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At least 919 records · Page 51

Transportation analysis and related design optimization of the Fermilab high-beta 650 MHz cryomodule

The Proton Improvement Plan-II (PIP-II) at Fermi National Accelerator Laboratory (FNAL) will create a new and vastly improved accelerator, which will be the source of high-energy particles for the experiments taking place at FNAL. The new linear accelerator (LINAC) contains several types of cryomodules, which are individual particle accelerators. The last cryomodule in the LINAC will be the High-Beta 650 (HB650), which will operate at 650 MHz. Each module is approximately 15 meters in length and 1.5 meters wide, weighs 13 tonnes, and shares many design features with three of the other cryomodules. The HB650 consists of two primary sections, the outer vacuum vessel and the components that reside within it, which will be cooled to cryogenic temperatures – the cold mass. Once assembly is complete at FNAL, it will be transported to one of three places: another location at FNAL, another national laboratory within the continental United States, or to a scientific partner in Europe. Any excitation the module experiences, such as going over rough roads when on a semitrailer, can create high stresses in components and cause failure if severe enough. Additionally, any delicate components with low resonant frequencies that match the excitation spectrum could achieve resonance, potentially causing a fatigue failure by repeated flexing. To ensure the successful transportation of the HB650, a transport analysis utilizing ANSYS simulation software has been performed on major subassemblies, as well as analysis of the subassemblies as a combined system. The optimization of components, design of support structures, and overall increasing of the lowest resonant frequencies have resulted in a cryomodule that will be better equipped to handle transportation and any large impact loads that come with it.

43 PARTICLE ACCELERATORS↗

Roundtable on Foundational Science for Carbon-Neutral Hydrogen Technologies (Technology Status Document)

This document summarizes the status of carbon-neutral hydrogen production, storage and transport, and utilization. The state of the art in the implementation, limitations, and challenges of these technologies are summarized. Sources of hydrogen are broadly categorized as hydrcoarbons or water and the processes used to convert these sources to hydrogen as catalytic, thermochemical, or electrochemical. Catalytic steam methane reforming of methane is the dominant process today. Other processes have smaller production volumes and the technology is less mature, but are being deployed at increasing rates, most notably water electrolyzers for hydrogen fueling stations. Efficient transport and storage of hydrogen is one of the major challenges facing a hydrogen-based energy economy. This arises in part from its low volumetric energy density necessitating very high pressures or cryogenic temperatures to store sufficient amounts for practical applications. High-pressure compressed hydrogen cylinders are the incumbent hydrogen storage technology for applications such as light-duty fuel cell electric vehicles, for example. The storage of hydrogen in materials or in chemicals is being pursued to address the issues associated with compression, such as parasitic energy loss and weight, size, and cost of storage containers. The complex nature of the chemical and physical processes involved in the uptake, storage, and release of hydrogen has slowed the discovery of suitable hydrogen storage materials. Both small and large-scale storage face the challenge of embrittlement of the storage media by hydrogen. There is a myriad of uses of hydrogen offering the promises of improving the efficiency of various applications and reducing or eliminating CO 2 emissions. These range from direct electrochemical conversion to electricity to power vehicles and grid-level stationary applications to combustion to production of chemicals and commodities. One of the most impactful applications in terms of reduction of CO 2 emissions is fuel cell passenger vehicles and heavy-duty vehicles such as class 8 trucks. The challenges facing widespread deployment of fuel cells, beyond the major hurdle of the lack of a hydrogen distribution infrastructure, are cost and durability, primarily related to the precious metal cathode catalyst and its durability. The other uses of hydrogen from conversion to hydrocarbons, polymer upcycling, and upgrading of bio-oils are at varying stages of maturity and also face fundamental challenges associated with catalytic processes and materials.

