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NASA NTRS2013

SparkJet Efficiency

A novel method for determining the thermal efficiency of the SparkJet is proposed. A SparkJet is attached to the end of a pendulum. The motion of the pendulum subsequent to a single spark discharge is measured using a laser displacement sensor. The measured displacement vs time is compared with the predictions of a theoretical perfect gas model to estimate the fraction of the spark discharge energy which results in heating the gas (i.e., increasing the translational-rotational temperature). The results from multiple runs for different capacitances of c = 3, 5, 10, 20, and 40 micro-F show that the thermal efficiency decreases with higher capacitive discharges.

Golbabaei-Asl, Mona↗

NASA NTRS1986

Development of an impulsive noise source to study the acoustic reflection characteristics of hard-walled wind tunnels

Two impulsive sound sources, one using multiple acoustic drivers and the other using a spark discharge were developed to study the acoustic reflection characteristics of hard-walled wind tunnels, and the results of laboratory tests are presented. The analysis indicates that though the intensity of the pulse generated by the spark source was higher than that obtained from the acoustic source, the number of averages needed for a particular test may require an unacceptibly long tunnel-run time due to the low spark generation repeat rate because of capacitor charging time. The additional hardware problems associated with the longevity of electrodes and electrode holders in sustaining the impact of repetitive spark discharges, show the multidriver acoustic source to be more suitable for this application.

Salikuddin, M.↗

NASA NTRS1983

Refinement and application of acoustic impulse technique to study nozzle transmission characteristics

An improved acoustic impulse technique was developed and was used to study the transmission characteristics of duct/nozzle systems. To accomplish the above objective, various problems associated with the existing spark-discharge impulse technique were first studied. These included (1) the nonlinear behavior of high intensity pulses, (2) the contamination of the signal with flow noise, (3) low signal-to-noise ratio at high exhaust velocities, and (4) the inability to control or shape the signal generated by the source, specially when multiple spark points were used as the source. The first step to resolve these problems was the replacement of the spark-discharge source with electroacoustic driver(s). These included (1) synthesizing on acoustic impulse with acoustic driver(s) to control and shape the output signal, (2) time domain signal averaging to remove flow noise from the contaminated signal, (3) signal editing to remove unwanted portions of the time history, (4) spectral averaging, and (5) numerical smoothing. The acoustic power measurement technique was improved by taking multiple induct measurements and by a modal decomposition process to account for the contribution of higher order modes in the power computation. The improved acoustic impulse technique was then validated by comparing the results derived by an impedance tube method. The mechanism of acoustic power loss, that occurs when sound is transmitted through nozzle terminations, was investigated. Finally, the refined impulse technique was applied to obtain more accurate results for the acoustic transmission characteristics of a conical nozzle and a multi-lobe multi-tube supressor nozzle.

Salikuddin, M.↗

NASA NTRS2021

Compact Augmented Spark Igniters for Liquid Rocket Engines

The objective of this dissertation is to characterize augmented spark impinging (torch) igniters. Torch igniters inject propellants into a small prechamber where a spark igniter imparts the activation energy to initiate combustion. The flame stabilizes within the prechamber and exits into the main combustion chamber where it ignites the main flow directly or by mixing with a coaxial flow to create a secondary flame. The underlying phenomena that promote reliable ignition are multifaceted and required a broad scope of investigations. Initial efforts focused on spark discharges across an annular geometry. Gaseous propellent projects the electrical arc toward the prechamber, where the arc and the thermal energy is imparted to the surrounding fluid then meets with a combustible mixture. Discharges are parametrically examined against pressure, spark-gap size, and exciter types to emulate transient engine startup. The energy imparted to the flow, approximate velocity, and distance traveled by the exhaust plume are determined. Spark quenching (no energy deposition) and its effects on perceived versus actual measurements are shown. Results outline the prechamber target zone where a combustible mixture is necessary for ignition. Next, three-dimensional, time-accurate, and nonreacting computational fluid dynamics simulations assess effects of geometric and mass flow differences on the size, location, and composition of a combustible mixture. Fluid dynamic phenomena are elucidated. Correlations between nondimensional variables are found. Results are coupled with a conservation-law analysis to produce novel objective functions. Lastly, a full-scale, modular torch igniter is tested. Injector sizes, mixture ratios, and injector momentum ratios are systematically varied to map ignition probability and ignition delay. Results show the importance of local mixture ratios, provide injector momentum ratios guidelines, and demonstrate reliable ignition of core mixture ratios typically outside flammability limits. The deliverable of this project is not a torch igniter or derivative thereof. Instead, this dissertation produces novel objective-functions for igniter design. These equations are functions of variables that may be constrained by engine-level requirements, physics, and experimental results from this work. They provide a foundation for future igniter design and will minimize iterative processes from the design cycle for next-generation ignition hardware.

