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All sourcesNASA NTRSDOE OSTI
NASA NTRS1989

Oxidation effects on the mechanical properties of SiC fiber-reinforced reaction-bonded silicon nitride matrix composites

The room temperature mechanical properties of SiC fiber reinforced reaction bonded silicon nitride composites were measured after 100 hrs exposure at temperatures to 1400 C in nitrogen and oxygen environments. The composites consisted of approx. 30 vol percent uniaxially aligned 142 micron diameter SiC fibers in a reaction bonded Si3N4 matrix. The results indicate that composites heat treated in a nitrogen environment at temperatures to 1400 C showed deformation and fracture behavior equivalent to that of the as-fabricated composites. Also, the composites heat treated in an oxidizing environment beyond 400 C yielded significantly lower tensile strength values. Specifically in the temperature range from 600 to 1000 C, composites retained approx. 40 percent of their as-fabricated strength, and those heat treated in the temperatures from 1200 to 1400 C retained 70 percent. Nonetheless, for all oxygen heat treatment conditions, composite specimens displayed strain capability beyond the matrix fracture stress; a typical behavior of a tough composite.

Bhatt, Ramakrishna T.↗
NASA NTRS1992

Oxidation effects on the mechanical properties of a SiC-fiber-reinforced reaction-bonded Si3N4 matrix composite

The room-temperature mechanical properties of SiC fiber reinforced reaction bonded silicon nitride composites were measured after 100 hrs exposure at temperatures to 1400 C in nitrogen and oxygen environments. The composites consisted of approx. 30 vol percent uniaxially aligned 142 micron diameter SiC fibers in a reaction bonded Si3N4 matrix. The results indicate that composites heat treated in a nitrogen environment at temperatures to 1400 C showed deformation and fracture behavior equivalent to that of the as-fabricated composites. Also, the composites heat treated in an oxidizing environment beyond 400 C yielded significantly lower tensile strength values. Specifically in the temperature range from 600 to 1000 C, composites retained approx. 40 percent of their as-fabricated strength, and those heat treated in the temperatures from 1200 to 1400 C retained 70 percent. Nonetheless, for all oxygen heat treatment conditions, composite specimens displayed strain capability beyond the matrix fracture stress; a typical behavior of a tough composite.

Bhatt, Ramakrishna T.↗
NASA NTRS1993

Flexure Test For Off-Axis Unidirectional Composites

Improved flexure test yields data on ply strength of off-axis unidirectional composite material. Rotatable end supports allow ends of specimen to twist freely. End supports apply only vertical loads, making simple three-point bending test. Ply-strength data provide basis for predicting onset of damage in composite structures and serve as measure of fiber-matrix adhesion.

Crews, John H., Jr.↗
NASA NTRS1928

Welding of high chromium steels

A brief description is given of different groups of high chromium steels (rustless iron and stainless steels) according to their composition and more generally accepted names. The welding procedure for a given group will be much the same regardless of the slight variations in chemical composition which may exist within a certain group. Information is given for the tensile properties (yield point and ultimate strength) of metal sheets and welds before and after annealing on coupons one and one-half inches wide. Since welds in rustless iron containing 16 to 18 percent chromium and 7 to 12 percent nickel show the best combination of strength and ductility in the 'as welded' or annealed condition, it is considered the best alloy to use for welded construction.

IRON - STAINLESS↗
NASA NTRS1951

Plastic Stress-strain Relations for 75S-T6 Aluminum Alloy Subjected to Biaxial Tensile Stresses

In this investigation, the material tested was a 75S-T6 aluminum alloy and the stresses were essentially biaxial and tensile. The biaxial tensile stresses were produced in a specially designed testing machine by subjecting a thin-walled tubular specimen to axial tension and internal pressure. Plastic stress-strain relations for various biaxial stress conditions were obtained using a clip-type SR-4 strain gage. Three types of tests were made: Constant-stress-ratio tests, variable-stress-ratio tests, and special tests. The constant-stress-ratio test results gave control data and showed the influence of biaxial stresses on the yield, fracture, and ultimate strength of the material. By means of the variable-stress-ratio tests, it is possible to determine whether there is any significant difference between the flow and deformation type of theory. Finally, special tests were conducted to check specific assumptions made in the theories of plastic flow. The constant-stress-ratio tests show that the deformation theory based on the octahedral, effective; or significant stress-strain relations is in approximate agreement with the test results. The variable-stress-ratio tests show that both the deformation and flow theory are in equally good agreement with the test results.