08 HYDROGEN↗

2022 Report - SRNL Aging and Lifetimes program tritium aging studies on structural alloys

This report documents work performed in fiscal year 2022 at SRNL in support of the Aging and Lifetimes program. This work is an enduring collaboration between SRNL and SNL to study tritium embrittlement of structural metals used in Gas Transfer System reservoirs. The measured data inform component lifetime assessments and predictions. Test coupons are thermally pre-charged with tritium and allowed to age at cryogenic temperatures to freeze out tritium diffusion and minimize off-gassing while allowing for decay helium levels to build. Coupons are removed and tested at planned intervals to measure how mechanical properties degrade as helium levels increase. This report summarizes test results from coupons which are in various stages of aging as they were tritium pre-charged in previous years, as well as documenting one new charging run.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Review of the application piezoelectric actuators for SRF cavity tuners

Modern particle accelerators and high-energy physics experiments that deployed up to several hundred of accelerating superconducting RF cavities require accurate frequency control. This is achieved by using cavity tuners typically actuated with the piezoelectric ceramic actuators. Piezoelectric ceramic actuators have become “standard” components of the SRF cavity tuner and depending on the application could be operated in different environments: in air, at cryogenic temperature, in vacuum, and submerged in liquid helium. Different applications place different requirements on the piezo actuators, but the important parameters common to all applications are the lifetime and reliability of the actuators. Several programs targeting the development of reliable piezo actuators are presented in this contribution.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Quantum Dot Based Solid-State Radiation Detectors

The detection and accurate identification of nuclear material is critical to the advancement of national security, medical technology, and environmental prosperity. The gold standard solid-state detector HPGe, suffers from high manufacturing costs and the need to operate at cryogenic temperatures to ensure reliable energy resolution. The other most common solid-state detector, cadmium zinc telluride (CZT), has the ability to operate at room temperature, but the grow process results in impurities decreasing performance. In this paper we have developed a continuous flow synthesis able to mass produce targeted size cadmium selenide quantum dots. The implementation of these QDs in QD/MEH-PPV composites has the ability to rival HPGe energy resolution at room temperature.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Conservation of Helium while Maintaining High System Purity

Recent helium shortages and helium price increases have lead to an increased emphasis being placed on conserving helium. The need to conserve helium must be balanced with need to maintain the high levels of purity necessary to prevent operational problems caused by contamination. Helium losses and contamination control are especially important for test stands that have cryogenic distribution systems operating continuously with frequent changeover of cryogenic temperature components that are being tested. This paper describes a mathematical model to estimate the quantity of helium lost and the purity of the helium after the pump and backfill procedure is complete. The process to determine the optimal time during pump down to cut off pumping and start backfilling is described. There is a tradeoff between trying to achieve the lowest possible pressure during pumping and the quantity of air leaking into the volume while pumping is occurring. An additional benefit of careful sel ection of pump and backfill parameters in conjunction with real-time pressure monitoring can reduce the labor and time required to complete a successful pump and backfill procedure. This paper is intended to be a tool for engineers to review their pump and backfill procedures and measured data to optimize helium losses, system purity, and labor required.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Surface structure studies in 2D and 3D Nb resonators using GI-XRD

Superconductor radio frequency (SRF) Nb-resonators are a key element in the development of new generations of particle accelerators as well as in the fabrication of 3D circuit QED architecture for quantum computing. Nevertheless, Niobium is extremally reactive to light elements such as C, N, O and H, and therefore to the impurities ordering under special conditions, e.g., cryogenic temperatures. Since these resonators are put through a series of metallurgical and chemical processes, the number of impurities in the solid increases in tens of ppm. Upon operational conditions ~1.6 K, Nb become vulnerable to H atoms ordering, which leads to the nucleation of secondary phases such as Nb-hydrides. Thereupon to the energy dissipation and eventually to the superconductivity breakdown known as Q-disease and potentially High-Field Q-slope. In this contribution, we present a detailed structural analysis by high-energy grazing-incidence X-ray diffraction of specimens extracted from 3D Nb resonators to shed light on the kinetic formation of the resulting secondary phases and their crystal phase identification upon cooling and heating cycles. To our knowledge, this is the first study carried out in resonators samples using a light source, shallow angles and temperatures near ~4 K. Consequently, this work opens new routes to understand the chemical and phase composition, crystal and electronic structure of the Nb surface at temperatures near the operating conditions as a strategy to improve the physical and functional properties of Nb superconducting resonators.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Ice Dusty Plasma (Final Report)

The NSF/DOE funding described in this final report was for constructing a substantial upgrade that would enable operation at variable and much lower cryogenic temperatures than was available in a previous experiment that operated from 2013 to 2019. Components for the upgraded experiment were designed and ordered from August to December 2019 and assembly began in early 2020. However, COVID-19 halted all lab work for much of 2020 and then when lab work resumed, numerous restrictions on lab access and in-lab time further impeded progress. Because of these delays, first plasma was obtained in late 2021 and a normal work pace resumed only in mid-2022. A no-cost extension was requested because the COVID-19 delays prevented work from being done at the anticipated rate. Constructing a water-ice experiment was a significant gamble because the parameter regime differs substantially from conventional laboratory plasmas and injecting water vapor into a plasma goes very much against convention as one normally goes to great lengths to avoid water vapor. This experiment opens a new frontier, namely the study of how charged ice grains form, grow, and interact with a plasma environment. The just-completed upgrade was a further gamble because it combines technology never previously used together (cryocoolers, plasma, and ice).