Torch Igniter↗

NASA NTRS2023

Formation of Amino Acids and Carboxylic Acids in Weakly Reducing Planetary Atmospheres by Solar Energetic Particles from the Young Sun

Life most likely started during the Hadean Eon; however, the environmental conditions which contributed to the complexity of its chemistry are poorly known. A better understanding of various environmental conditions, including global (heliospheric) and local (atmospheric, surface, and oceanic), along with the internal dynamic conditions of the early Earth, are required to understand the onset of abiogenesis. Herein, we examine the contributions of galactic cosmic rays (GCRs) and solar energetic particles (SEPs) associated with superflares from the young Sun to the formation of amino acids and carboxylic acids in weakly reduced gas mixtures representing the early Earth’s atmosphere. We also compare the products with those introduced by lightning events and solar ultraviolet light (UV). In a series of laboratory experiments, we detected and characterized the formation of amino acids and carboxylic acids via proton irradiation of a mixture of carbon dioxide, methane, nitrogen, and water in various mixing ratios. These experiments show the detection of amino acids after acid hydrolysis when 0.5% (v/v) of initial methane was introduced to the gas mixture. In the set of experiments with spark discharges (simulation of lightning flashes) performed for the same gas mixture, we found that at least 15% methane was required to detect the formation of amino acids, and no amino acids were detected in experiments via UV irradiation, even when 50% methane was used. Carboxylic acids were formed in non-reducing gas mixtures (0% methane) by proton irradiation and spark discharges. Hence, we suggest that GCRs and SEP events from the young Sun represent the most effective energy sources for the prebiotic formation of biologically important organic compounds from weakly reducing atmospheres. Since the energy flux of space weather, which generated frequent SEPs from the young Sun in the first 600 million years after the birth of the solar system, was expected to be much greater than that of GCRs, we conclude that SEP-driven energetic protons are the most promising energy sources for the prebiotic production of bioorganic compounds in the atmosphere of the Hadean Earth.

Kensei Kobayashi↗

NASA NTRS1991

Electrostatic fields in a dusty Martian environment

While there have been several studies suggesting the possibility of electrical activity on Mars, to date there have been no measurements to search for evidence of such activity. In the absence of widespread water clouds and convective storm systems similar to those on the Earth and Jupiter, the most likely candidate for the creation of electrostatic charges and fields is triboelectric charging of dust, i.e., the friction between blown dust and the ground, and of dust particles with each other. Terrestrial experience demonstrates that electric fields 5 to 15 kV-m(exp -1) are not uncommon in dust storms and dust devils in desert regions, where the polarity varies according to the chemical composition and grain size. Simple laboratory experiments have demonstrated that modest electrostatic fields of roughly 5,000 V-m(exp -1) may be produced, along with electrical spark discharges and glow discharges, in a simulation of a dusty, turbulent Martian surface environment. While the Viking landers operated for several years with no apparent deleterious effects from electrostatic charging, this may have been at least partly due to good engineering design utilizing pre-1976 electronic circuitry to minimize the possibility of differential charging among the various system components. However, free roaming rovers, astronauts, and airborne probes may conceivably encounter an environment where electrostatic charging is a frequent occurrence, either by way of induction from a static electric field or friction with the dusty surface and atmosphere. This raises the possibility of spark discharges or current surges when subsequent contact is made with other pieces of electrical equipment, and the possibility of damage to modern microelectronic circuitry. Measurements of electrostatic fields on the surface of Mars could therefore be valuable for assessing this danger. Electric field measurements could also be useful for detecting natural discharges that originate in dust storms. This detection could be performed at distances ranging from 10s of km in the case of J-charge-like discharge signatures, to planetary distances if there exists a global electrical circuit or Schumann resonance spectrum.

