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At least 415 records · Page 23

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NASA NTRS1985

High-thermal-gradient Superalloy Crystal Growth

Single, (001)-oriented crystals of PWA 1480 were processed in alumina/silica shell molds in a laboratory high gradient furnace. The furnace employs a graphite resistance heated element, a radiation baffle, and a water cooled radiation trap below the baffle. All crystals were grown in vacuum (10 torr) and all heat transfer was radiative. The element is constructed with a variable cross section that is tapered just above the baffle to maximize heat input and therefore thermal gradient. A maximum alloy temperature of 1600 C was used. A thermal gradient of 130 deg C/cm was recorded at 1370 C just above the solidus of the PWA 1480 alloys. Crystal bars with 14.4 and 17.5 mm diameters were grown in alumina/silica shell molds. Each crystal was started from a 1.6 mm pencil seed at a rate of 76 mm/hr and slowly accelerated to a rate of 200 mm/hr under computer control. Volume percent porosity and average pore size were measured as functions of distance in representative bars. Low cycle fatigue behavior and stress rupture properties were determined.

Pearson, D. D.↗

NASA NTRS1985

Concept development evaluation for John Deere/UA STS middeck experiment location

The purpose of this effort was to consider and evaluate some specific concepts for performing a number of extremely low gravity (i.e., microgravity) experiments involving the directional solidification of samples of high carbon, cast iron alloys. The specific experiments considered herein were conceived to permit scientific investigation of the resultant microstructures and mechanical properties of the test samples after the microgravity environment processing. This study was limited to consideration of the NASA/MSFC furnace payloads, referred to herein as the Automated Directional Solidification Furnace (ADSF) systems. Three ADSF systems were reviewed and are as follows: (1) Low temperature ADSF (ADSF-1); (2) High temperature ADSF (ADSF-2); and (3) Advanced ADSF (AADSF).

Youngblood, W. W.↗

NASA NTRS1986

Comparative Thermal-Conductivity Test Technique

Approximate thermal conductivities determined rapidly. Two specimens, to be compared, placed in assembly with insulation. One end of assembly placed in furnace. Temperature of furnace, of each end, and of center of each specimen recorded. Procedure used to rate quickly candidate materials for applications in which thermal conductivity prime consideration.

Webster, C. N.↗

NASA NTRS1985

Heat Flow and Segregation in Directional Solidification

This research is composed of three major components: (1) development of interface morphology control for automated Bridgman growth of semiconductor systems; (2) comparative analysis of segregation during crystal growth in a reduced gravity environment and in the presence of magnetic fields; and (3) consequences of seeding by meltback in Bridgman growth under reduced gravity conditions. In attempts to optimize furnace design for crystal growth in a reduced gravity environment, an analytical approach to heat transfer was developed. It was thus found that charge confining crucibles diminish the ability to control the growth interface morphology through its position within the gradient zone. A heat pipe hot zone system for Bridgman growth, in reduced gravity environment, of crystal with diameters up to 16 mm was developed. For growth of Ga-doped germanium in the multipurpose (ASTP) furnace, it was found that the application of transverse magnetic fields (up to 36 kg) does not substantially increase the effective distribution coefficient; i.e., diffusion-controlled segregation observed in reduced gravity environment cannot be reached nor approached by magnetic field induced melt stabilization.

Witt, A. F.↗

NASA NTRS1986

Role of molybdenum in the Na sub 2SO sub 4 induced corrosion of superalloys at high temperatures

Sodium sulfate induced corrosion of a molybdenum containing nickel-base superalloy, Udimet 700, was studied in laboratory furnace tests and in a high velocity (Mach 0.3) burner rig. The effect of SO2 content in the atmosphere on the corrosion behavior in the laboratory furnace tests was determined. Catastrophic corrosion occurs only when the melt contains MoO3 in addition to Na2SO4 and Na2MoO4. The conditions under which catastrophic corrosion occurs are identified and a mechanism is described to explain the catastrophic corrosion.

Misra, A. K.↗

NASA NTRS1986

Containerless high purity pulling process and apparatus for glass fiber

Apparatus and method for pulling optical glass fibers in a containerless environment is disclosed which includes a single axis acoustical levitation furnace in which a specimen is levitated and melted. A reflector unit is carried in the interior of the furnace and includes a reflector disposed centrally about the acoustical axis of the levitator. The reflector unit includes a circular shroud of insulation and a copper sleeve inserted in the unit which is hollow at for receiving a cooling medium. A fiber pulling bore is formed centrally in the reflector unit surrounded by cooling jacket to enhance solidification and formation of a fiber. A starting fiber strand is introduced into the melt and pulled outwardly through bore whereby the specimen fiber is started and formed as pulled therethrough. In order to replenish the melt and thus enable a continous process, a movable secondary reflector is provided which captures a supplemental specimen pellet and by movement of the reflector transfers it to the melt.

