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NASA NTRSDate not supplied

Variable Pressure - Scanning Electron Microscopy (VP-SEM)

Variable Pressure (or Environmental) Scanning Electron Microscopy (VP-SEM) combined with Energy Dispersive X-ray Spectroscopy (EDS) is one of the most powerful methods for characterizing the sub-micron topography and chemical composition of uncoated samples. Terrestrially, VP-SEM is extensively used to non-destructively study geologic and manufactured materials with high spatial resolution (tens of nanometers) and large depth-of-field. An SEM offers a geologist a first survey of microscopic mineral phases via secondary electron imaging (SEI), which provides a topographic look at a sample, as well as backscattered electron (BEI) imaging, which contrasts the phases present based on their geochemistry (atomic number). A VP-SEM utilizes a gas in the sample chamber as a charge dissipation and signal amplification method, allowing analysis of a sample without preparation in the form of a conductive coating. A miniaturized VP-SEM operating in-situ on a lander or rover would be able to use the CO2-rich Martian atmosphere (e.g., Nier et al., 1976; Williams 2016) as an imaging medium for this purpose. Adaptation of a VP-SEM for in-situ Mars surface studies will provide a new imaging capability (via SEI) that is at least an order of magnitude higher resolution than the Mars Hand Lens Imager (MAHLI) on the Mars Science Laboratory (Williams et al., 2015), and equal to or better than the achieved resolution of the Atomic Force Microscope on the Phoenix Mars lander (Pike et al., 2011). In addition, the MVP-SEM is capable of BSI and simultaneous chemical analysis of the imaged region. In this sense, the MVP-SEM can be regarded as an instrument suite that will provide a new set of information not achievable by any other instrument. The Miniaturized Variable Pressure Scanning Electron Microscope (MVP-SEM) was designed, built, and benchtop tested by a team at NASA’s Marshall Space Flight Center and Jet Propulsion Laboratory (JPL), Jacobs Space Exploration Group, Applied Physics Technologies, Inc. (AP-Tech), and Creare LLC, working with a team of technical and science collaborators. Benchtop testing was successful, proving concept feasibility. To date, the MVP-SEM has achieved an imaging resolution of <100 nm in the lab, and with continued optimization, even better performance (~50 nm resolution) is possible. Use in-situ on the lunar or other planetary surfaces would require some redesign to optimize instrument performance, but such an instrument would be equally useful.

Variable Pressure Scanning Electron Microscopy↗
NASA NTRSDate not supplied

Miniature Variable Pressure - Scanning Electron Microscopy (MVP-SEM)

Variable Pressure (or Environmental) Scanning Electron Microscopy (VP-SEM) combined with Energy Dispersive X-ray Spectroscopy (EDS) is one of the most powerful methods for characterizing the sub-micron topography and chemical composition of uncoated samples. Terrestrially, VP-SEM is extensively used to non-destructively study geologic and manufactured materials with high spatial resolution (tens of nanometers) and large depth-of-field. An SEM offers a geologist a first survey of microscopic mineral phases via secondary electron imaging (SEI), which provides a topographic look at a sample, as well as backscattered electron (BEI) imaging, which contrasts the phases present based on their geochemistry (atomic number). A VP-SEM utilizes a gas in the sample chamber as a charge dissipation and signal amplification method, allowing analysis of a sample without preparation in the form of a conductive coating. A miniaturized VP-SEM operating in-situ on a lander or rover would be able to use the CO2-rich Martian atmosphere (e.g., Nier et al., 1976; Williams 2016) as an imaging medium for this purpose. Adaptation of a VP-SEM for in-situ Mars surface studies will provide a new imaging capability (via SEI) that is at least an order of magnitude higher resolution than the Mars Hand Lens Imager (MAHLI) on the Mars Science Laboratory (Williams et al., 2015), and equal to or better than the achieved resolution of the Atomic Force Microscope on the Phoenix Mars lander (Pike et al., 2011). In addition, the MVP-SEM is capable of BSI and simultaneous chemical analysis of the imaged region. In this sense, the MVP-SEM can be regarded as an instrument suite that will provide a new set of information not achievable by any other instrument. The Miniaturized Variable Pressure Scanning Electron Microscope (MVP-SEM) was designed, built, and benchtop tested by a team at NASA’s Marshall Space Flight Center and Jet Propulsion Laboratory (JPL), Jacobs Space Exploration Group, Applied Physics Technologies, Inc. (AP-Tech), and Creare LLC, working with a team of technical and science collaborators. Benchtop testing was successful, proving concept feasibility. To date, the MVP-SEM has achieved an imaging resolution of <100 nm in the lab, and with continued optimization, even better performance (~50 nm resolution) is possible. Use in-situ on the lunar or other planetary surfaces would require some redesign to optimize instrument performance, but such an instrument would be equally useful.

