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NASA NTRS2011

Analysis of ALTAIR 1998 Meteor Radar Data

We describe a new analysis of a set of 32 UHF meteor radar traces recorded with the 422 MHz ALTAIR radar facility in November 1998. Emphasis is on the velocity measurements, and on inferences that can be drawn from them regarding the meteor masses and mass densities. We find that the velocity vs altitude data can be fitted as quadratic functions of the path integrals of the atmospheric densities vs distance, and deceleration rates derived from those fits all show the expected behavior of increasing with decreasing altitude. We also describe a computer model of the coupled processes of collisional heating, radiative cooling, evaporative cooling and ablation, and deceleration - for meteors composed of defined mixtures of mineral constituents. For each of the cases in the data set we ran the model starting with the measured initial velocity and trajectory inclination, and with various trial values of the quantity mPs 2 (the initial mass times the mass density squared), and then compared the computed deceleration vs altitude curves vs the measured ones. In this way we arrived at the best-fit values of the mPs 2 for each of the measured meteor traces. Then further, assuming various trial values of the density Ps, we compared the computed mass vs altitude curves with similar curves for the same set of meteors determined previously from the measured radar cross sections and an electrostatic scattering model. In this way we arrived at estimates of the best-fit mass densities Ps for each of the cases. Keywords meteor ALTAIR radar analysis 1 Introduction This paper describes a new analysis of a set of 422 MHz meteor scatter radar data recorded with the ALTAIR High-Power-Large-Aperture radar facility at Kwajalein Atoll on 18 November 1998. The exceptional accuracy/precision of the ALTAIR tracking data allow us to determine quite accurate meteor trajectories, velocities and deceleration rates. The measurements and velocity/deceleration data analysis are described in Sections II and III. The main point of this paper is to use these deceleration rate data, together with results from a computer model, to determine values of the quantities mPs 2 (the meteor mass times its material density squared); and further, by combining these m s 2 values with meteor mass estimates for the same set of meteors determined separately from measured radar scattering

Zinn, J.↗

NASA NTRS2018

Working Fluid Trade Study for a Two-Phase Mechanically Pumped Loop Thermal Control System

NASA Jet Propulsion Laboratory is investigating a two-phase mechanically pumped fluid loop (MPFL) technology for spacecraft thermal control for future planetary space science mission concepts. The two-phase technology combines the potential of single-phase MPFL and the passive two-phase heat pipe systems. Previous two-phase MPFL studies at JPL have identified an evaporator system with a separated flow architecture as providing a robust light mass thermal control system with very high spatial and temporal thermal stability required by the science instruments on these missions. These studies have further identified the thermophysical properties of the working fluid to be key to the performance of a two-phase fluid loop. This paper describes the methodology used in the selection of the working fluids for optimizing the performance of the two-phase MPFL. A high level model was developed that includes the constraints and boundaries driven by the system components. The performance of fluids from the REFPROP database are investigated and rated for this system. The working fluid attributes such as cost, hazardous properties, and heritage were taken into account in this selection. A typical spacecraft dissipating 1000 W and a fluid loop consisting of an evaporator, accumulator, radiator, and associated tubing components is used as an example in this study.

Daimaru, Takuro↗

NASA NTRS2018

Working Fluid Trade Study for a Two-Phase Mechanically Pumped Loop Thermal Control System

NASA Jet Propulsion Laboratory is investigating a two-phase mechanically pumped fluid loop (MPFL) technology for spacecraft thermal control for future planetary space science mission concepts. The two-phase technology combines the potential of single-phase MPFL and the passive two-phase heat pipe systems. Previous two-phase MPFL studies4,5 at JPL have identified an evaporator system with a separated flow architecture as providing a robust light mass thermal control system with very high spatial and temporal thermal stability required by the science instruments on these missions. These studies have further identified the thermophysical properties of the working fluid to be key to the performance of a two-phase fluid loop. This paper describes the methodology used in the selection of the working fluids for optimizing the performance of the two-phase MPFL. A high level model was developed that includes the constraints and boundaries driven by the system components. The performance of fluids from the REFPROP database were investigated and rated for this system. The working fluid attributes such as cost, hazardous properties, and heritage were taken into account in this selection. A typical spacecraft dissipating 1000 W and a fluid loop consisting of an evaporator, accumulator, radiator, and associated tubing components was used as an example in this study.