Sentman, D. D.↗

NASA NTRS1992

Hydrothermal organic synthesis experiments

The serious scientific debate about spontaneous generation which raged for centuries reached a climax in the nineteenth century with the work of Spallanzani, Schwann, Tyndall, and Pasteur. These investigators demonstrated that spontaneous generation from dead organic matter does not occur. Although no aspects of these experiments addressed the issue of whether organic compounds could be synthesized abiotically, the impact of the experiments was great enough to cause many investigators to assume that life and its organic compounds were somehow fundamentally different than inorganic compounds. Meanwhile, other nineteenth-century investigators were showing that organic compounds could indeed be synthesized from inorganic compounds. In 1828 Friedrich Wohler synthesized urea in an attempt to form ammonium cyanate by heating a solution containing ammonia and cyanic acid. This experiment is generally recognized to be the first to bridge the artificial gap between organic and inorganic chemistry, but it also showed the usefulness of heat in organic synthesis. Not only does an increase in temperature enhance the rate of urea synthesis, but Walker and Hambly showed that equilibrium between urea and ammonium cyanate was attainable and reversible at 100 C. Wohler's synthesis of urea, and subsequent syntheses of organic compounds from inorganic compounds over the next several decades dealt serious blows to the 'vital force' concept which held that: (1) organic compounds owe their formation to the action of a special force in living organisms; and (2) forces which determine the behavior of inorganic compounds play no part in living systems. Nevertheless, such progress was overshadowed by Pasteur's refutation of spontaneous generation which nearly extinguished experimental investigations into the origins of life for several decades. Vitalism was dealt a deadly blow in the 1950's with Miller's famous spark-discharge experiments which were undertaken in the framework of the Oparin and Haldane hypotheses concerning the origin of life. These hypotheses were constructed on some basic assumptions which included a reduced atmosphere, and a low surface temperature for the early Earth. These ideas meshed well with the prevailing hypothesis of the 1940's and 50's that the Earth had formed through heterogeneous accretion of dust from a condensing solar nebula. Miller's experiments were extremely successful, and were followed by numerous other experiments by various investigators who employed a wide variety of energy sources for abiotic synthesis including spark discharges, ultra-violet radiation, heat, shock waves, plasmas, gamma rays, and other forms of energy. The conclusion reached from this body of work is that energy inputs can drive organic synthesis from a variety of inorganic starting materials.

Shock, Everett L.↗

NASA NTRS1991

Effect of pressure on electrostatic processes on Mars

Paschen's Law as illustrated by Paschen curves for various gases shows that the minimum breakdown voltage for gases for breakdown distances of interest, i.e., 1 to 1000 mm is at or near the surface pressure on Mars. This means that the physics of many electrostatic processes is markedly different on Mars than on Earth. The primary effect is that voltage potentials above 100 volts are subject to breakdown in the Martian atmosphere. Sharp electrodes, dusty atmospheric conditions, or other anomalies modify the breakdown voltage, usually causing lower breakdown voltages. Paschen's curves for most common pure gases were experimentally determined. A very small amount of mixing of different gases radically changes the curve as shown in the curve for neon plus 0.1 percent argon compared to either neon or argon. Paschen's curve for the exact composition of gases for Mars was not determined; thus, the breakdown voltages are not known. A second important effect is that the breakdown for most Martian cases is a glow discharge rather than a spark discharge. It would seem that simple measurements of breakdown manner and voltage should be included on a Mars lander vehicle.