Variable Pressure Scanning Electron Microscopy↗
NASA NTRS1995

The Spreading of Variable-Viscosity Axisymmetric Radial Gravity Currents: Applications to the Emplacement of Venusian 'Pancake' Domes

The Magellan images of Venus have revealed a number of intriguing volcanic features, including the steep-sided or 'pancake' domes. These volcanic domes or flows have morphologies that suggest formation by a single continuous emplacement of lava with a higher viscosity than that of the surrounding basaltic plains. Numerous investigators have suggested that such high viscosity is due to high silica content, leading to the conclusion that the domes are evidence of evolved magmatic products on Venus. However, viscosity depends on crystallinity as well as on silica content: high viscosity could therefore also be due to a cooler (and therefore higher crystal content) lava. Models of dome emplacement which include both cooling and composition factors are thus necessary in order to determine the ranges of crystallinity and silica content which might lead to the observed gross dome morphologies. Accordingly, in this study domes are modelled as radial viscous gravity currents with an assumed cooling-induced viscosity increase to include both effects. Analytical and numerical results indicate that pancake dome formation is feasible with compositions ranging from basaltic to rhyolitic. Therefore, observations of gross dome morphology alone are insufficient for determining composition and the domes do not necessarily represent strong evidence for evolved magmatism on Venus.

Sakimoto, S. E. H.↗
NASA NTRS2016

Large-Scale and Global Hydrology

Powered by the sun, water moves continuously between and through Earths oceanic, atmospheric, and terrestrial reservoirs. It enables life, shapes Earths surface, and responds to and influences climate change. Scientists measure various features of the water cycle using a combination of ground, airborne, and space-based observations, and seek to characterize it at multiple scales with the aid of numerical models. Over time our understanding of the water cycle and ability to quantify it have improved, owing to advances in observational capabilities, the extension of the data record, and increases in computing power and storage. Here we present some of the most recent estimates of global and continental ocean basin scale water cycle stocks and fluxes and provide examples of modern numerical modeling systems and reanalyses.Further, we discuss prospects for predicting water cycle variability at seasonal and longer scales, which is complicated by a changing climate and direct human impacts related to water management and agriculture. Changes to the water cycle will be among the most obvious and important facets of climate change, thus it is crucial that we continue to invest in our ability to monitor it.

land hydrology↗
NASA NTRS2008

The HD 163296 Circumstellar Disk in Scattered Light: Evidence of Time-Variable Self-Shadowing

We present the first multi-color view of the scattered light disk of the Herbig Ae star HD 163296, based on coronagraphic observations from the Hubble Space Telescope Advanced Camera for Surveys (ACS). Radial profile fits of the surface brightness along the disk's semi-major axis indicates that the disk is not continuously flared, and extends to approx.540 AU. The disk's color (V-I)=1.1 at a radial distance of 3.5" is redder than the observed stellar color (V-I)=0.15. This red disk color might be indicative of either an evolution in the grain size distribution (i.e. grain growth) and/or composition, both of which would be consistent with the observed non-flared geometry of the outer disk. We also identify a single ansa morphological structure in our F435W ACS data, which is absent from earlier epoch F606W and F814W ACS data, but corresponds to one of the two ansa observed in archival HST STIS coronagraphic data. Following transformation to similar band-passes, we find that the scattered light disk of HD 163296 is 1 mag arcsec(sup -2) fainter at 3.5" in the STIS data than in the ACS data. Moreover, variations are seen in (i) the visibility of the ansa(e) structures, in (ii) the relative surface brightness of the ansa(e) structures, and in (iii) the (known) intrinsic polarization of the system. These results indicate that the scattered light from the HD 163296 disk is variable. We speculate that the inner disk wall, which Sitko et al. suggests has a variable scale height as diagnosed by near-IR SED variability, induces variable self-shadowing of the outer disk. We further speculate that the observed surface brightness variability of the ansa(e) structures may indicate that the inner disk wall is azimuthally asymmetric. Subject headings: circumstellar matter - stars: individual (HD 163296) - planetary systems: formation - planetary systems: protoplanetary disks