Marin, Joseph↗
NASA NTRS1994

Statistical design study of lunar ceramic

Fabrication of a lunar ceramic was conducted according to a statistically designed experiment. The method of cold pressing was used since the consumption of electrical energy is kept to a minimum (a priority in the lunar environment). This traditional fabrication technique also provides an initial data source on which further investigations can be based. Results obtained from using two percent binder, a cold pressing pressure of 276 MPa, and 24 hours sintering time yielded the greatest compressive strength of 247 MPa. Analysis of each variable's influence on the compressive strength is also presented.

Effinger, Mike↗
NASA NTRS1999

Craters as an Indicator of Martian Regolith Thickness

Two craters (D approx.900 m) found in MOC images of Xanthe Terra have concentric terraced morphologies, where one crater lies within a second, larger crater. This type of morphology has been documented on the Moon and attributed to an impact into fragmental material overlying a more competent substrate. These craters offer a mechanism by which to estimate thickness of unconsolidated surface material over large areas on Mars. Such measurements may constrain deflation rates and volume estimates of hydrologic reservoirs on Mars and yield information on the strength of the local bedrock. Additional information is contained in the original extended abstract.

Gilmore, M. S.↗
NASA NTRS1961

Optimum Design of Insulated Compression Plates Subjected to Aerodynamic Heating

A method to determine the optimum thicknesses of insulation and load-carrying structure has been applied to insulated compression plates subjected to aerodynamic heating. The optimum design results in the lowest combined weight of insulation and load-carrying plate. Load parameters which included the imposed load, insulation conductivity and density, and flight time were found for design strength criteria of compressive yield, compressive buckling, and postbuckling failure. Charts of optimum total weight were prepared for 2024-T3 aluminum alloy, HK3lA magnesium alloy, 17-7 PH stainless steel, and Inconel X for each design criterion. The results show that 17-7 PH stainless steel and Inconel X are most efficient for compressive yield stress and that HK3lA magnesium is most efficient for buckling. HK31A magnesium is also most efficient for the postbuckling failure criterion except under conditions of light loading and long flight periods; under such conditions uninsulated Inconel X may be superior for environmental temperature less than 1,200 F. Insulated magnesium is more efficient than insulated aluminum because the lower density of magnesium permits the use of thick plates with large heat capacity. When more than one failure mode was applied to a design, it was found that the minimum weight structure was one in which all modes of failure occurred at the design load.

Davidson, John R.↗
NASA NTRS2007

Polymer-Layered Silicate Nanocomposites for Cryotank Applications

Previous composite cryotank designs have relied on the use of conventional composite materials to reduce microcracking and permeability. However, revolutionary advances in nanotechnology derived materials may enable the production of ultra-lightweight cryotanks with significantly enhanced durability and damage tolerance, as well as reduced propellant permeability. Layered silicate nanocomposites are especially attractive in cryogenic storage tanks based on results that have been reported for epoxy nanocomposite systems. These materials often exhibit an order of magnitude reduction in gas permeability when compared to the base resin. In addition, polymer-silicate nanocomposites have been shown to yield improved dimensional stability, strength, and toughness. The enhancement in material performance of these systems occurs without property trade-offs which are often observed in conventionally filled polymer composites. Research efforts at NASA Glenn Research Center have led to the development of epoxy-clay nanocomposites with 70% lower hydrogen permeability than the base epoxy resin. Filament wound carbon fiber reinforced tanks made with this nanocomposite had a five-fold lower helium leak rate than the corresponding tanks made without clay. The pronounced reduction observed with the tank may be due to flow induced alignment of the clay layers during processing. Additionally, the nanocomposites showed CTE reductions of up to 30%, as well as a 100% increase in toughness.

