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All sources NASA NTRS DOE OSTI

DOE OSTI2020

Developing Novel Electrode Materials for Aqueous Battery

Aqueous rechargeable batteries (ARBs) are particularly interesting for large-scale energy storage due to their inherent safety, superior rate capability and environmental friendliness. However, ARBs are not widely explored as yet, so we proposed designing, preparing, and testing new intercalation materials for ARBs. Development of these electrodes will enrich the electrode chemistry of existing ARBs, open up new avenues for high-performance electrode and system design, offer opportunities to improve energy efficiency of water purification, and inform future development of controls strategies and management systems for stationary aqueous energy storage. Researchers from Bosch and LBNL collaborated on relevant materials to pursue and the general design of experiments to implement. Bosch researchers prepared and fabricated the electrodes and used various characterization facilities at LBNL to evaluate electrode performance in-device. The research collaboration resulted in identifying electrode materials capable of Na + and Ca 2+ intercalation in aqueous systems, and their application for desalination was explored using testing platform available at LBNL. Besides the specific materials and their performance, the data collected during the study was also used to inform a broader techno-economic analysis to compare intercalation-desalination technique to commercially available capacitive desalination approach. Outcomes of this research effort will be published in peer-reviewed journals.

25 ENERGY STORAGE↗

DOE OSTI2026

Prioritizing Uncertainties in Hydrogen Contribution to Risk in Post-Crash Outcomes for Rail

This report presents analysis from Sandia National Laboratories predicting contributions to risk associated with the use of hydrogen technology for rail. Event sequence diagrams are used to describe possible accident scenarios and progressions. Initiating event frequencies and branch event probabilities for each scenario are quantified with uncertainty using distributions fit to Federal Railroad Administration and U.S. Department of Transportation Pipeline and Hazardous Materials Safety Administration data on applicable accidents from 2000 to 2020. Uncertainty is propagated through the event sequence diagram to estimate the frequency and conditional probability of accident end states. The analysis identifies four scenarios with significant contributions to risk from hydrogen that are predicted to occur relatively frequently, which may inform priorities for reducing uncertainty. These scenarios are 1) overpressure events resulting from collisions with hydrogen release due to mechanical damage and delayed ignition, 2) jet fire events resulting from collisions with hydrogen release due to mechanical damage and immediate ignition, 3) jet fires resulting from fire or explosion initiating events involving the hydrogen tank and correct operation of the thermally-activated pressure relief device (TPRD) subsequent to the thermal insult, and 4) pressure burst resulting from fire or explosion initiating events involving the hydrogen tank and failure of the TPRD. Delayed and immediate hydrogen ignition probabilities are identified as being highly uncertain and potential candidates for reducing conservatism in the predicted frequencies for these two scenarios.

08 HYDROGEN↗

DOE OSTI2025

Robust Polymer Electrolytes For Flexible Energy Storage (CRADA Final Report)

As part of the Cyclotron Road program, Anthro Energy investigated the formulation, synthesis, and application of advanced supramolecular compounds for lithium-ion batteries. Anthro Energy developed and tested formulations and chemistries to create polymeric materials with improved mechanical strength, safety, and electrochemical performance. These materials were explored for use in next-generation batteries with a variety of form factors. Initially, Anthro Energy tested these materials to create flexible and deformable batteries, which are in high demand for the wearable/flexible electronics industry. In future work, Anthro Energy’s materials may be applied to create rigid structural batteries, or to enable novel chemistries such as silicon anodes or lithium metal anodes. In the process of testing the company’s unique lithium-ion cells, Anthro Energy explored the development and utilization of novel cell components, cell architectures, and testing protocols. These next-generation flexible and structural batteries may eventually enable new categories of electronic devices.