Wisniewski, John P.↗
DOE OSTI2020

Seasonal mixing from intermittent flow drives concentration-discharge behaviour in a stream affected by coal mine drainage

Abandoned mining operations continue to severely degrade many ecosystems worldwide by releasing acidic water and/or heavy metals into surface and groundwater. Contaminant concentrations in affected streams vary with discharge in patterns that reflect both geochemical reactions and variable mixing of contaminated and non-contaminated waters. However, controls on concentration-discharge (C-Q) patterns remain unclear, particularly for constituents that experience changing solubility across redox and pH gradients. Understanding the C-Q behaviour of contaminants aids in predicting both downstream transport and effects on aquatic life under variable flow. Here, we examined the C-Q behaviours of non-reactive (Na, K, Ca, Mg, Cl - ) and reactive (Fe, Mn, Al, H + , SO 4 2- ) solutes in a stream contaminated with acid mine drainage in northeastern Ohio, USA. Concentration-discharge patterns at the watershed outlet primarily reflected mixing of contaminated baseflow with intermittent inputs of high pH water draining from a passive limestone treatment system into the stream. The treatment system acted as an ephemeral tributary that mitigated contamination in the stream by diluting solutes, raising pH, and driving metal precipitation, but only when flow was present during wet seasons. Consequently, AMD-derived reactive solutes (H + , Fe, Mn, Al) decreased with increasing stream discharge while relatively conservative solutes (e.g., Ca, Mg, K, Na) decreased only slightly or were chemostatic. This study highlights both the unique C-Q patterns of reactive solutes when compared to those of non-reactive solutes and the potential for intermittent streams to control C-Q behaviour in headwater catchments.

58 GEOSCIENCES↗
DOE OSTI2021

Using non-invasive MEMS pressure sensors for measuring building envelope air leakage

Micro-electromechanical systems (MEMS)-based sensors have seen significant improvements in accuracy and cost over the past several years, and due to the need for altitude sensing in unmanned aerial vehicles and wearable technologies, absolute pressure sensors have shown the most dramatic improvements. This paper investigates applications of MEMS sensors in commercial buildings, including pairing two absolute pressure sensors to determine differential pressures between different locations in and around buildings. Differential pressure measurements are commonly made in commercial buildings for a number of applications, including static pressure measurements for variable-speed supply fan control, air balancing in hospitals, and for envelope and duct air leakage testing. This paper focuses specifically on envelope air-leakage testing applications of these sensors. The use of continuous pressure measurements in addition to one-time non-intrusive outdoor airflow measurements of rooftop packaged units is investigated. A comparison with standardized leakage testing indicated that continuous measurements with MEMS pressure-sensors were able to estimate envelope leakage to within 3–16% of the standardized test result. In addition, the magnitude and stability of differential pressure differences that can be resolved with absolute pressure sensors are also investigated in the laboratory and the field. Results show that the sensors can be effectively used for pressures seen in low rise buildings with rooftop units.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2025

Tunable high Néel temperature and large anomalous Hall response in antiferromagnetic Weyl semimetal Mn 3 Sn 1− x Ga x thin films