Daimaru, Takuro↗

DOE OSTI2021

In Situ Recrystallization of Co-Evaporated Cu(In,Ga)Se2 Thin Films by Copper Chloride Vapor Treatment towards Solar Cell Applications

Cu(In,Ga)Se2 (or CIGS) thin films and devices were fabricated using a modified three-stage process. Using high deposition rates and a low temperature during the process, a copper chloride vapor treatment was introduced in between the second and third stages to enhance the films properties. X-ray diffraction and scanning electron microscopy demonstrate that drastic changes occur after this recrystallization process, yielding films with much larger grains. Secondary ion mass spectrometry shows that the depth profile of many elements is not modified (such as Cu, In and Se) while others change dramatically (such as Ga and Na). Because of the competing effects of these changes, not all parameters of the solar cells are enhanced, yielding an increase of 15% in the device efficiency at the most.

14 SOLAR ENERGY↗

DOE OSTI2023

Computational study of the ECN spray C via one-way coupling of internal nozzle flow and ensuing spray

Here, in this study, computational fluid dynamics simulations of the Engine Combustion Network Spray C injector were performed to investigate the effect of the internal nozzle flow on the development of the ensuing spray in automotive fuel injectors. A set of simulation best practices was first developed to achieve an accurate representation of the internal nozzle flow. Detailed, spatiotemporally defined information was extracted at the injector’s orifice exit and stored in maps that were subsequently employed to initialize a Lagrangian spray by means of a static, one-way coupling (OWC) approach. To highlight the impact of the in-nozzle flow on the spray, the OWC approach was compared with the conventional rate-of-injection (ROI) approach, for which the spray parcels are commonly initialized using a blob injection model. The results indicated that, using the ROI approach, considerable evaporation was observed within the plume in the near-nozzle region. On the other hand, the OWC approach showed evidence of evaporation farther downstream and at the plume periphery. The different behavior observed with the two approaches was mostly due to substantial differences in fuel mass distribution. The liquid fuel concentration predicted by the OWC approach matched well with X-ray tomography measurements of projected fuel mass per unit volume, in terms of both magnitude and distribution. In contrast, an unphysical distribution of fuel mass characterized by an extremely low liquid concentration was predicted by the ROI approach. In the far-field, the effect of the in-nozzle flow was found to be weaker as the spray penetrated and interacted with the ambient gas. In this region, the OWC and ROI approaches provided similar predictions of vapor penetration, spray morphology, and mixing-related characteristics.

33 ADVANCED PROPULSION SYSTEMS↗

NASA NTRS1985

A novel X-ray photoelectron spectroscopy study of the Al/SiO2 interface

The nondestructive measurement of the chemical and physical characteristics of the interface between bulk SiO2 and thick aluminum films is reported. Both X-ray phototelectron spectroscopy (XPS) and electrical measurements of unannealed, resistively evaporated Al films on thermal SiO2 indicate an atomically abrupt interface. Post metallization annealing at 450 C induces reduction of the SiO2 by the aluminum, at a rate consistent with the bulk reaction rate. The XPS measurement is performed from the SiO2 side after the removal of the Si substrate with XeF2 gas and thinning of the SiO2 layer with HF:ETOH. This represents a powerful new approach to the study of metal-insulator and related interfaces.

