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At least 127 records · Page 7

Influence of various surface pretreatments on adherence of sputtered molybdenum disulfide to silver, gold, copper, and bronze

Solid film lubricants of radio frequency sputtered molybdenum disulfide (MoS2) were applied to silver, gold, copper, and bronze surfaces that had various pretreatments (mechanical polishing, sputter etching, oxidation, and sulfurization). Optical and electron transmission micrographs and electron diffraction patterns were used to interpret the film formation characteristics and to evaluate the sputtering conditions in regard to the film and substrate compatibility. Sputtered MoS2 films flaked and peeled on silver, copper, and bronze surfaces except when the surfaces had been specially oxidized. The flaking and peeling was a result of sulfide compound formation and the corresponding grain growth of the sulfide film. Sputtered MoS2 films showed no peeling and flaking on gold surfaces regardless of surface pretreatment.

Spalvins, T.↗

Remote analysis of planetary soils: X-ray diffractometer development

A system is described suitable for remote low power mineralogical analysis of lunar, planetary, or asteroid soils. It includes an X-ray diffractometer, fluorescence spectrometer, and sample preparation system. A one Curie Fe-55 source provides a monochromatic X-ray beam of 5.9 keV. Seeman-Bohlin or focusing geometry is employed in the camera, allowing peak detection to proceed simultaneously at all angles and obviating the need for moving parts. The detector system is an array of 500-600 proportional counters with a wire-spacing of 1 mm. An electronics unit comprising preamplifier, postamplifier, window discriminators, and storage flipflops requiring only 3.5 milliwatts was designed and tested. Total instrument power is less than 5 watts. Powder diffraction patterns using a flat breadboard multiwire counter were recorded.

Gregory, J. C.↗

Glancing incidence telescopes for space astronomy

A technique for determining the state of polarization of a light source by evaluating its image at the focus of a glancing telescope is reported. An analysis of the central disc of the diffraction image reveals if the light source is polarized, the plane of polarization, and the degree of polarization. When polarized light is incident at the aperture of a diffraction limited glancing telescope, the central disc of the diffraction pattern takes on an elliptical configuration. This ellipticity is caused by the tendency of the electric vector component in the plane of incidence to be absorbed by the reflecting material. As the state of polarization goes from plane polarized to decreasing degrees of elliptically polarized light, the ellipticity of the central disc goes from a maximum at plane polarization to zero at circular polarization. These curves give a direct relationship between the degree of polarization of a light source and the ellipticity of the central disc for this particular telescope, independent of the light source wavelength.

Alonso, J., Jr.↗

Electron petrography of Apollo sample 14310.

Thin sections prepared from Apollo sample 14310 have been examined with 100-kV transmission electron microscopy. The sample is composed principally of anorthite and pyroxene. The anorthites fall into two categories. The transitional anorthites that show the characteristic 'c' type diffraction maxima are characterized by very fine antiphase domain structures and some fine twinning. The body-centered anorthites that show no 'c' reflections are characterized by an absence of fine twinning and a less well-defined antiphase domain structure. Although both orthopyroxene and clinopyroxenes are reported in sample 14310, only clinopyroxenes were observed in this study and all show exsolution structures. The augite exsolved in pigeonite commonly is along lamellae parallel to (100), although (001) lamellae are also present. This unusual orientation was verified by diffraction patterns. The pigeonite commonly shows antiphase domains, attributed to stacking errors when the sample inverted from its high-temperature disordered form. In augite as the host phase, the pigeonite lamellae contain very complex structures including antiphase domains.

Smith, D. K.↗

Josephson junction interference grating.

The maximum current through multiple Josephson structures as a function of applied magnetic field is presented. Particular emphasis is placed on the Josephson penetration depth effects and geometrical considerations. The symmetrical and asymmetrical current feed two-, three-, four-, and five-junction gratings are analyzed and discussed. The Josephson penetration depth is shown to control the amplitude of the interference and diffraction patterns of the interference grating. In addition the interior-junction-length/interference-loop-area product is shown to control the operating mode of the interference grating. The dependence of the magnetic field sensitivity and interference pattern amplitude on the number of junctions is discussed.