25 ENERGY STORAGE↗

DOE OSTI2012

SILER: Seismic-Initiated events risk mitigation in Lead-cooled Reactors

SILER is a Collaborative Project, partially funded by the European Commission, aimed at studying the risk associated to seismic initiated events in Generation IV Heavy Liquid Metal reactors and developing adequate protection measures. The attention is focused on the evaluation of the effects of earthquakes (with particular regards to beyond design seismic events) and to the identification of mitigation strategies, acting both on structures and components design (as well as on the development of seismic isolation devices) which can also have positive effects on economics, leading to an high level of plant design standardization. Attention is also devoted to the identification of plant layout solutions able to avoid risks of radioactive release from both the core and other structures (i.e. the spent fuel storage pools). Specific effort is paid to the development of guidelines and design recommendations for addressing the seismic issue in next generation reactor systems. In addition, consideration will be devoted to transfer the knowledge developed in the project to Generation III advanced systems, in line with the objective of the SNE-TP SRA to support present and future Light Water Reactors and their further development, for which safety issues are key aspects to be addressed. Note, in this respect, that the benefits of base isolation in terms of response to design seismic actions are already widely recognized for Generation III LWRs, along with the possibility of a significant standardization of structural and equipment design. SILER activities started on October 1 st 2011 and are carried out by 18 partners: ENEA (Italy, Coordinator), AREVA NP SAS (France), SCK-CEN (Belgium), FIP Industriale (Italy), MAURER SOHENE (Germany), EC-JRC (Ispra (Italy)), SINTEC (Italy), KTH (Sweden), BOA-BKT (Germany), IDOM (Spain), ANSALDO (Italy), IPUL (Latvia), NUMERIA (Italy), VCE (Austria), SRS (Italy), CEA (France), EA (Spain), NUVIA (France). (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2012

Facilities for macromolecular crystallography at the Helmholtz-Zentrum Berlin

Three macromolecular crystallography (MX) beamlines at the Helmholtz-Zentrum Berlin (HZB) are available for the regional, national and international structural biology user community. The state-of-the-art synchrotron beamlines for MX BL14.1, BL14.2 and BL14.3 are located within the low-[beta] section of the BESSY II electron storage ring. All beamlines are fed from a superconducting 7 T wavelength-shifter insertion device. BL14.1 and BL14.2 are energy tunable in the range 5-16 keV, while BL14.3 is a fixed-energy side station operated at 13.8 keV. All beamlines are equipped with CCD detectors. BL14.1 and BL14.2 are in regular user operation providing about 200 beam days per year and about 600 user shifts to approximately 50 research groups across Europe. BL14.3 has initially been used as a test facility and was brought into regular user mode operation during the year 2010. BL14.1 has recently been upgraded with a microdiffractometer including a mini-[kappa] goniometer and an automated sample changer. Other user facilities include office space adjacent to the beamlines, a sample preparation laboratory, a biology laboratory (safety level 1) and high-end computing resources. In this article the instrumentation of the beamlines is described, and a summary of the experimental possibilities of the beamlines and the provided ancillary equipment for the user community is given.

43 PARTICLE ACCELERATORS↗

DOE OSTI2013

4D tumor centroid tracking using orthogonal 2D dynamic MRI: Implications for radiotherapy planning

Purpose: Current pretreatment, 4D imaging techniques are suboptimal in that they sample breathing motion over a very limited “snapshot” in time. Heretofore, long-duration, 4D motion characterization for radiotherapy planning, margin optimization, and validation have been impractical for safety reasons, requiring invasive markers imaged under x-ray fluoroscopy. To characterize 3D tumor motion and associated variability over durations more consistent with treatments, the authors have developed a practical dynamic MRI (dMRI) technique employing two orthogonal planes acquired in a continuous, interleaved fashion.Methods: 2D balanced steady-state free precession MRI was acquired continuously over 9–14 min at approximately 4 Hz in three healthy volunteers using a commercial 1.5 T system; alternating orthogonal imaging planes (sagittal, coronal, sagittal, etc.) were employed. The 2D in-plane pixel resolution was 2 × 2 mm{sup 2} with a 5 mm slice profile. Simultaneous with image acquisition, the authors monitored a 1D surrogate respiratory signal using a device available with the MRI system. 2D template matching-based anatomic feature registration, or tracking, was performed independently in each orientation. 4D feature tracking at the raw frame rate was derived using spline interpolation.Results: Tracking vascular features in the lung for two volunteers and pancreatic features in one volunteer, the authors have successfully demonstrated this method. Registration error, defined here as the difference between the sagittal and coronal tracking result in the SI direction, ranged from 0.7 to 1.6 mm (1σ) which was less than the acquired image resolution. Although the healthy volunteers were instructed to relax and breathe normally, significantly variable respiration was observed. To demonstrate potential applications of this technique, the authors subsequently explored the intrafraction stability of hypothetical tumoral internal target volumes and 3D spatial probability distribution functions. The surrogate respiratory information allowed the authors to show how this technique can be used to study correlations between internal and external (surrogate) information over these prolonged durations. However, compared against the gold standard of the time stamps in the dMRI frames, the temporal synchronization of the surrogate 1D respiratory information was shown to be likely unreliable.Conclusions: The authors have established viability of a novel and practical pretreatment, 4D tumor centroid tracking method employing a commercially available dynamic MRI sequence. Further developments from the vendor are likely needed to provide a reliably synchronized surrogate 1D respiratory signal, which will likely broaden the utility of this method in the pretreatment radiotherapy planning context.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2018

