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At least 703 records · Page 39

The Sealing Mechanisms of a Fracture in Opalinus Clay as Revealed by in situ Synchrotron X-Ray Micro-Tomography

The detailed mechanisms of the sealing of a single fracture, from hydration to almost complete closure by increase of confining pressure, as monitored from in situ synchrotron X-ray microtomography during the flow of carbonated water, is here shown for the first time. Different mechanisms play the key role at different stages in the evolution of the fracture. Hydration mechanically weakens the surfaces of the fracture and induces a first closure due to microcracking at the asperity contacts, increasing their size and creating choke points. Increase in confining stress promptly hydraulically seals the fracture by closing the main choke point, with a relative small deformation of the sample. Finally, the more pervasive mechanical deformation observed at higher stresses almost completely seals the whole fracture. The evolution of the sample has been described and quantified using 4D image processing, focusing on the evolution of aperture and digital volume correlation. Hydraulic properties of the sample at different stages have been modeled via Stokes flow simulation, and the results compared to the morphometric analysis, finding positive correlations with the average fracture aperture variation along the flowpath in function of confining pressure. Opalinus Clay is found to be a rock markedly prone to sealing in case of flow with carbonated water; this behavior is the result of the large fraction of clays and of its microstructure, lacking both cementing phases and large stiff particles. CO2 in this sample has no evident role in the evolution of the fracture; chemically induced weathering on the surface has not been detected, in contrast with the behavior observed in samples with carbonates as cementing phase.

58 GEOSCIENCES↗

Performance Evaluation of an Actuator Dust Seal for Lunar Operation

Exploration of extraterrestrial surfaces (e.g. moon, Mars, asteroid) will require durable space mechanisms that will survive potentially dusty surface conditions in addition to the hard vacuum and extreme temperatures of space. Baseline tests with lunar simulant were recently completed at NASA GRC on a new Low-Temperature Mechanism (LTM) dust seal for space actuator application. Following are top-level findings of the tests completed to date in vacuum using NU-LHT-2M lunar-highlands simulant. A complete set of findings are found in the conclusions section.Tests were run at approximately 10-7 torr with unidirectional rotational speed of 39 RPM.Initial break-in runs were performed at atmospheric conditions with no simulant. During the break-in runs, the maximum torque observed was 16.7 lbf-in. while the maximum seal outer diameter temperature was 103F. Only 0.4 milligrams of NU-LHT-2M simulant passed through the sealshaft interface in the first 511,000 cycles while under vacuum despite a chip on the secondary sealing surface.Approximately 650,000 of a planned 1,000,000 cycles were completed in vacuum with NU-LHT-2M simulant.Upon test disassembly NU-LHT-2M was found on the secondary sealing surface.

lunar↗

Advanced Seal Sessions I and II

As aircraft operators continue to seek higher fuel efficiency, lower emissions, and longer on-wing performance, turbine engine designers are scrutinizing all components for areas of improvement. To achieve overall goals, turbine pressure ratios and by-pass ratios continue to climb. Also, designers are seeking to minimize parasitic and cooling flows to extract the most useful work out of the flow stream, placing a renewed interest on seal technology and secondary flow path management. In the area of future manned spacecraft, advancements are being examined for both habitat seals and re-entry thermal protection system thermal barrierseals. For long duration space craft, designers are continuing to look for savings in parasitic losses to reduce the amount of cabin re-supply air that needs to be brought along. This is placing greater demands on seal designs and materials to exhibit low leakage and be resistant to space environments. For future missions to and from distant planets, the re-entry heating will be higher than for low-earth orbit or lunar return motivating advanced thermal barrier development. This presentation will provide an overview of the seal challenges and opportunities in these diverse areas.