Hecht, M. H.↗

NASA NTRS2016

Terrestrial Testing of the CapiBRIC, a Microgravity Optimized Brine Processor

Utilizing geometry based static phase separation exhibited in the radial vaned capillary drying tray, a system was conceived to recover water from brine. This technology has been named the Capillary BRIC; abbreviated CapiBRIC. The CapiBRIC utilizes a capillary drying tray within a drying chamber. Water is recovered from clean water vapor evaporating from the free surface leaving waste brine solids behind. A novel approach of optimizing the containment geometry to support passive capillary flow and static phase separation provides the opportunity for a low power system that is not as susceptible to fouling as membranes or other technologies employing physical barriers across the free brine surface to achieve phase separation in microgravity. Having been optimized for operation in microgravity, full-scale testing of the CapiBRIC as designed cannot be performed on the ground as the force of gravity would dominate over the capillary forces. However, subscale units relevant to full-scale design were used to characterize fill rates, containment stability, and interaction with a variable volume reservoir in the PSU Dryden Drop Tower (DDT) facility. PSU also using tested units scaled such that capillary forces dominated in a 1-g environment to characterize evaporation from a free-surface in 1-g upward, sideways and downward orientations. In order to augment the subscale testing performed by PSU, a full scale 1-g analogue of the CapiBRIC drying unit was initiated to help validate performance predictions regarding expected water recovery ratio, estimated processing time, and interface definitions for inlets, outlets, and internal processes, including vent gas composition. This paper describes the design, development and test of the terrestrial CapiBRIC prototypes.

Sargusingh, Miriam J.↗

NASA NTRS1979

Preprototype vapor compression distillation subsystem

A three-person capacity preprototype vapor compression distillation subsystem for recovering potable water from wastewater aboard spacecraft was designed, assembled, and tested. The major components of the subsystem are: (1) a distillation unit which includes a compressor, centrifuge, central shaft, and outer shell; (2) a purge pump; (3) a liquids pump; (4) a post-treat cartridge; (5) a recycle/filter tank; (6) an evaporator high liquid level sensor; and (7) the product water conductivity monitor. A computer based control monitor instrumentation carries out operating mode change sequences, monitors and displays subsystem parameters, maintains intramode controls, and stores and displays fault detection information. The mechanical hardware occupies 0.467 m3, requires 171 W of electrical power, and has a dry weight of 143 kg. The subsystem recovers potable water at a rate of 1.59 kg/hr, which is equivalent to a duty cycle of approximately 30% for a crew of three. The product water has no foul taste or odor. Continued development of the subsystem is recommended for reclaiming water for human consumption as well as for flash evaporator heat rejection, urinal flushing, washing, and other on-board water requirements.

Ellis, G. S.↗

DOE OSTI2026

Substrate-Mediated Evaporation and Stochastic Evolution of Supported Au Nanoparticles

Here, we use in situ transmission electron microscopy with automated tracking to study supported gold nanoparticles (NPs) during high-temperature vacuum annealing. The average mass loss per NP is governed by a flat, nearly size-independent substrate-mediated evaporation profile. On top of this mean shrinkage, individual NPs show significant fluctuations in apparent growth or shrinkage, and NP volume follows a random-walk-like trajectory. To rationalize both the ensemble-mean behavior and the particle-resolved variability, we develop a self-consistent theory that couples substrate-mediated evaporation to collective 2D Ostwald-type mass exchange through a shared adatom field, described in terms of a renormalized screening length and background concentration. In the experimentally relevant regime, the theory predicts an approximately size-independent mean shrinkage rate and clarifies how net mass loss suppresses classical coarsening. Superimposed on this deterministic drift, we quantify stochastic volume trajectories and capture their fluctuation spectrum with a minimal Langevin description consistent with intermittent adatom attachment and detachment events. In addition, we characterize the lateral diffusive motion of NPs, which is responsible for their coalescence. Altogether, our results highlight that stochasticity is intrinsic at the nanoscale and that predicting the evolution of supported NPs at early and intermediate times requires a unified framework combining substrate-mediated evaporation, collective mass exchange, and stochastic fluctuations.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

NASA NTRS1993

Hydrodynamics of winds from irradiated companion stars in low-mass X-ray binaries

We study the hydrodynamics of evaporative winds driven by X-rays and/or soft gamma-rays irradiating the outer layers of companion stars in low-mass X-ray binaries (LMXBs). We consider several irradiating fluxes and spectra for LMXBs with white dwarf and main-sequence companion stars. The thermal structure of the base of the coronal region, the position of the sonic point, and the value of the mass-loss rate are calculated in the case of spherical geometry. We consider photospheric and coronal heating from both X-ray photoionization and Compton scattering of X-rays and soft gamma-rays with energy about 1 MeV possibly irradiating the companion star in LMXBs. Evaporative winds may play a relevant role for the evolution of a special class of radiation-driven LMXBs, and this study is a step toward a quantitative understanding of the mechanism driving LMXB evolution.