Antiferromagnetic Weyl semimetals based on Mn 3 X(X = Ge, Sn, Ga) kagome compounds exhibit the same ferromagnetic-like responses, including anomalous Hall, Nernst, and magneto-optical effects, as recently discussed for altermagnets. Driven by the Berry curvature due to Weyl fermions, these materials show a disproportionately large magnitude of electromagnetic effects even in the absence of large magnetization. For applications it is crucial to realize these responses in a wide range of temperatures both below and above 300 K. While stoichiometric Mn 3 X materials do not offer optimal performance, we show that Mn 3 Sn 1−x Ga x sputtered films with a variable composition offers a tunable Néel temperature, T N ≈ 425 ± 6–500 ± 15 K, which is crucial for device applications, together with a large tunable anomalous Hall effect. Our thin film growth method enables continuous and precise control over the film composition between x = 0 and x = 1. Through a detailed magnetization and Hall transport, we establish the magnetic phase diagram for the hexagonal Mn 3 Sn 1−x Ga x . Our results reveal an enhanced T N and antichiral magnetic phase in Ga-doped Mn 3 Sn and an enhanced anomalous Hall magnitude in Sn-doped Mn 3 Ga compared to their stoichiometric undoped forms. Our work demonstrates a route to optimize the technologically relevant antiferromagnets for various applications.

Magnetic properties and materials↗
DOE OSTI2021

Regional Emissions Analysis of Light-Duty Battery Electric Vehicles

Light-duty battery electric vehicles (BEVs) can reduce both greenhouse gas (GHG) and criteria air pollutant (CAPs) emissions, when compared to gasoline vehicles. However, research has found that while today’s BEVs typically reduce GHGs, they can increase certain CAPs, though with significant regional variability based on the electric grid mix. In addition, the environmental performance of electric and gasoline vehicles is not static, as key factors driving emissions have undergone significant changes recently and are expected to continue to evolve. In this study, we perform a cradle-to-grave life cycle analysis using state-level generation mix and vehicle operation emission data. We generated state-level emission factors using a projection from 2020 to 2050 for three light-duty vehicle types. We found that BEVs currently provide GHG benefits in nearly every state, with the median state’s benefit being between approximately 50% to 60% lower than gasoline counterparts. However, gasoline vehicles currently have lower total NOx, urban NOx, total PM 2.5 , and urban PM 2.5 in 33%; 15%; 70%; and 10% of states, respectively. BEV emissions will decrease in 2050 due to a cleaner grid, but the relative benefits when compared to gasoline vehicles do not change significantly, as gasoline vehicles are also improving over this time.

33 ADVANCED PROPULSION SYSTEMS↗
NASA NTRS1972

Hot-salt stress-corrosion of titanium alloys as related to turbine operation

In an effort to simulate typical compressor operating conditions of current turbine engines, special test facilities were designed. Air velocity, air pressure, air dewpoint, salt deposition temperature, salt concentration, and specimen surface condition were systematically controlled and their influence on hot-salt stress-corrosion evaluated. The influence of both continuous and cyclic stress-temperature exposures was determined. The relative susceptibility of a variety of titanium alloys in commonly used heat-treated conditions was determined. The effects of both environmental and material variables were used to interpret the behavior of titanium alloys under hot-salt stress-corrosion conditions found in jet engines and to appraise their future potential under such conditions.

Gray, H. R.↗
NASA NTRS1984

Computer simulation of protein systems

Ligand binding to dihydrofolate reductase (DHFR) is discussed. This is an extremely important enzyme, as it is the target of several drugs (inhibitors) which are used clinically as antibacterials, antiprotozoals and in cancer chemotherapy. DHFR catalyzes the NADPH (reduced nicotinamide adenine dinucleotide phosphate) dependent reduction of dihydrofolate to tetrahydrofolate, which is used in several pathways of purine and pyrimidine iosynthesis, including that of thymidylate. Since DNA synthesis is dependent on a continuing supply of thymidylate, a blockade of DHFR resulting in a depletion of thymidylate can lead to the cessation of growth of a rapidly proliferating cell line. DHFR exhibits a significant species to species variability in its sensitivity to various inhibitors. For example, trimethoprim, an inhibitor of DHFR, binds to bacterial DHFR's 5 orders of magnitude greater than to vertebrate DHFR's. The structural mechanics, dynamics and energetics of a family of dihydrofolate reductases are studied to rationalize the basis for the inhibitor of these enyzmes and to understand the molecular basis of the difference in the binding constants between the species. This involves investigating the conformational changes induced in the protein on binding the ligand, the internal strain imposed by the enzyme on the ligand, the restriction of fluctuations in atom positions due to binding and the consequent change in entropy.