Stuehm, D. L.↗

Automated thematic mapping and change detection of ERTS-A images

The author has identified the following significant results. For the recognition of terrain types, spatial signatures are developed from the diffraction patterns of small areas of ERTS-1 images. This knowledge is exploited for the measurements of a small number of meaningful spatial features from the digital Fourier transforms of ERTS-1 image cells containing 32 x 32 picture elements. Using these spatial features and a heuristic algorithm, the terrain types in the vicinity of Phoenix, Arizona were recognized by the computer with a high accuracy. Then, the spatial features were combined with spectral features and using the maximum likelihood criterion the recognition accuracy of terrain types increased substantially. It was determined that the recognition accuracy with the maximum likelihood criterion depends on the statistics of the feature vectors. Nonlinear transformations of the feature vectors are required so that the terrain class statistics become approximately Gaussian. It was also determined that for a given geographic area the statistics of the classes remain invariable for a period of a month but vary substantially between seasons.

Gramenopoulos, N.↗

Parabolic cylinder antennas

Some of the features of single and dual parabolic-cylinder reflector antenna systems are discussed in terms of wave conversions, field divergence, and wavefronts in Fresnel and Fraunhofer regions. Beam-squinting, by mechanical displacement and electrical phase gradient methods, is introduced together with the combination of these methods. In the case of dual parabolic cylinders there is also a discussion of surface-truncation, parametric representation of surface intersections, main-aperture blockage by the subsystem, and beam squinting. A few diffraction patterns are presented to illustrate the type of data available via a formulation equivalent to the complex-vector Kirchhoff-Kottler formulation. Main and cross-polarization components of the solution are available as they are inherently part of the field solution in the Cartesian coordinate system. A means of displaying main and cross-polarization components for arbitrary beam-scanning in space is outlined. Extensions to monopulse tracking with variable-beamwidth (zooming) capability are introduced.

Schmidt, R. F.↗

Automated thematic mapping and change detection of ERTS-A images

The author has identified the following significant results. A diffraction pattern analysis of MSS images led to the development of spatial signatures for farm land, urban areas and mountains. Four spatial features are employed to describe the spatial characteristics of image cells in the digital data. Three spectral features are combined with the spatial features to form a seven dimensional vector describing each cell. Then, the classification of the feature vectors is accomplished by using the maximum likelihood criterion. It was determined that the recognition accuracy with the maximum likelihood criterion depends on the statistics of the feature vectors. It was also determined that for a given geographic area the statistics of the classes remain invariable for a period of a month, but vary substantially between seasons. Three ERTS-1 images from the Phoenix, Arizona area were processed, and recognition rates between 85% and 100% were obtained for the terrain classes of desert, farms, mountains, and urban areas. To eliminate the need for training data, a new clustering algorithm has been developed. Seven ERTS-1 images from four test sites have been processed through the clustering algorithm, and high recognition rates have been achieved for all terrain classes.

Gramenopoulos, N.↗

Automated thematic mapping and change detection of ERTS-1 images

Results of an automated thematic mapping investigation using ERTS-1 MSS images are presented. A diffraction pattern analysis of MSS images led to the development of spatial signatures for farm land, urban areas, and mountains. Four spatial features are employed to describe the spatial characteristics of image cells in the digital data. Three spectral features are combined with the spatial features to form a seven dimensional vector describing each cell. Then, the classification of the feature vectors is accomplished by using the maximum likelihood criterion. Three ERTS-1 images from the Phoenix, Arizona area were processed, and recognition rates between 85% and 100% were obtained for the terrain classes of desert, farms, mountains and urban areas. To eliminate the need for training data, a new clustering algorithm has also been developed.

Gramenopoulos, N.↗

Optical instrumentation engineering in science, technology and society; Proceedings of the Sixteenth Annual Technical Meeting, San Mateo, Calif., October 16-18, 1972

Visual tracking performance in instrumentation is discussed together with photographic pyrometry in an aeroballistic range, optical characteristics of spherical vapor bubbles in liquids, and the automatic detection and control of surface roughness by coherent diffraction patterns. Other subjects explored are related to instruments, sensors, systems, holography, and pattern recognition. Questions of data handling are also investigated, taking into account minicomputer image storage for holographic interferometry analysis, the design of a video amplifier for a 90 MHz bandwidth, and autostereoscopic screens. Individual items are announced in this issue.

Katz, Y. H.↗

Interstellar scattering of pulsar radiation. 1: Scintillation

An investigation of the intensity fluctuations of 28 pulsars near 0.4 GHz indicates that scintillation spectra have a Gaussian shape, scintillation indices are near unity, and the scintillation bandwidth depends linearly on dispersion measure. Observations near 2.5 GHz suggest a strong dependence of the frequency at which scintillation indices fall below unity on dispersion measure. Multistation measurements of scintillation provide values or limits for the scale size of the scattering diffraction pattern. The dependences of scattering parameters on dispersion measure is discussed in terms of the current models. It is suggested that any line of sight through the galaxy encounters increasingly rare, increasingly large deviations of thermal electron density on the scale of 10 to the 11th power cm.