Tavani, Marco↗

DOE OSTI2025

Clustering and runaway merging in a primordial black hole dominated universe

If primordial black holes (PBHs) are present in the early Universe, their contribution to the energy budget grows relative to that of radiation and generically becomes dominant unless the initial abundance is exponentially small. This black hole domination scenario is largely unconstrained for PBHs with masses ≲ 10 9 g, which evaporate prior to big bang nucleosynthesis. However, if the era of PBH domination is sufficiently long, the PBHs form clusters and can merge appreciably within these objects. We calculate the population statistics of these clusters within the Press-Schechter formalism and find that, for a wide range of PBH masses and Hubble rates at the onset of PBH domination, the mergers within PBH clusters can exhibit runaway behavior, where the majority of the cluster will eventually form a single black hole with a mass much greater than the original PBH mass. Finally, these mergers can dramatically alter the PBH mass distribution and leave behind merged relic black holes that evaporate after big bang nucleosynthesis and yield various observational signatures, excluding parameter choices previously thought to be viable.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

NASA NTRS2015

Loop Heat Pipe Temperature Oscillation Induced by Gravity Assist and Reservoir Heating

The Laser Thermal Control System (LCTS) for the Advanced Topographic Laser Altimeter System (ATLAS) to be installed on NASA's Ice, Cloud, and Land Elevation Satellite (ICESat-2) consists of a constant conductance heat pipe and a loop heat pipe (LHP) with an associated radiator. During the recent thermal vacuum testing of the LTCS where the LHP condenser/radiator was placed in a vertical position above the evaporator and reservoir, it was found that the LHP reservoir control heater power requirement was much higher than the analytical model had predicted. Even with the control heater turned on continuously at its full power, the reservoir could not be maintained at its desired set point temperature. An investigation of the LHP behaviors found that the root cause of the problem was fluid flow and reservoir temperature oscillations, which led to persistent alternate forward and reversed flow along the liquid line and an imbalance between the vapor mass flow rate in the vapor line and liquid mass flow rate in the liquid line. The flow and temperature oscillations were caused by an interaction between gravity and reservoir heating, and were exacerbated by the large thermal mass of the instrument simulator which modulated the net heat load to the evaporator, and the vertical radiator/condenser which induced a variable gravitational pressure head. Furthermore, causes and effects of the contributing factors to flow and temperature oscillations intermingled.

Thermal Control Systems↗

NASA NTRS2015

Loop Heat Pipe Temperature Oscillation Induced by Gravity Assist and Reservoir Heating

0000↗

NASA NTRS2012

Century Scale Evaporation Trend: An Observational Study

Several climate models with different complexity indicate that under increased CO2 forcing, runoff would increase faster than precipitation overland. However, observations over large U.S watersheds indicate otherwise. This inconsistency between models and observations suggests that there may be important feedbacks between climate and land surface unaccounted for in the present generation of models. We have analyzed century-scale observed annual runoff and precipitation time-series over several United States Geological Survey hydrological units covering large forested regions of the Eastern United States not affected by irrigation. Both time-series exhibit a positive long-term trend; however, in contrast to model results, these historic data records show that the rate of precipitation increases at roughly double the rate of runoff increase. We considered several hydrological processes to close the water budget and found that none of these processes acting alone could account for the total water excess generated by the observed difference between precipitation and runoff. We conclude that evaporation has increased over the period of observations and show that the increasing trend in precipitation minus runoff is correlated to observed increase in vegetation density based on the longest available global satellite record. The increase in vegetation density has important implications for climate; it slows but does not alleviate the projected warming associated with greenhouse gases emission.