Osguthorpe, D. J.↗
NASA NTRS1984

On the dynamics in evaporating cloud envelopes

Cowie and McKee (1977) have conducted an analytical study of the case of an isolated, spherical cloud at rest in an infinite, hot medium. The present investigation is concerned with the theoretical model considered by Cowie and McKee for a thermally evaporating cloud. An analysis is conducted under the same conditions of inviscid flow with temperature equipartition. The current analysis allows for a continuous change in the saturation of the conductivity, rather than abrupt transitions from a classical to a fully saturated regime and back again, as in the model employed by Cowie and McKee. By suitable variable transformations, the momentum and energy equations can be reduced in the inviscid limit to a single equation for the Mach number in terms of a modified radius, and the solutions represented in a phase plane. An analytic model for the structure of the shock layer is developed.

Giuliani, J. L., Jr.↗
NASA NTRS1999

Method of Fabricating Chopped-Fiber Composite Piston

A three-dimensional piston molding is fabricated from a mixture of chopped, carbon tow filaments of variable length, which are prepregged with carbonaceous organic resins and/or pitches and molded by conventional molding processes into a near net shape, to form a carbon-fiber reinforced organic-matrix composite part. Continuous reinforcement in the form of carbon-carbon composite tapes or pieces of fabric can be also laid in the mold before or during the charging of the mold with the chopped-fiber mixture, to enhance the strength in the crown and wrist-pin areas. The molded chopped-fiber reinforced organic-matrix composite parts are then pyrolized in an inert atmosphere, to convert the organic matrix materials to carbon. These pyrolized parts are then densified by reimpregnation with resins or pitches, which are subsequently carbonized. Densification is also accomplished by direct infiltration with carbon by vapor deposition processes. Once the desired density has been achieved, the piston molds are machined to final piston dimensions, and piston ring grooves are added. To prevent oxidation and/or to seal the piston surface or near surface, the chopped-fiber piston is coated with ceramic and/or metallic sealants: and/or coated with a catalyst.

Rivers, H. Kevin↗
NASA NTRS2001

Kepler Mission: Detecting Earth-sized Planets in Habitable Zones

The Kepler Mission, which is presently in Phase A, is being proposed for launch in 5 years for a 4-year mission to determine the frequency of Earth-sized or larger planets in habitable zones in our galaxy. Kepler will be placed in an Earth-trailing orbit to provide stable physical environments for the sensitive scientific instruments. The satellite is equipped with a photometric system with the precision of 10E-5, which should be sufficient for detecting the transits of Earth-sized or larger planets in front of dwarf stars similar to the Sun. Approximately 100,000 or more sun-like stars brighter than the 14th apparently magnitude will be monitored continuously for 4 years in a preselected region of the sky, which is about 100 square degrees in size. In addition, Kepler will have a participating scientist program that will enable research in intrinsic variable stars, interacting binaries including cataclysmic stars and X-ray binaries, and a large number of solar analogs in our galaxy. Several ten thousand additional stars may be investigated in the guest observer program open to the whole world.

Kondo, Yoji↗
NASA NTRS2005

Unified Planetary Coordinates System: A Searchable Database of Geodetic Information

Over the past 40 years, an enormous quantity of orbital remote sensing data has been collected for Mars from many missions and instruments. Unfortunately these datasets currently exist in a wide range of disparate coordinate systems, making it extremely difficult for the scientific community to easily correlate, combine, and compare data from different Mars missions and instruments. As part of our work for the PDS Imaging Node and on behalf of the USGS Astrogeology Team, we are working to solve this problem and to provide the NASA scientific research community with easy access to Mars orbital data in a unified, consistent coordinate system along with a wide variety of other key geometric variables. The Unified Planetary Coordinates (UPC) system is comprised of two main elements: (1) a database containing Mars orbital remote sensing data computed using a uniform coordinate system, and (2) a process by which continual maintainance and updates to the contents of the database are performed.