Backer, D. C.↗

A study to analyze six band multispectral images and fabricate a Fourier transform detector

An automatic Fourier transform diffraction pattern sampling system, used to investigate techniques for forestry classification of six band multispectral aerial photography is presented. Photographs and diagrams of the design, development and fabrication of a hybrid optical-digital Fourier transform detector are shown. The detector was designed around a concentric ring fiber optic array. This array was formed from many optical fibers which were sorted into concentric rings about a single fiber. All the fibers in each ring were collected into a bundle and terminated into a single photodetector. An optical/digital interface unit consisting of a high level multiplexer, and an analog-to-digital amplifier was also constructed and is described.

Shackelford, R. G.↗

Photoelectron spectra of the decomposition of ethylene on /110/ tungsten

The experimental apparatus used in the investigation consisted of an ultrahigh-vacuum chamber, a triple-grid, a microwave-excited resonance lamp, and an electron energy analyzer. The chemical nature of the chemisorbed species was studied, taking into account the energy distribution of photoemitted electrons, work function determinations, and low-energy electron diffraction patterns.

Plummer, E. W.↗

Effect of additions of coarse grains and fibers on the densification of a sinterable SiC

This note reports the effects on densification of independent additions of coarse equiaxed SiC grains and fibrous SiC that were mixed with fine beta-SiC to develop a duplex microstructure with improved toughness. The fine-matrix SiC did not contain excess boron and carbon. The equiaxed CVD beta-SiC was introduced in the fine beta-SiC matrix material in amounts of 5 and 10 wt%. Results indicate that the CVD beta-SiC, which is quite coarse, exhibits little indication of sinterability. The effect of these coarse-grained and fibrous additions on the sinterability of fine beta-SiC may result from a geometric type of interaction. This interpretation is reinforced by X-ray diffraction of the powders and sintered pellets via monochromatic CuK-alpha radiation; the diffraction patterns of the sintered composite structures are virtually a combination of those of the components. The addition of nonsinterable SiC to the sinterable material slightly reduces sinterability, the larger particles interacting geometrically with the fine matrix material to prevent complete densification.

Abe, H.↗

Cube corner retroreflector test and analysis

Cube corner retroreflectors with nominal dihedral angles of 90 deg 0 min 1.5 sec were fabricated, tested, and analyzed to determine the return energy in the annular ring of the far field diffraction pattern required by the Laser Geodynamic Satellite. Performance was assessed for variations in the dihedral angles, optical surfaces, and thermal environment. Despite relatively high independent axial and radial sensitivities, the changes caused by the anticipated thermal environment were found to be negligible; however, there were substantial variations between the analytical predictions and measured performance.-

Zurasky, J. L.↗

Diffraction effects on angular response of X-ray collimators

Angular responses have been measured for X-ray collimators with half-widths ranging from minutes of arc down to 10 arcsec. In the seconds-of-arc range, diffraction peaks at off-axis angles can masquerade as side lobes of the collimator angular response. Measurements and qualitative physical arguments lead to a rule of thumb for collimator design; namely, the angle of first minimum in the Fraunhofer single-slit diffraction pattern should be less than one-fourth of the collimator geometrical full-width at half-maximum intensity.

Blake, R. L.↗

Determination of particle size using measurement of scatter

A literature search was conducted to determine the state of the art particle size measurement by the light scatter technique. This technique may involve diffraction pattern analysis, location of minima and maxima in angular dependence of scattered light, magnitude of intensity verses angle, forward lobe scattered intensity ratio using two small angles, forward scatter in a small cone, and total scatter. Some of the more modern recordings and detection systems are video, holographic, and systems using optical processing.

Scott, R. L., Jr.↗

Method of calculating retroreflector-array transfer functions

Techniques and equations used in calculating the transfer functions to relate the observed return laser pulses to the center of mass of the Lageos satellite retroflector array, and for most of the retroreflector-equipped satellites now in orbit are described. The methods derived include the effects of coherent interference, diffraction, polarization, and dihedral-angle offsets. Particular emphasis is given to deriving expressions for the diffraction pattern and active reflecting area of various cube-corner designs.

Arnold, D. A.↗