36 MATERIALS SCIENCE↗

Cryo Chiplets for Quantum Applications

Heterogeneous chiplets operating at cryogenic temperatures open up opportunities for the readout of qubits and related applications.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Progress Report for W911NF-23-1-0323: Development of Scalable Three-Dimensional Ion Traps for Quantum Information Processing

Trapped atomic ions are a promising platform for scalable quantum information processing. They lead in many key metrics such as single and two qubit gate fidelities, as well as quantum volume. We recently realized novel 3D ion traps with a high resolution 3D-printing process. The traps combine the scalability potential of surface chip traps with the superior trap performance of macroscopic 3D ion traps. Like photolithography, 3D-printing is a digitally defined process and hence allows for rapid iteration between design and fabrication. In contrast to photolithography, it also allows for fully defined 3D structures and, thus, is an ideal process to develop large, well-defined trap arrays with complex 3D electrode structures. Our current goal is to implement key procedures and perform critical measurements that justify incorporation of 3D-printed traps into large-scale quantum computing efforts. En route, we recently realized trapping in horizontal traps that are operating at cryogenic temperatures.

74 ATOMIC AND MOLECULAR PHYSICS↗

Axion Dark Matter EXperiment 2A Cavity Characterization

The axion is a highly motivated dark matter candidate for its capacity to solve the strong CP problem in quantum chromodynamics. To detect the axion, the 2A phase of the Axion Dark Matter EXperiment (ADMX) utilizes four identical cylindrical resonant cavities that can detect the photons converted from axions in a strong magnetic field. We found the quality factors for various tunings in cavity D, and we also learned that the piezo motors are not currently equipped to handle cryogenic temperatures. However, the measured quality factors are much more promising than those shown in the last 2A cooldown, improving by about a factor of five.

Maglione, Diego↗

Refinement and Modeling of a Blackbody-Based Calibration Method in the InfraBREAD Detector

The Broadband Reflector Experiment for Axion Detection (BREAD) is an ongoing experiment searching for the conversion of yet undiscovered axion-like dark matter particles to photons in the presence of a magnetic field. InfraBREAD, a sub-experiment of BREAD, uses a superconducting nanowire single photon detector (SNSPD), a high-efficiency and low-noise device, to specifically detect infrared-range photons produced by $\mathcal{O}$(eV) axion-like particles. The unique BREAD reflector setup allows for the focusing of all converted signal photons to a 1mm $\times$ 1mm SNSPD. However, when the detector is cooled to cryogenic temperatures during operation, uneven thermal contraction of reflector components may lead to a small shift in the location of the focal spot. A novel calibration method using blackbody radiation is proposed to locate the true focal spot of the detector \textit{in situ}. Through ray tracing simulations done in FRED Optical Engineering Software, this method is demonstrated to locate the focus to within 50 $\mu$m in three dimensions.

Rao, Shardul↗

Development of electro-optical quantum transducers based on three-dimensional superconducting cavities

Quantum transducers enable the conversion of quantum information and signals between different physical platforms. Based on the pioneering works in three-dimensional superconducting cavity technology developed at Fermilab, we are advancing the development of three-dimensional microwave-optical transducers and exploring their applications in quantum information processing and sensing. We present our progress in the design, fabrication, and characterization of three-dimensional microwave cavities integrated with bulk lithium niobate resonators. The material characterization using three-dimensional cavities based on a resonant-type method allows for understanding of complex permittivity and loss mechanism of electro-optic materials at cryogenic temperatures. We also evaluate the potential of the high-efficiency quantum transducers in enhancing the performance of quantum sensors for applications such as dark matter detection, compared to conventional homodyne detection approaches. This manuscript has been authored by Fermi Research Alliance, LLC under Contract No. DE-AC0207CH11359 with the U.S. Department of Energy, Office of Science, Office of High Energy Physics. This work is funded by the DOE's Early Career Research Program. This research used resources of the U.S. Department of Energy, Office of Science, National Quantum Information Science Research Centers, Superconducting Quantum Materials and Systems Center (SQMS) under Contract No. DE-AC02-07CH11359.