Becker, K. J.a↗
NASA NTRS2005

X-Rays from Saturn and its Rings

In January 2004 Saturn was observed by Chandra ACIS-S in two exposures, 00:06 to 11:00 UT on 20 January and 14:32 UT on 26 January to 01:13 UT on 27 January. Each continuous observation lasted for about one full Saturn rotation. These observations detected an X-ray flare from the Saturn's disk and indicate that the entire Saturnian X-ray emission is highly variable -- a factor of $\sim$4 variability in brightness in a week time. The Saturn X-ray flare has a time and magnitude matching feature with the solar X-ray flare, which suggests that the disk X-ray emission of Saturn is governed by processes happening on the Sun. These observations also unambiguously detected X-rays from Saturn's rings. The X-ray emissions from rings are present mainly in the 0.45-0.6 keV band centered on the atomic OK$\alpha$ fluorescence line at 525 eV: indicating the production of X-rays due to oxygen atoms in the water icy rings. The characteristics of X-rays from Saturn's polar region appear to be statistically consistent with those from its disk X-rays, suggesting that X-ray emission from the polar cap region might be an extension of the Saturn disk X-ray emission.

Bhardwaj, Anil↗
NASA NTRS2019

Bringing Analysis Closer to Data: Developing a Visualization Tool for L2 Earth Science Satellite Data

Earth Science satellite missions provide a unique opportunity for scientists to visualize complex and multifaceted observations projected geospatially across maps of the Earth. While visualization tools can help scientists comprehend, analyze, and share data, visualizing Level-2 Earth Sciences data poses its own specific set of challenges. Since the geospatial information in Level-2 data files is stored as independent variables, the plotting process involves matching dimensional information from latitude and longitude with a desired variable. Variables are stored in different ways across various Earth Science data file formats, which complicates the process of extracting data and plotting variables from a given file without requiring extensive user input and prerequisite familiarity with the file type variable structure. In coordination with NASA’s Goddard Earth Sciences Data Information Services Center (GES DISC), the team developed a Level-2 Earth Science data visualization tool that aims to address some of the complexities associated with plotting Level-2 data. This tool offers command-line and user interface support for file and variable selection to accommodate varying use cases and degrees of user familiarity with the structure of a given file. The visualization tool is written in Python 3 and utilizes a modular approach to facilitate continued expansion and reuse. In addressing some common complications involved in plotting Level-2 Earth Sciences data, the tool aims to help to link the process of analysis more directly with data acquisition and visualization, bringing analysis closer to data across levels of processing.

Li, Angela W.↗
NASA NTRS2019

Editorial: North Pacific Environment and Paleoclimate from the Late Pleistocene to Present

The vast area of the North Pacific, spanning ~55° longitude, represents a challenge for documenting and understanding the geologic history of ocean, atmosphere, and terrestrial environmental change. This special issue highlights site-specific analyses to address various questions and provides clues that arise in response to continued North Pacific warming today in a rapidly changing climate (Figure 1). The emergence of new methods and novel application of existing methods serve to enhance our fundamental understanding of natural modes of climate variability driven by ocean and atmospheric circulation patterns, including the role of external (e.g., insolation) vs. internal forcing [e.g., El Niño Southern Oscillation (ENSO) and the Pacific Decadal Oscillation (PDO)]. Included in this volume are geographically diverse studies that present new and traditional methods for the interpretation of climate records drawn from pollen, macrofossils, tree rings, diatoms, grain size, and glacial studies. Many provide new geographic comparisons, such as Kamchatka and Hawaii, or emerge from novel geologic archives and environments, such as the marine shelf, a thermokarst lake, and a fossil forest.

Jones, Miriam C.↗