Bounoui, Lahouari↗

DOE OSTI2022

Rapid scalable fabrication of roll-to-roll slot-die coated flexible perovskite solar cells using intense pulse light annealing

Perovskite solar cells have achieved high efficiencies at the lab scale using batch processes that often may not be scalable. Processes that can be integrated into a continuous manufacturing platform, such as roll-to-roll, where several processes can be carried out sequentially are necessary to develop a new cost-competitive solar technology. In this work, intense pulsed light thermal post-processing is coupled with scalable slot-die coating and air knife evaporation in a high-speed roll-to-roll process of up to 2 m min –1 . The optimization of IPL energy parameters, web speeds, solution flow rates, and concentration of precursor inks yielded a champion power conversion efficiency of 11.24% for a 1 cm 2 roll-to-roll coated device. The overall processing time for a single layer in this process is reduced from minutes to seconds and the overall footprint of the manufacturing process is decreased. Furthermore, this demonstrates the promising capabilities for intensed pulsed light to reduce manufacturing costs and paves a roadmap for scalable and efficient PSCs on a roll-to-roll platform.

14 SOLAR ENERGY↗

DOE OSTI2025

Thermal evaporation of thin Li films

Thermal evaporation of lithium is considered a promising technique for the fabrication of clean lithium thin films for solid-state batteries. Here, in this study, we present a practical investigation of nanometer scale lithium films prepared by evaporation on different substrates. These substrates include Li-alloying and nonalloying metals as well as different classes of solid-state lithium-ion conductors. The deposition rate was also varied. For films less than 100 nm thick, the data show that the deposition rate has the biggest impact on the surface coverage. At 50 Å/s, Li forms small particles <1 μm in diameter while higher deposition rate of 150 Å/s resulted in more uniform film morphology on all the substrates. At the lower deposition rates, the wetting of Li to the substrate will impact the particle morphology. We also used the particles to estimate a contact angle between Li and the substrate to qualitatively compare the adhesion from substrate to substrate. The smallest contact angle was observed from lithium films on Li 7 La 3 Zr 2 O 12 and LiPON (nominal Li 2.94 PO 3.5 N 0.31 ) solid-state electrolytes.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1993

Stable Ni isotopes and Be-10 and Al-26 in metallic spheroids from Meteor Crater, Arizona

The Canyon Diablo spheroids, which are found around Meteor Crater, Arizona, are nickel-enriched objects with diameters from less than 0.1 to several mm. Previous studies have suggested that the enrichment of nickel resulted either from shock-melting of S-rich areas followed by solidification of the liquids under strongly non-equilibrium conditions at rapid cooling rates during flight outward from the crater or from the selective oxidation of iron. Isotopic studies are an effective tool for constraining the degree of open-system evaporation experienced by a system. The purpose of this study was to see whether Ni isotopes had been fractionated by volatilization during spheroid formation. In addition, the cosmogenic nuclides Be-10 and Al-26 were measured to try to estimate the depths in the parent meteorite from which the spheroids came.

Xue, S.↗

NASA NTRS1996

The Ultrafine Mineralogy of a Molten Interplanetary Dust Particle as an Example of the Quench Regime of Atmospheric Entry Heating

Melting and degassing of interplanetary dust particle L2005B22 at approx. 1200 C was due to flash heating during atmospheric entry. Preservation of the porous particle texture supports rapid quenching from the peak heating temperature whereby olivine and pyroxene nanocrystals (3 nm-26 nm) show partial devitrification of the quenched melt at T approx. = 450 C - 740 C. The implied ultrahigh cooling rates are calculated at approx. 105 C/h-106 C/h, which is consistent with quench rates inferred from the temperature-time profiles based on atmospheric entry heating models. A vesicular rim on a nonstoichiometric relic forsterite grain in this particle represents either evaporative magnesium loss during flash heating or thermally annealed ion implantation texture.

Rietmeijer, Frans J. M.↗