Zorzetti, Silvia↗

ODU Optimization of Nb3Sn supttering on SRF structures

High efficiency Superconducting radio-frequency (SRF) cavities are the key technology to cost-effective Continuous Wave (CW) SRF accelerators. Recent advances in Nb3Sn coatings on the inner surface of SRF cavities showed the potential for this material to significantly cut the capital and operating cost of SRF accelerators. The best results are presently achieved with Nb3Sn films coated by using the so-called vapor diffusion technique. Several alternative approaches have been and are being investigated such as electrochemical deposition, bronze routes, and sputtering. Among these techniques, magnetron sputtering is a versatile technique, which has been demonstrated to deposit Nb3Sn films on SRF cavities. The technique requires further development to compete with the results demonstrated on the cavities coated with the vapor diffusion techniques. The team to develop the novel technique includes a graduate student from Old Dominion University (ODU) and other experts. ODU Prof. Elsayed-Ali directs the graduate student to coat samples and cavities in the new coating system and analyze samples with different surface science techniques. Dr. Grigory Eremeev from Fermilab assists with 2.6 GHz cavities for coating, cavity characterization at cryogenic temperature, and result analysis. The research is funded by the Office of High Energy Physics at the US Department of Energy at both Fermilab and ODU

43 PARTICLE ACCELERATORS↗

Studies of Helium Behavior in Uranium Hexafluoride

Several issues have arisen from experimental observations and/or theoretical postulation related to the behavior of helium in uranium hexafluoride (UF 6 ) matrices and how it may impact the ability to use this noble gas to quantify the fill date of the cylinder. A series of experiments was conducted to address several such issues, and the results and implications are reported here. Two issues relate to bias in the helium measurement due to ambient air from extraneous sources such as atmospheric air or from potential holdup in a large, activated alumina chemical trap. These issues are really a question of differential retention of helium versus three other inert gas isotopes (representative of other noble gases found in air) used as a calibration for air in leakage. Discernable bias was not detected in either case. Another issue had to do with helium potentially brought into the cylinder by a liquid UF 6 fill and subsequently released as the material solidifies and/or during storage. The solubility of helium in liquid UF 6 was measured to investigate this theory. The experiment quantified the potential magnitude of the initial helium contribution if present. The final issue was that of retention of helium in solid UF 6 . Investigation of this theory necessitated quantifying both the solubility and the diffusivity of helium in UF 6 . In one experiment, the solubility was measured at cryogenic temperature, allowing quantification of helium in solid UF 6 such as would be found in a cold trap. In a second experiment, transport of helium into and through a macroscopic plug of solid UF 6 was examined. The transport was very slight although apparently detectible. Effectively, only an upper limit to the transport could be determined, but that limit implied that helium holdup in solid UF 6 is a real possibility.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

High Insulating Vacuum Pump Cart Analysis

To maintain superconductive and cryogenic temperature, it is necessary to utilize high vacuum to eliminate convective heat transfer. To reach the desirable pressure of 10^-6 Torr at a reasonable time, the vacuum pumps and vessel geometry are evaluated for compatibility. Based on the analysis, a list of dry scroll pumps and turbomolecular pumps are recommended.

Chicas, Kelly [Illinois U., Urbana]↗

X-ARAPUCA Photon Detectors in SBND

The Short-Baseline Near Detector (SBND) is a liquid argon time projection chamber (LArTPC) for detecting neutrinos from Fermilab's Booster Neutrino Beam. Located 110 m downstream of the beam target, SBND collects both ionization electrons and scintillation photons from particle interactions within the detector volume. The photon detection system (PDS) consists of both PMTs and X-ARAPUCAs, a novel technology featuring large area cost-effective coverage with single photo-electron resolution at cryogenic temperatures. SBND utilizes two types of X-ARAPUCAs: one sensitive to vacuum ultra-violet (VUV) scintillation light produced and one sensitive to visible light for the light reflected off TPB-coated reflective foils. SBND is the only experiment currently testing the X-ARAPUCA technology in a neutrino beam over a period of several years, and will provide critical information for deployment in future detectors like DUNE. This poster will cover the calibration and early performance of X-ARAPUCAs in SBND.

Dalager, Olivia [Fermilab]↗