Miller, Sandi G.↗
NASA NTRS2014

Bone Metabolism on ISS Missions

Spaceflight-induced bone loss is associated with increased bone resorption (1, 2), and either unchanged or decreased rates of bone formation. Resistive exercise had been proposed as a countermeasure, and data from bed rest supported this concept (3). An interim resistive exercise device (iRED) was flown for early ISS crews. Unfortunately, the iRED provided no greater bone protection than on missions where only aerobic and muscular endurance exercises were available (4, 5). In 2008, the Advanced Resistive Exercise Device (ARED), a more robust device with much greater resistance capability, (6, 7) was launched to the ISS. Astronauts who had access to ARED, coupled with adequate energy intake and vitamin D status, returned from ISS missions with bone mineral densities virtually unchanged from preflight (7). Bone biochemical markers showed that while the resistive exercise and adequate energy consumption did not mitigate the increased bone resorption, bone formation was increased (7, 8). The typical drop in circulating parathyroid hormone did not occur in ARED crewmembers. In 2014, an updated look at the densitometry data was published. This study confirmed the initial findings with a much larger set of data. In 42 astronauts (33 male, 9 female), the bone mineral density response to flight was the same for men and women (9), and those with access to the ARED did not have the typical decrease in bone mineral density that was observed in early ISS crewmembers with access to the iRED (Figure 1) (7). Biochemical markers of bone formation and resorption responded similarly in men and women. These data are encouraging, and represent the first in-flight evidence in the history of human space flight that diet and exercise can maintain bone mineral density on long-duration missions. However, the maintenance of bone mineral density through bone remodeling, that is, increases in both resorption and formation, may yield a bone with strength characteristics different from those that existed before space flight. Studies to assess bone strength after flight are underway at NASA, to better understand the results of bone remodeling. Studies are also underway to evaluate optimized exercise protocols and nutritional countermeasures. Regardless, there is clear evidence of progress being made to protect bone during spaceflight.

Smith, S. M.↗
NASA NTRS2016

Engineering Polymer Blends for Impact Damage Mitigation

Structures containing polymers such as DuPont's Surlyn® 8940, demonstrate puncture healing when impacted by a 9 millimeter projectile traveling from speeds near 300 meters per second (1,100 feet per second) to hypervelocity impacts in the micrometeoroid velocity range of 5 kilometers per second (16,000 feet per second). Surlyn® 8940 puncture heals over a temperature range of minus 30 degrees Centigrade to plus 70 degrees Centigrade and shows potential for use in pressurized vessels subject to impact damage. However, such polymers are difficult to process and limited in applicability due to their low thermal stability, poor chemical resistance and overall poor mechanical properties. In this work, several puncture healing engineered melt formulations were developed. Moldings of melt blend formulations were impacted with a 5.56 millimeter projectile with a nominal velocity of 945 meters per second (3,100 feet per second) at about 25 degrees Centigrade, 50 degrees Centigrade and 100 degrees Centigrade, depending upon the specific blend being investigated. Self-healing tendencies were determined using surface vacuum pressure tests and tensile tests after penetration using tensile dog-bone specimens (ASTM D 638-10). For the characterization of tensile properties both pristine and impacted specimens were tested to obtain tensile modulus, yield stress and tensile strength, where possible. Experimental results demonstrate a range of new puncture healing blends which mitigate damage in the ballistic velocity regime.

Gordon, Keith L.↗
NASA NTRS2017

Exotic Optical Fibers and Glasses: Innovative Material Processing Opportunities in Earth's Orbit

Exotic optical fibers and glasses are the platform material for photonics applications, primarily due to their superior signal transmission (speed, low attenuation), with extending bandwidth deep into the infrared, exceeding that of silica fibers. Gravitational effects (convection sedimentation) have a direct impact on the phase diagram of these materials and influence melting properties, crystallization temperatures, and viscosity of the elemental mix during the manufacturing process. Such factors constitute limits to the yield, transmission quality, and strength and value of these fibers; they also constrain the range of applications. Manufacturing in a gravity-free environment such as the Earth’s Orbit also helps with other aspects of the fabrication process (i.e., improved form factor of the manufacturing unit, sustainability). In this article, revolutionary developments in the field of photonics over the past decade merge with the paradigm shift in the privatization of government-owned capabilities supporting a more diverse infrastructure (parabolic, suborbital, orbital), reduced price, and increased frequency to access space and the microgravity environment. With the increased dependence on data (demand, bandwidth, efficiency), space and the microgravity environment provide opportunities for optimized performance of these exotic optical fibers and glasses underlying the development of enabling technologies to meet future data demand. Existing terrestrial markets (Internet, telecommunications, market transactions) and emerging space markets (onorbit satellite servicing, space manufacturing, space resources, space communications, etc.) seem to converge, and this innovative material processing opportunity of exotic optical fibers and glasses might just be that ‘‘killer app’’: technologically competitive, economically viable, and with the ability to close the business case.