Sensor Commercialization

The objective of this CRADA was the transfer the BaDx technology to a commercial partner, Aquila Technologies, to develop BaDx for medium-scale production. BaDx is a stand-alone, diagnostics cartridge for use in resourcelimited and challenging environments to sense low concentrations (<100 spores) of virulent pathogenic bacteria. The fully sealed cartridge also contains a “self-destruct” feature in which the device contents are sterilized post-assay. The ultimate goal of this CRADA was realized as validated and full-functioning BaDx cartridges are currently available for purchase and acquisition from Aquila. This project also resulted in significant and prestigious recognitions including, a R&D100 Award (2014), a Federal Laboratory Consortium (FLC) Excellence in Technology Transfer Award (2015), Popular Science Magazine naming BaDx ‘One of the Greatest Innovations of 2015,” and a TechConnect National Innovation Award (2015). Further, this CRADA resulted in a commercially viable bioagent detection platform transitioned from a national laboratory to industry that may significantly enhance national security by reducing the threat from biological agents that are stored and maintained in laboratories with poor safety and security protocols. Hospital, health clinic and at-home healthcare could also be revolutionized by this technology. This work has already lead to two follow-on projects, one funded by the US Department of Homeland Security (DHS), and the other by the US State Department.

47 OTHER INSTRUMENTATION↗

DOE OSTI2010

RELAP5 Model of the Vacuum Vessel Primary Heat Transfer System

This report describes the RELAP5 models that have been developed for the Vacuum Vessel (VV) Primary Heat Transfer System (PHTS). The models are intended to be used to examine the transient performance of the VV PHTS, and evaluate control schemes necessary to maintain parameters within acceptable limits during transients. Some preliminary results are presented to show the maturity of the models and to examine general VV PHTS transient behavior. The models can be used as a starting point to develop transient modeling capability in several directions including control system modeling, safety evaluations, etc, and are not intended to represent the final VV PHTS design. Preliminary calculations using the models indicate that during normal pulsed operation, heat exchanger control may not be necessary, and that temperatures within the vacuum vessel during decay heat operation remain low.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2015

Novel real-time 3D radiological mapping solution for ALARA maximization, D and D assessments and radiological management

Good management of dismantling and decontamination (D and D) operations and activities is requiring safety, time saving and perfect radiological knowledge of the contaminated environment as well as optimization for personnel dose and minimization of waste volume. In the same time, Fukushima accident has imposed a stretch to the nuclear measurement operational approach requiring in such emergency situation: fast deployment and intervention, quick analysis and fast scenario definition. AREVA, as return of experience from his activities carried out at Fukushima and D and D sites has developed a novel multi-sensor solution as part of his D and D research, approach and method, a system with real-time 3D photo-realistic spatial radiation distribution cartography of contaminated premises. The system may be hand-held or mounted on a mobile device (robot, drone, e.g). In this paper, we will present our current development based on a SLAM technology (Simultaneous Localization And Mapping) and integrated sensors and detectors allowing simultaneous topographic and radiological (dose rate and/or spectroscopy) data acquisitions. This enabling technology permits 3D gamma activity cartography in real-time. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2019

Solid-state electrolyte considerations for electric vehicle batteries

This paper is an overview of materials and cell fabrication considerations for all solid-state batteries meant for large format applications.

Shen, Hao↗

DOE OSTI2011

First Observation of Edge Localized Modes Mitigation with Resonant and Nonresonant Magnetic Perturbations in ASDEX Upgrade

First experiments with nonaxisymmetric magnetic perturbations, toroidal mode number n=2, produced by newly installed in-vessel saddle coils in the ASDEX Upgrade tokamak show significant reduction of plasma energy loss and peak divertor power load associated with type-I edge localized modes (ELMs) in high-confinement mode plasmas. ELM mitigation is observed above an edge density threshold and is obtained both with magnetic perturbations that are resonant and not resonant with the edge safety factor profile. Compared with unperturbed type-I ELMy reference plasmas, plasmas with mitigated ELMs show similar confinement, similar plasma density, and lower tungsten impurity concentration.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2012

Vortex Diode Analysis and Testing for Fluoride Salt-Cooled High-Temperature Reactors