turbine engines↗

Elastomeric Seal Performance after Terrestrial Ultraviolet Radiation Exposure

Ultraviolet radiation was evaluated to determine its negative effects on the performance of elastomeric gas pressure seals. The leak rates of the silicone elastomer S0383-70 O-ring test articles were used to quantify the degradation of the seals after exposure to vacuum-ultraviolet and/or middle-to-near-ultraviolet wavelength radiation. Three groups of seals were exposed in terrestrial facilities to 115-165 nm wavelength radiation, 230-500 nm wavelength radiation, or both spectrums, for an orbital spaceflight equivalent of 125 hours. The leak rates of the silicone elastomer S0383-70 seals were quantified and compared to samples that received no radiation. Each lot contained six samples and statistical t-tests were used to determine the separate and combined influences of exposure to the two wavelength ranges. A comparison of the mean leak rates of samples exposed to 115-165 nm wavelength radiation to the control specimens showed no difference, suggesting that spectrum was not damaging. The 230-500 nm wavelength appeared to be damaging, as the mean leak rates of the specimens exposed to that range of wavelengths, and those exposed to the combined 115-165 nm and 230-500 nm spectrums, were significantly different from the leak rates of the control specimens. Most importantly, the test articles exposed to both wavelength spectrums exhibited mean leak rates two orders of magnitude larger than any other exposed specimens, which suggested that both wavelength spectrums are important when simulating the orbital environment.

leakage↗

RADIOLOGICAL SEALED SOURCE LIBRARY: A NUCLEAR FORENSICS TOOL

If a terrorist were to obtain and possibly detonate a device that contained radiological material, radiological forensic analysis of the material and source capsule could provide law enforcement with valuable clues about the origin of the radiological material; this information could then provide further leads on where the material and sealed source was obtained, and the loss of control point. This information could potentially be utilized for attribution and prosecution. Analyses of nuclear forensic signatures for radiological materials are generally understood to include isotopic ratios, trace element concentrations, the time since irradiation or purification, and morphology. Radiological forensic signatures for sealed sources provide additional information that leverages information on the physical design and chemical composition of the source capsule and containers, physical markings indicative of an owner or manufacturer. Argonne National Laboratory (Argonne), in collaboration with Idaho National Laboratory (INL), has been working since 2003 to understand signatures that could be used to identify specific source manufacturers. These signatures include the materials from which the capsule is constructed, dimensions, weld details, elemental composition, and isotopic abundances of the radioactive material. These signatures have been compiled in a library known as the Argonne/INL Radiological Sealed Source Library. Data collected for the library has included open-source information from vendor catalogs and web pages; discussions with source manufacturers and touring of production facilities (both protected through non-disclosure agreements); technical publications; and government registries such as the U.S. Nuclear Regulatory Commission’s Sealed Source and Device Registry.

National Nuclear Forensics Library↗

Consumer Guide to Air Sealing the Home

Learn how air sealing can improve your home's energy efficiency, comfort, and durability. This fact sheet from Energy Saver includes information on proper ventilation, why to air seal, how to find and seal air leaks, working with contractors to seal your home, and materials to do-it-yourself.

air sealing, air leaks, caulking, weatherstripping↗

Management of Disused Radioactive Sealed Sources in Egypt - 13512

The future safe development of nuclear energy and progressive increasing use of sealed sources in medicine, research, industry and other fields in Egypt depends on the safe and secure management of disused radioactive sealed sources. In the past years have determined the necessity to formulate and apply the integrated management program for radioactive sealed sources to assure harmless and ecological rational management of disused sealed sources in Egypt. The waste management system in Egypt comprises operational and regulatory capabilities. Both of these activities are performed under legislations. The Hot Laboratories and Waste Management Center HLWMC, is considered as a centralized radioactive waste management facility in Egypt by law 7/2010. (authors)

07 ISOTOPE AND RADIATION SOURCES↗

A Collaborative Regulatory Effort for Sealed Source Disposal - 15735

The State of Utah, Department of Environmental Quality, Division of Radiation Control (DRC), EnergySolutions, the Conference of Radiation Control Program Directors (CRCPD), and the Department of Energy's Global Threat Reduction Initiative (GTRI) collaborated on a truly innovative effort to expand opportunities for cost-effective sealed source disposal. These entities developed a first-of-its-kind initiative to dispose of certain sealed sources at the EnergySolutions disposal facility near Clive, Utah, which normally cannot accept sealed sources of any type. This creative and collaborative effort to improve radiation health, safety, and security was recognized by the Richard S. Hodes, M.D. Honor Lecture Award. This award is presented annually by the Southeast Compact Commission at the Waste Management Symposia to encourage environmental professionals and political leaders to develop innovative approaches to waste management in the United States. The participants in the collaborative initiative are honored to receive special recognition for this effort. They also recognize that the hard work remains to be done in order to ensure the continued safe management and disposal of sealed sources. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Significant slowdown of plasma-optimized surface energy deactivation by vacuum sealing for efficient adhesive bonding