Ioana Cozmuta↗
NASA NTRSDate not supplied

TPSAS-NF1676L-31264-DND

Nonlinear unsteady aerodynamic models (TSD, Euler/Navier-Stokes (RANS), LES) are complex, expensive solutions. CFD used by industry mostly for steady/static loads cases. Limit Cycle Oscillation (LCO) is an equilibrium point of the nonlinear aeroelastic system induced by nonlinear unsteady aerodynamics (shock dynamics, separated flow) and/or nonlinear structural dynamics (geometric and material nonlinearities). While Euler solutions can generate LCOs, viscosity yields improved accuracy (shock strength, position). Most common aeroelastic CFD codes currently consist of nonlinear unsteady aerodynamics with linear structural dynamics. Van der Pol system is a simple example of LCOs.

Walter A Silva↗
NASA NTRS2022

Kink Oscillation of a Flux Rope During a Failed Solar Eruption

We report a decaying kink oscillation of a flux rope during a confined eruptive flare, observed off the solar limb by SDO/AIA, that lacked a detectable white-light coronal mass ejection. The erupting flux rope underwent kinking, rotation, and apparent leg–leg interaction during the event. The oscillations were observed simultaneously in multiple AIA channels at 304, 171, and 193 Å, indicating that multithermal plasma was entrained in the rope. After reaching the overlying loops in the active region, the flux rope exhibited large-amplitude, decaying kink oscillations with an apparent initial amplitude of 30 Mm, period of about 16 min, and decay time of about 17 min. We interpret these oscillations as a fundamental standing kink mode of the flux rope. The oscillation polarization has a clear vertical component, while the departure of the detected waveform from a sinusoidal signal suggests that the oscillation could be circularly or elliptically polarized. The estimated kink speed is 1080 km s−1, corresponding to an Alfv'en speed of about 760 km s−1. This speed, together with the estimated electron density in the rope from our DEM analysis, ne ≈ (1.5–2.0) ×109 cm−3, yields a magnetic field strength of about 15 G. To the best of our knowledge, decaying kink oscillations of a flux rope with non-horizontal polarization during a confined eruptive flare have not been reported before. These oscillations provide unique opportunities for indirect measurements of the magnetic-field strength in low-coronal flux ropes during failed eruptions.

Pankaj Kumar↗
NASA NTRSDate not supplied

Space Environmental Effects on Additively Manufactured (AM) Parts on MISSE-9/10

The Materials on International Space Station Experiment (MISSE) experiments have made a continuous presence on the ISS and allowed for testing of performance and durability of materials exposed to the Low Earth Orbit (LEO) space environment. Additive Manufacturing (AM) has been included on several MISSE flights, and many companies (Made in Space and Stratasys) and NASA centers wanted to test various AM material samples. The goal of studying Space Environmental Effects on AM Parts with MISSE 9/10 was to fly promising metal and polymer AM material samples (dogbones) that could have future manufacturing capabilities in space and conduct post-flight analysis of these materials via mechanical and optical properties. On these flights, MISSE-9 contained three Inconel and 12 polymer samples and MISSE-10 included three Inconel and 16 polymer samples. Before flying to the ISS, all the samples underwent thermal vacuum bakeout (at 60°C for 24 hours and 10-6 torr). After bakeout, control and flight experiments were weighed, and optical properties were taken. Optical properties such as solar absorptance and infrared emittance were taken on the control samples and the flight samples (preflight and postflight). To understand more about the mechanical properties of the AM samples, tensile testing was conducted on the samples to determine the yield and ultimate tensile strength of the dogbone samples against the control. Lastly, the torque on the fasteners securing the dogbone samples were loosened and measured using a torque wrench, and they were compared to their preflight torque specification required. Optical properties and masses were recorded before flight, and the postflight results were recorded and collected in June 2022 to study the effects. With the postflight analysis, NASA engineers can now better characterize how UV radiation and thermal cycling affect the material properties.