Fluidic diodes are presently being considered for use in several fluoride salt-cooled high-temperature reactor designs. A fluidic diode is a passive device that acts as a leaky check valve. These devices are installed in emergency heat removal systems that are designed to passively remove reactor decay heat using natural circulation. The direct reactor auxiliary cooling system (DRACS) uses DRACS salt-to-salt heat exchangers (DHXs) that operate in a path parallel to the core flow. Because of this geometry, under normal operating conditions some flow bypasses the core and flows through the DHX. A flow diode, operating in reverse direction, is-used to minimize this flow when the primary coolant pumps are in operation, while allowing forward flow through the DHX under natural circulation conditions. The DRACSs reject the core decay heat to the environment under loss-of-flow accident conditions and as such are a reactor safety feature. Fluidic diodes have not previously been used in an operating reactor system, and therefore their characteristics must be quantified to ensure successful operation. This report parametrically examines multiple design parameters of a vortex-type fluidic diode to determine the size of diode needed to reject a particular amount of decay heat. Additional calculations were performed to size a scaled diode that could be tested in the Oak Ridge National Laboratory Liquid Salt Flow Loop. These parametric studies have shown that a 152.4 mm diode could be used as a test article in that facility. A design for this diode is developed, and changes to the loop that will be necessary to test the diode are discussed. Initial testing of a scaled flow diode has been carried out in a water loop. The 150 mm diode design discussed above was modified to improve performance, and the final design tested was a 171.45 mm diameter vortex diode. The results of this testing indicate that diodicities of about 20 can be obtained for diodes of this size. Experimental results show similar trends as the computational fluid dynamics (CFD) results presented in this report; however, some differences exist that will need to be assessed in future studies. The results of this testing will be used to improve the diode design to be tested in the liquid salt loop system.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2017

Advanced and Exploratory Shock Sensing Mechanisms.

Mechanical component response to shock environments must be predictable in order to ensure reliability and safety. Whether the shock input results from accidental drops during transportation to projectile impact scenarios, the system must irreversibly transition into a safe state that is incapable of triggering the component . With this critical need in mind, the 2017 Nuclear Weapons Summer Product Realization Institute (NW SPRINT) program objective sought the design of a passive shock failsafe with emphasis on additively manufactured (AM) components. Team Advanced and Exploratory (A&E) responded to the challenge by designing and delivering multiple passive shock sensing mech anisms that activate within a prescribed mechanical shock threshold. These AM failsafe designs were tuned and validated using analytical and computational techniques including the shock response spectrum (SRS) and finite element analysis (FEA). After rapid prototyping, the devices experienced physical shock tests conducted on Sandia drop tables to experimentally verify performance. Keywords: Additive manufacturing, dynamic system, failsafe, finite element analysis, mechanical shock, NW SPRINT, shock respon se spectrum

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

DOE OSTI2013

DOE Hanford Network Upgrades and Disaster Recovery Exercise Support the Cleanup Mission Now and into the Future

In 2013, the U.S. Department of Energy's (DOE) Hanford Site, located in Washington State, funded an update to the critical network infrastructure supporting the Hanford Federal Cloud (HFC). The project, called ET-50, was the final step in a plan that was initiated five years ago called "Hanford's IT Vision, 2015 and Beyond." The ET-50 project upgraded Hanford's core data center switches and routers along with a majority of the distribution layer switches. The upgrades allowed HFC the network intelligence to provide Hanford with a more reliable and resilient network architecture. The culmination of the five year plan improved network intelligence and high performance computing as well as helped to provide 10 Gbps capable links between core backbone devices (10 times the previous bandwidth). These improvements allow Hanford the ability to further support bandwidth intense applications, such as video teleconferencing. The ET-50 switch upgrade, along with other upgrades implemented from the five year plan, have prepared Hanford's network for the next evolution of technology in voice, video, and data. Hand-in-hand with ET-50's major data center outage, Mission Support Alliance's (MSA) Information Management (IM) organization executed a disaster recovery (DR) exercise to perform a true integration test and capability study. The DR scope was planned within the constraints of ET-50's 14 hour datacenter outage window. This DR exercise tested Hanford's Continuity of Operations (COOP) capability and failover plans for safety and business critical Hanford Federal Cloud applications. The planned suite of services to be tested was identified prior to the outage and plans were prepared to test the services ability to failover from the primary Hanford data center to the backup data center. The services tested were: Core Network (backbone, firewall, load balancers); Voicemail; Voice over IP (VoIP); Emergency Notification; Virtual desktops; and, Select set of production applications and data. The primary objective of the exercise was to test COOP around the emergency operations at Hanford to provide information on capabilities and dependencies of the current system to insure improved focus of emergency, safety and security capacity in a disaster situation. The integration of the DR test into the ET-50 project allowed the testing of COOP at Hanford and allowed the lessons learned to be defined. These lessons learned have helped improve the understanding of Hanford's COOP capabilities and will be critical for future planning. With the completion of the Hanford Federal Cloud network upgrades and the disaster recovery exercise, the MSA has a clearer path forward for future technology implementations as well as network improvements to help shape the usability and reliability of the Hanford network in support of the cleanup mission.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2017

