the core. PE of Apollo core 73002 is distinct from science activities with the main goal to produces a sample catalog with a level of detail about sample characterization that is sufficient for the ANGSA PIs (and later on the lunar sample community) to select and request the samples to conduct their individual, scientific studies. Ultimately, the PE catalog of 73002 will help to establish a better understanding of the stratigraphy of the land slide deposit; the processes of the landslide including the trigger(s) and possibly number of landslide events, as well as the role of volatiles [1] and will aid in the careful preservation of the material for future studies [2].

Apollo↗

From Apollo to Artemis: How Processing ANGSA Core Samples 73001/2 Can Help to Prepare for Future Sample Return Missions to the Moon and Beyond.

Introduction: Apollo Sample 73001/2 is a ~71cm long double drive tube consisting of an upper part (73002) and a lower part (73001) that contains regolith collected near Lara Crater at the Apollo 17 site, Station 3. The double drive tube is believed to have penetrated a lunar landslide deposit that was transported from the slope of the South Massif into the Taurus-Littrow Valley [1]. As part of the ANGSA (Apollo Next Generation Sample Analyses) initiative, preparing a preliminary examination (PE) catalog of 73001/2 is a crucial first step for the early identification of material types such as rock fragments and potential stratigraphy within the core. Many new curation and scientific tools such as X-ray computed tomography (XCT) [3], multi-spectral imaging [4], and gas extraction manifold with piercing tool [5-7], have been applied to the ANGSA core to benefit curation strategy, PE efforts, sample allocation to the planetary science community, and ultimately help to prepare for future sample return missions like Artemis. 73001/2 Preliminary Examination and Processing: Sample 73002 was successfully opened and extruded in Nov. 2019 and fully dissected at the end of 2021. Sample 73001 (Fig. 1) was successfully extruded in March 2022 after careful planning before opening the Core Sample Vacuum Container (CSVC) that was holding the drive tube of 73001. XCT, as part of PE, was used to scan the bottom and top part of the 73001 core tube within the CSVC prior to opening it to 1) facilitate non-destructive, rapid detection of any contamination potentials due to piercing of the CSVC during gas extraction [7]; and 2) to aid in the Artemis sample tool development and provide data on the knife edge seal of the CSVC. This knowledge will help us connect the mechanics of the implemented design (i.e., XCT data) to the performance of the seal (i.e., data on the gas samples will tell us how well the seal preserved the volatile record of lunar samples). Both type of information will feed forward into Artemis tool and storage strategies for future samples. Results and Lessons learned: The XCT data of the CSVC and core tube within showed that the bottom Teflon cap was not pierced during gas extraction (Fig. 1c) and thus, the sample integrity remained guaranteed during piercing and subsequent gas extraction. However, the XCT scan of the top of the core (Fig. 1b) revealed that the drive tube was overfilled with lunar soil and the tool that keeps the soil constrained within the drive tube was not fully deployed. These preliminary data allowed us to implement the necessary steps to prevent loss of sample integrity, including any potential stratigraphy shifts during extrusion. Processing Apollo core 73001/2, creating an informative PE catalog, and applying new and refined tools and technologies for sample analyses are invaluable activities that will assist in circumventing any potential pitfalls, aid in the characterization of samples, and help in the assessment of how well any lunar material has been collected and preserved in the past. This will aid in designing future sample collections and curation procedures and help to prepare for future human exploration and sampling missions such as Artemis. References: [1] Schmitt H. (2017) Icarus 298, 2-33. [3] Zeigler et al. (2021) LPSC 52nd, #2632; [4] Sun et al. (2021), LPSC 52nd, #1789; [5] Parai et al. (2021), LPSC 52nd #2665; [6] Schild et al. (2021) LPSC 52nd #1888; [7] McDonald (2022) ESL 2022.

ANGSA↗

Application of Long-Path Gas Cell Assisted Infrared Spectroscopy for Detection of Lunar Volatiles and Advanced Curation Efforts

The motivation behind analyzing gaseous samples from the Permanently Shadowed Regions (PSRs) on the lunar surface is built upon the volatiles observed during the LCROSS mission. Advanced curation techniques under cold conditions are essential to the critical scientific analysis of these returned samples. The detection of various volatiles in returned samples by gas-phase infrared (IR) spectroscopy is known to be a powerful tool to understand the resources present in planetary bodies and Astro-materials. The identification and quantification of volatile compounds in returned planetary samples and regolith simulants by advanced and custom-built analytical devices are areas of primary research interest in our group and the Planetary Exploration & Astromaterials Research Laboratory (PEARL) facility. In this context, we discuss recent advancements and experimental results for quick analysis of the major volatiles detected by the LCROSS (water, CO 2 , CH 3 OH, and NH 3 ) by a long-path gas cell/FTIR (Fourier Transform Infrared) spectrometer system. The applicability of this system is demonstrated by qualitative analysis of a series of volatiles measured individually. In addition, the linear dependence of absorption intensity on headspace sample volumes was checked by measuring gas-phase IR absorption spectra of increasing volumes of pure CO 2 gas aliquots. Finally, the instrument performance was evaluated by measuring the relative concentration of NH 3 (g) in methanol solution.

Curation↗