Materials on International Space Station Experimen↗
NASA NTRS2026

Mechanical Design and Operation of a Novel Lunar Environment Structural Test Rig (LESTR)

The Lunar Environment Structural Test Rig (LESTR) was developed to address a critical gap in mechanical property data for metal alloy wire materials under lunar-relevant conditions down to 40 K. Conventional aerospace material databases provide thermophysical properties for bulk metals over a wide temperature range, but validated mechanical and physical property data below 77 K, particularly for small-diameter wires, remain limited and are generally the exception rather than the rule. These conditions are essential for Artemis mission hardware such as shape memory alloy (SMA) rover tires. LESTR’s design requirements were to combine a high-stiffness electrodynamic load frame with closed- cycle cryogenic cooling, high-vacuum capability (10–6 torr), and noncontact optical strain measurement to enable tensile, four-point bend, and fatigue testing of wires or other materials and geometries at temperatures from 40 to 125 K. These considerable requirements were merged with the need to lower the barrier of testing for the end user as measured in terms of cost-per-test cycle, safety improvement, and reduction in upkeep costs associated with state-of-the-art solutions associated with cryomechanical material characterization. The system incorporates modular gripping and alignment fixtures; precision thermal management using cryocoolers and embedded heaters; and integrated instrumentation for displacement, load, temperature, and vacuum control. Calibration procedures establish correlations between tooling and specimen temperature, ensuring accurate thermal conditions across the design envelope unbound by cryofluid conditions in heritage immersion-based test systems. Initial validation tests using Inconel (Special Metals Corp.) wire demonstrated accurate ultimate strength and post-yield behavior. The load frame operation was also verified under representative service conditions, including thermal cycling and prolonged fatigue loading. By generating mechanical property data at ultralow temperatures, LESTR fills a critical gap in existing materials databases and provides a scalable platform for iterative alloy development and durability assessment for planetary hardware. This capability supports NASA’s long-term objectives for surface exploration by enabling design confidence for components operating in extreme cryogenic environments.

LESTR↗
DOE OSTI2021

Flexural strength of a conventionally processed and additively manufactured debased 94% alumina

Mechanical strength of a 94 wt% debased alumina was measured using ASTM-C1161 specimens fabricated via conventional and lithography-based ceramic manufacturing (LCM) methods. The effects of build orientation and a 1500°C wet hydrogen fire added to the LCM firing sequence on strength were evaluated. Additionally, a Weibull fit to the conventional flexural specimen data yielded 20 and 356 MPa for the modulus and characteristic strength, respectively. Weibull fits of the data from the LCM specimens yielded moduli between 7.5 and 11.3 and characteristics strengths between 333 and 339 MPa. A Weibull fit to data from LCM specimens subjected to the wet hydrogen fire yielded 14.2 and 376 MPa for the modulus and characteristic strength, respectively. The 95% confidence intervals for all Weibull parameters are reported. Average Archimedes bulk densities of LCM and conventional specimens were 3.732 and 3.730 g/cm 3 , respectively. Process dependent differences in surface morphology were observed in scanning electron microscope (SEM) images of specimen surfaces. SEM images of LCM specimen cross-sections showed alumina grain texture dependent on build direction, but no evidence of porosity concentrated in planes between printed layers. Fracture surfaces of LCM and conventionally processed specimens revealed hackle lines and mirror regions indicative of fracture initiation at the sample surface rather than the interior.

36 MATERIALS SCIENCE↗
NASA NTRS1987

Lithospheric structure on Venus from tectonic modelling of compressional features

In previous studies, extensional models were used that incorporated realistic rheologies in order to constrain lithospheric structure. Lithospheric modelling is considered herein from the standpoint of compressional deformation. Features of presumed compressional tectonic origin are reviewed and a model for compressional folding based on lithospheric strength envelopes are presented that include the effects of both brittle and ductile yielding as well as finite elastic strength. Model predictions are then compared with the widths and spacings of observed tectonic features and it is concluded that the results are consistent with a thin crust overlying a relatively stronger mantle, with thermal gradients probably in the range of 10 to 15 deg/km.

Banerdt, W. B.↗