Equipment for subcriticality monitoring by pulse method - 240

At the present time methods and means of determining, evaluating, and monitoring the effective neutron multiplication factor or the subcriticality are becoming very important for validating and monitoring nuclear safety in connection with the accumulation of a large number of spent fuel assemblies and the transition to a more tight mode of their storage arrangement in the spent-fuel pools of NPP. Pulse method is an effective subcriticality monitoring tool for subcritical reactors and spent nuclear fuel storages. This method is based on the use neutron generator, fission chambers and instrumentation for data acquisition and processing. The measurement and control equipment was designed. It allows: neutron pulses generation with specified parameters; neutron flux response monitoring by measuring the count rate at predetermined set of sequential time intervals; data transmitting to the personal computer; data processing and subcriticality calculation; self diagnostics and health monitoring; data recording, archiving and storage. The special device is proposed to check the electronic equipment. This device simulates a signal of a neutron detector counting rate after neutron generator pulses appear. The paper presents hardware structure and composition, specification and software of the control unit, which provides neutron generator operation, data acquisition and processing. (authors)

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2024

Refining Absorber Shroud Geometry to Maximize Power Output and Reduce Power Peaking in ATF Test Train

In the wake of the Fukushima Daiichi nuclear power plant accident in 2011, the accident tolerant fuels (ATF) program was initiated to enhance the safety of light-water reactor fuels, placing significant emphasis on cladding. A crucial step for the broad implementation of ATF in commercial reactors involves irradiation testing of the fuel designs. ATF-2D, the latest experiment in the ATF series, is slated to undergo irradiation in the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL). ATF-2D is a joint effort of the INL with industry partners General Electric Global Research; Framatome; General Atomics; the Japan Atomic Energy Agency; Hitachi-GE Nuclear Energy, Ltd; Global Nuclear Fuel-Japan Co., Ltd; Nippon Nuclear Fuel Development Co., Ltd; and Mitsubishi Heavy Industries, Ltd. The ATF-2D test train design consists of four tiers, each housing six rodlets. The device will be inserted in Loop 2A within the central flux trap of the ATR, and is anticipated to undergo irradiation throughout three 60-day cycles. Typical pressurized water reactor conditions will be emulated during the irradiation. The objective of the work presented here is to dimension neutron-absorbing hafnium (Hf) components surrounding the fuel rodlets, such that the axial power profile is flattened, while simultaneously ensuring that the total fission power output of the entire test train remains below 200 kW.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2024

Refining Absorber Shroud Geometry to Maximize Power Output and Reduce Power Peaking in ATF Test Train

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2025

Harnessing the Power of AI: Status and Expansion of Current Domestic Transport Security Through Flexible Embedded Hardware

As applications of Artificial Intelligence (AI) continue to expand, there are increasing opportunities to leverage applied AI methodologies with mobile transportation focused embedded systems. Current applications of AI in transportation focus on a variety of areas, including fuel efficiency, safety, security, and other broad fields of optimization or detection. To leverage these AI workflows and methodologies in the field, teams must utilize complex embedded systems capable of implementing these AI-enabled algorithms in real-time. In this paper, we will investigate how these algorithms can be integrated into existing technologies leveraging vehicle data - such as the Controller Area Network Transport Security Tracking and Reporting Unit (C-STAR). The C-STAR technology is an embedded platform with onboard computation capable of running next generation algorithms in vehicle systems AI, such as preventative maintenance, driver authentication, and transport security. As deployed in the field, the C-STAR has a limited AI functionality –this paper will directly discuss how a device like C-STAR can be utilized and the advantages of integrating these new technologies. We will open with relevant background information and transportation projects that leverage AI, focusing specifically on those around transport security such as vehicle identification, anomaly detection, and deterrence. We will then extend this into potential opportunities and scaling for AI methodologies using platforms like the C-STAR. Finally, we will speak directly to the challenges of deploying AI-powered workflows, such as computing power needs, bandwidth, hallucinations, and other regulatory considerations.

Cook, Adian [ORNL] (ORCID:0000000160825395)↗