Naumann, R. J.↗

NASA NTRS1986

Solar silicon from directional solidification of MG silicon produced via the silicon carbide route

A process of metallurgical grade (MG) silicon production is presented which appears particularly suitable for photovoltaic (PV) applications. The MG silicon is prepared in a 240 KVA, three electrode submerged arc furnace, starting from high grade quartz and high purity silicon carbide. The silicon smelted from the arc furnace was shown to be sufficiently pure to be directionally solidified to 10 to 15 kg. After grinding and acid leaching, had a material yield larger than 90%. With a MG silicon feedstock containing 3 ppmw B, 290 ppmw Fe, 190 ppmw Ti, and 170 ppmw Al, blended with 50% of off grade electronic grade (EG) silicon to reconduct the boron content to a concentration acceptable for solar cell fabrication, the 99% of deep level impurities were concentrated in the last 5% of the ingot. Quite remarkably this material has OCV values higher tham 540 mV and no appreciable shorts due to SiC particles.

Rustioni, M.↗

NASA NTRS1986

Electrical conductivity of carbonaceous chondrites and electric heating of meteorite parent bodies

The electrical conductivity of samples of the Murchison and Allende carbonaceous chondrites is 4 to 6 magnitudes greater than rock forming minerals such as Olivine up to 700 C. The remarkably high electrical conductivity of these meteorites is attributed to carbon at grain boundaries. The environment in the wake of the space station can be exploited to produce conditions which will allow pyrolysis of carbonaceous chondrites. An experimental package consisting of a one square meter shield attached to a 15 cm diameter by 40 cm long furnace and tied to a conductance bridge, furnace controller, and digital voltmeter inside the space station via umbilical cable could make the required measurements. Since heating rates as low as 0.1 C/hour are required to study kinetics of the pyrolysis reations which are the cause of the high conductivity of the carbonaceous chondrites, experimental times up to 3 months will be needed.

Duba, A.↗

NASA NTRS1984

Thermal dependence of stress-induced birefringence in single mode optical fibers

Measurements of the change in stress-induced birefringence with temperature in single mode optical fibers are reported. The fibers examined include those with low residual stress birefringence that have circular and elliptical cores. A section of each fiber was placed under constant load with weights and heated inside a furnace. Polarized light was coupled into and out of the fiber ends outside the furnace. Two mutually perpendicular polarization components were analyzed and detected at the fiber output end. Changes in the detected signal levels were monitored as a function of the temperature of the single mode fiber stressed under constant load. Discussion of results and applications to localized stress measurements at high temperatures are presented.

Berthold, J. W., III↗

NASA NTRS1987

Corrosion of SiC by Molten Salt

Advanced ceramic materials considered for wide range of applications as in gas turbine engines and heat exchangers. In such applications, materials may be in corrosive environments that include molten salts. Very corrosive to alloys. In order to determine extent of problem for ceramic materials, corrosion of SiC by molten salts studied in both jet fuel burners and laboratory furnaces. Surface of silicon carbide corroded by exposure to flame seeded with 4 parts per million of sodium. Strength of silicon carbide decreased by corrosion in flame and tube-furnace tests.

Jacobson, Nathan S.↗

NASA NTRS1987

Computational analyses of crystal growth

Two important aspects of Hg/Cd/Te crystal growth processes are discussed. First, the thermal field and second, the fluid movement in the melt zone. The thermal analysis includes numerical calculation of axisymmetric heat conduction within the sample. It also includes a three-dimensional radiation model to calculate the radiative heat exchange between the furnace and the crystal as determined by the complex geometry of the furnace and the adiabatic shield. The thermal analysis also includes a crystal conductivity which is dependent on temperature and composition. To tackle the fluid flow aspect of the problem, an attempt was made to use a newly developed incompressible flow code based on the slight compressibility, and hence the finite sound speed, of all real fluids.