This work proposes an approach to minimize surface energy deactivation of plasma-treated metal and carbon fiber-reinforced polymer (CFRP) surfaces by vacuum sealing. Plasma treatments enhance adhesive wettability on post-treated surfaces for adhesive joints, but the treated surfaces deactivate quickly in air. The surface energy of aluminum alloy AA6061 and carbon fiber-reinforced polymer-polyamide (CFRP-PA66) optimally treated by a blown air plasma instrument returns to the original surface energy within one hour. Vacuum sealing of AA6061 and CFRP-PA66 reduced the surface energy deactivation over 7 days by at least 230 times and 970 times compared to in air. Double Cantilever Beam (DCB) tests performed on adhesively-bonded AA6061/CFRP-PA66 joints showed that the total energy release and energy dissipation before failure of plasma-treated and vacuum-sealed materials was up to 60% more than plasma-treated materials without vacuum sealing and up to 125% more than non-plasma-treated materials.

42 ENGINEERING↗

Examination of the ambient effects on the stability of amorphous indium-gallium-zinc oxide thin film transistors using a laser-glass-sealing technology

The effect of an ambient atmosphere with a positive bias constant current stress (CCS) and a negative bias illumination stress (NBIS) on the stability of amorphous In-Ga-Zn-O thin film transistors (TFTs) is examined by utilizing a glass-hermetic-sealant with a moisture permeability of less than 10{sup −6} g/m{sup 2} · day. In the CCS test, the threshold voltage shift (ΔV{sub th}) was remarkably suppressed in the glass-sealed TFTs. The unsealed and resin-sealed TFTs exhibited large ΔV{sub th} values. During the NBIS tests, the glass-sealed TFTs had almost the same negative ΔV{sub th} as the unsealed and resin sealed TFTs. Among the different TFTs, no significant differences were observed in the threshold voltage, the subthreshold swing and the saturation mobility as a function of the photon energy. It is concluded that ambient molecules were the primary origin of the instability of the ΔV{sub th}, induced by a CCS, but they were not related to the NBIS instability. The major role of the effective passivation layers in the NBIS test was not to simply block out the ambient effects, but to reduce the extra density of states at/near the surface of the back channel.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Evaluating the Effect of Vane Trailing Edge Flow on Turbine Rim Sealing

Abstract Modern gas turbine development continues to move toward increased overall efficiency, driven in part by higher firing temperatures that point to a need for more cooling air to prevent catastrophic component failure. However, using additional cooling flow bled from the upstream compressor causes a corresponding detriment to overall efficiency. A primary candidate for cooling flow optimization is purge flow, which contributes to sealing the stator–rotor cavity and prevents ingestion of hot main gas path (MGP) flow into the wheelspace. Previous research has identified that the external main gas path flow physics play a significant role in driving rim seal ingestion. However, the potential impact of other cooling flow features on ingestion behavior, such as vane trailing edge (VTE) flow, is absent in the open literature. This paper presents experimental measurements of rim cavity cooling effectiveness collected from a one-stage turbine operating at engine-representative Reynolds and Mach numbers. Carbon dioxide (CO2) was used as a tracer gas in both the purge flow and vane trailing edge flow to investigate flow migration into and out of the wheelspace. Results show that the vane trailing edge flow does in fact migrate into the rim seal and that there is a superposition relationship between individual cooling flow contributions. Computational fluid dynamics (CFD) simulations using unsteady Reynolds-averaged Navier–Stokes (URANS) were used to confirm VTE flow ingestion into the rim seal cavity. Radial and circumferential traverse surveys were performed to quantify cooling flow radial migration through the main gas path with and without vane trailing edge flow. The surveys confirmed that vane trailing edge flow is entrained into the wheelspace as purge flow is reduced. Local CO2 measurements also confirmed the presence of VTE flow deep in the wheelspace cavity.