Dakhoul, Youssef M.↗

NASA NTRS1986

Flat-plate solar array project process development area: Process research of non-CZ silicon material

Several different techniques to simultaneously diffuse the front and back junctions in dendritic web silicon were investigated. A successful simultaneous diffusion reduces the cost of the solar cell by reducing the number of processing steps, the amount of capital equipment, and the labor cost. The three techniques studied were: (1) simultaneous diffusion at standard temperatures and times using a tube type diffusion furnace or a belt furnace; (2) diffusion using excimer laser drive-in; and (3) simultaneous diffusion at high temperature and short times using a pulse of high intensity light as the heat source. The use of an excimer laser and high temperature short time diffusion experiment were both more successful than the diffusion at standard temperature and times. The three techniques are described in detail and a cost analysis of the more successful techniques is provided.

Campbell, R. B.↗

NASA NTRS1986

Containerless processing technology

Ground- and space-based containerless processing levitation devices are described. Experiments performed in the MSFC drop tube, the JPL drag-free drop facilities, a single-axis tuned cavity acoustic levitator furnace on TEXUS-I, and a three-axis acoustic levitator and furnace on the STS-11 mission are discussed. Neither acoustic interference nor aerodynamic levitation trials have yielded promising results in sounding rocket and STS based experiments. An electrostatic levitator has furnished a high degree of positioning control with multiple objects in a terrestrial laboratory.

Naumann, R. J.↗

NASA NTRS1988

Imaging Of Directional-Solidification Interfaces

X-ray and gamma-ray technique developed at NASA Langley Research Center enables melt/solid interface to be observed visually during crystal growth by directional solidification in Bridgman furnace. Technique used to observe movement and shape of interface in germanium and in lead tin telluride. Valuable tool in efforts to grow seeded semiconductor materials in Bridgman furnaces.

Fripp, Archibald L., Jr.↗

NASA NTRS1988

A payload for investigating the influence of convection on GaAs crystal growth

A comparative study of the influence of buoyancy driven fluid flow on gallium arsenide (GaAs) crystal growth was undertaken. Crystals will be grown from melts with different degrees of convective flow including growth in the microgravity environment of space. The space growth of GaAs will be performed in a Get Away Special payload. A well insulated growth furnace was designed for both Earth-based and space-based experiments. The self contained payload will carry two such furnaces in addition to a large battery power source and a microprocessor-based control and data acquisition system for regulating the growth process with high precision. The microcomputer will also monitor the growth conditions and measure and record the acceleration in 3 axes.

Bellows, Alfred H.↗

NASA NTRS1987

Role of molybdenum in the Na2SO4 induced corrosion of superalloys at high temperature

Sodium sulfate induced corrosion of a molybdenum containing nickel-base superalloy, Udimet 700, was studied in laboratory furnace test and in a high velocity (Mach 0.3) burner rig. Tlhe effect of SO2 content in the atmosphere on the corrosion behavior in the laboratory furnace tests was determined. catastrophic corrosion occursonly when the melt contains MoO3 in addition to Na2SO4 and Na2MoO4. The conditions under which catastrophic corrosion occurs are identified and a mechanism is described to explain the catastrophic corrosion.

Misra, A. K.↗

NASA NTRS1988

Preparation for microgravity - The role of the Microgravity Material Science Laboratory

Experiments at the NASA Lewis Research Center's Microgravity Material Science Laboratory using physical and mathematical models to delineate the effects of gravity on processes of scientific and commercial interest are discussed. Where possible, transparent model systems are used to visually track convection, settling, crystal growth, phase separation, agglomeration, vapor transport, diffusive flow, and polymer reactions. Materials studied include metals, alloys, salts, glasses, ceramics, and polymers. Specific technologies discussed include the General Purpose furnace used in the study of metals and crystal growth, the isothermal dendrite growth apparatus, the electromagnetic levitator/instrumented drop tube, the high temperature directional solidification furnace, the ceramics and polymer laboratories and the center's computing facilities.

Johnston, J. Christopher↗

NASA NTRS1989

Thermal Analysis Of Reluctant Glass Formers

Thermocouple holds sample and monitors temperature during cooling. Ellipsoidal furnace provides controlled cooling rates for studies of thermal properties of reluctant glass formers. Glass tube inserted into furnace and used to blow helium on specimen to cool rapidly. Cooling curve analyzed to determine rate of cooling and such properties of sample as nucleation and recalescence temperatures at cooling rate. Continuous-cooling-crystallization boundaries determined empirically from plots of nucleation time vs. nucleation temperature from runs at large number of different rates of cooling. Apparatus used to examine glass-formation ability of material and critical cooling rate to form glass.

Ethridge, Edwin C.↗