Engineering↗

Training Students to Analyze Spatial and Temporal Heterogeneities in Reservoir and Seal Petrology, Mineralogy, and Geochemistry: Implications for CO{sub 2} Sequestration Prediction, Simulation, and Monitoring

The objective of this project was to expose and train multiple students in geological tools that are essential to reservoir characterization and geologic sequestration including but not limited to advanced petrological methods, mineralogical methods, and geochemical methods; core analysis, and geophysical well-log interpretation. These efforts have included training of multiple students through geologically based curriculum and research using advanced petrological, mineralogical, and geochemical methods. In whole, over the last 3+ years, this award has supported 5,828 hours of student research, supporting the work of several graduate and undergraduate students. They have all received training directly related to ongoing CO{sub 2} sequestration demonstrations. The students have all conducted original scientific research on topics related to understanding the importance of lithological, textural, and compositional variability in formations that are being targeted as CO{sub 2} sequestration reservoirs and seals. This research was linked to the Mount Simon Sandstone reservoir and overlying Eau Claire Formation seal in the Illinois Basin- a system where over one million tons of CO{sub 2} are actively being injected with the first large-scale demonstration of anthropogenic CO{sub 2} storage in the U.S. Student projects focused specifically on 1) reservoir porosity characterization and evaluation, 2) petrographic, mineralogical, and geochemical evidence of fluid-related diagenesis in the caprock, 3) textural changes in reservoir samples exposed to experimental CO{sub 2} + brine conditions, 4) controls on spatial heterogeneity in composition and texture in both the reservoir and seal, 5) the implications of small-scale fractures within the reservoir, and 6) petrographic and stable isotope analyses of carbonates in the seal to understand the burial history of the system. The student-led research associated with this project provided real-time and hands-on experience with a relevant CO{sub 2} system, provided relevant information to the regional partnerships who are working within these formations, and provides more broadly applicable understanding and method development for other carbon capture and storage systems.

54 ENVIRONMENTAL SCIENCES↗

Special Analysis for the Disposal of the Neutron Products Incorporated Sealed Source Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

The purpose of this special analysis (SA) is to determine if the Neutron Products Incorporated (NPI) Sealed Sources waste stream (DRTK000000056, Revision 0) is suitable for disposal by shallow land burial (SLB) at the Area 5 Radioactive Waste Management Site (RWMS). The NPI Sealed Sources waste stream consists of 850 60Co sealed sources (Duratek [DRTK] 2013). The NPI Sealed Sources waste stream requires a special analysis (SA) because the waste stream 60Co activity concentration exceeds the Nevada National Security Site (NNSS) Waste Acceptance Criteria (WAC) Action Levels.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Special Analysis for the Disposal of the Idaho National Laboratory Contact Handled Sealed Sources Waste Stream at the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This special analysis (SA) evaluates whether the Idaho National Laboratory (INL) Contact Handled Sealed Sources waste stream is suitable for disposal by shallow land burial at the Area 5 Radioactive Waste Management Site (RWMS) on the Nevada National Security Site (NNSS). The INL Contact Handled Sealed Sources waste stream consists of sealed radioactive sources. The INL Contact Handled Sealed Sources waste stream requires an SA to determine whether the Area 5 RWMS can accept radium-226 ( 226 Ra), tritium ( 3 H), and europium-152 ( 152 Eu) at activity concentrations exceeding the NNSS Waste Acceptance Criteria Action Levels and whether to accept four long-lived radionuclides (curium-247 [ 247 Cm], 250 Cm, californium-249 [ 249 Cf], 251 Cf) without action levels.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

H-Canyon Jumper Gasket Sealing Evaluation

H-Canyon Documented Safety Analysis approved December 2019 credits the leak integrity of H-Canyon (HCA) process tanks, piping, and jumpers in preventing the release of radioactive material in a post seismic environment. Demonstration of leak tightness capability for this equipment was achieved through substantial analytical effort. However, one potential weak point that affects leak integrity exists at the gasketed joint between Hanford Connectors (HC) and nozzles. Review of the HCA Crane Log over a three-year period indicates the HCs periodically leak. Savannah River National Laboratory (SRNL) was requested to perform gasket compression tests that evaluate gasket relaxation characteristics, i.e., creep, and provide improvements to the HC installation process that can reduce or eliminate the frequency of leaks at HCs. A HC torque value of 312 ft-lbf is the target value used because it is the minimum torque value, with 95% confidence, when an unlubricated HC is impacted for standard sealing period of 9 seconds. In the HCA pipe-jumper connections are installed remotely by using HCs. HCs inherently add to the uncertainty of a gasketed joint because a calibrated torque value cannot be applied. The gasket material is a special material made of asbestos-fiber impregnated with Teflon. This material has been used for decades and generally performs well but does leak intermittently as gaskets creep and preloaded torque is lost. Gasket types are either snap-ring (SR) or lampshade (LS). Both gasket types cover the same seating area. The SR gasket is designed to remain with the jumper when the jumper is removed leaving the nozzle faces clean of any debris. SR gaskets are initially installed when the jumper is fabricated. Changing gaskets is time consuming and the radioactive environment presents risks to personnel. When jumpers are removed LS gaskets could be used to better seal the connection to reduce down time and ALARA concerns. That is, an LS gasket would be remotely positioned over the nozzle and the HC reinstalled. Testing also included two situations not typical of plant operation. One situation was the use of the non-standard double-layered gaskets (DG), and the other situation was the use of a LS without removal of the installed SR gasket. The DG was used when the supply of LS gaskets ended, so that testing could continue. It was of interest to demonstrate this gasket’s creep response because the DG, which was two gaskets glued together, was thicker than the LS gasket and the thicker material was expected to elicit a greater creep characteristics. The second situation of using two gaskets together by installing an LS gasket without removing the installed gasket is not allowed by the ASME Codes. However, by demonstrating the creep history of such a gasket arrangement it could be considered as an option that could possibly seal a connection while significantly reducing operational down time and personnel risk. Forty tests were conducted, and the overall results demonstrate the initial applied force and how the gasket changes with time. The change in sealing force, in terms of torque, was then measured to obtain a force history as the gaskets creep. This report documents the results of those tests as well as the method used to perform the tests.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

The Cypress Sandstone Seal System

The Cypress Sandstone is the youngest and shallowest unit in the Illinois Basin that was featured in the United States Carbon Utilization and Storage Atlas IV as a target for saline carbon storage with an estimated 0.2 to 2.3 GT of storage potential. Additional research on a residual oil zone (ROZ) developed within the Cypress Sandstone has delineated 27 prospects with approximately 290.8 million m3 (1.8 billion barrels) of oil in place. 21 to 31 million m 3 (144 to 196 million barrels) of oil is estimated to be recoverable using carbon dioxide enhanced oil recovery (CO 2 -EOR). Storage of CO 2 associated with EOR in these ROZ prospects alone, not accounting for associated main pay zones (MPZs), underlying brine formation, or intervals adjacent to or between prospects, is estimated to be up to 10.4 billion tonnes. The Cypress Sandstone is thus well understood to be a CO 2 injection target, both for EOR and associated storage. However, the seal system overlying the Cypress Sandstone is poorly understood. Unlike deeper formations such as the Mt. Simon Sandstone or the St. Peter Sandstone which are either in use as a CO 2 sink or being characterized for prospective storage, respectively, the Cypress is not overlain by hundreds of feet of impermeable shale. Rather, the Cypress is overlain by a lithologically variable interval that is composed generally of shales and limestones with some sandstone in the part of the Basin where the Cypress is deep enough to facilitate CO 2 storage. Also, due to its status as one of the shallowest and most prolific oil reservoirs in the Basin, the seal system overlying the Cypress Sandstone has a relatively high number of legacy well penetrations. The purpose of this report is to characterize the Cypress Sandstone seal system using well logs and available core. Gross thickness, lithology (facies), and mineralogy of seals is described and mapped across the Basin. The column height of CO 2 that can be held is calculated using capillary pressure data from a representative core.

02 PETROLEUM↗

Investigation of positive shaft seals

Welded metal bellows secondary seals prevent secondary seal leakage with a minimum number of potential leak paths. High performance seal is obtained by controlling the potentially unstable seal-face movements induced by mechanical vibrations and fluid pressure pulsations.

Pfouts, J. O.↗