Leach, Rodman N.↗

NASA NTRS2014

Conducting Miller-Urey Experiments

In 1953, Stanley Miller reported the production of biomolecules from simple gaseous starting materials, using apparatus constructed to simulate the primordial Earth's atmosphere-ocean system. Miller introduced 200 ml of water, 100 mmHg of H2, 200mmHg of CH4, and 200mmHg of NH3 into the apparatus, then subjected this mixture, under reflux, to an electric discharge for a week, while the water was simultaneously heated. The purpose of this manuscript is to provide the reader with a general experimental protocol that can be used to conduct a Miller-Urey type spark discharge experiment, using a simplified 3 L reaction flask. Since the experiment involves exposing inflammable gases to a high voltage discharge, it is worth highlighting important steps that reduce the risk of explosion. The general procedures described in this work can be extrapolated to design and conduct a wide variety of electric discharge experiments simulating primitive planetary environments.

Prebiotic chemistry↗

NASA NTRS1975

A composition analyzer for microparticles using a spark ion source

Iron microparticles were fired onto a capacitor-type microparticle detector which responded to an impact with a spark discharge. Ion currents were extracted from the spark and analyzed in a time-of-flight mass spectrometer. The mass spectra showed the element of both detector and particle materials. The total extracted ion currents was typically 10A within a period of 100ns, indicating very efficient vaporization of the particle and ionization of the vapor. Potential applications include research on cosmic dust, atmospheric aerosols and cloud droplets, particles ejected by rocket or jet engines, by machining processes, or by nuclear bomb explosions.

Auer, S. O.↗

NASA NTRS1975

Composition analyzer for microparticles using a spark ion source

Iron microparticles were fired onto a capacitor-type microparticle detector which responded to an impact with a spark discharge. Ion currents were extracted from the spark and analyzed in a time-of-flight mass spectrometer. The mass spectra showed the elements of both detector and particle materials. The total extracted ion current was typically 10 A within a period of 100 nsec, indicating very efficient vaporization of the particle and ionization of the vapor. Potential applications include research on cosmic dust, atmospheric aerosols and cloud droplets, particles ejected by rocket or jet engines, by machining processes or by nuclear bomb explosions.

Auer, S.↗

NASA NTRS1971

Pyrotechnic hazards classification and evaluation program. Electrostatic vulnerability of the E8 and XM15/XM165 clusters, phase 2

An investigation into the electrostatic phenomena associated with the manufacturing and handling of explosives is discussed. The testing includes measurement of the severity of the primary charge generation mechanism, triboelectric effects between dissimilar surfaces; refinement of equivalent circuits of the XM15/XM165 and E8 fuse trains; evaluation of the electrostatic spark discharge characteristics predicted by an equivalent circuit analysis; and determination of the spark ignition sensitivity of materials, components, junctions, and subassemblies which compose the XM15/XM165 and E8 units. Special studies were also performed. These special tests included ignition sensitivity of the complete XM15 fuse train when subjected to discharges through its entire length, measurement of electrostatic potentials which occur during the E8 foaming operation during fabrication, and investigation of the inadvertent functioning of an XM15 cluster during manufacturing. The test results are discussed and related to the effectiveness of suggested modification to reduce the electrostatic ignition sensitivity.

Source record↗

NASA NTRS1925

Flame Speed and Spark Intensity

This report describes a series of experiments undertaken to determine whether or not the electrical characteristics of the igniting spark have any effect on the rapidity of flame spread in the explosive gas mixtures which it ignites. The results show very clearly that no such effect exists. The flame velocity in carbon-monoxide oxygen, acetylene oxygen, and gasoline-air mixtures was found to be unaffected by changes in spark intensity from sparks which were barely able to ignite the mixture up to intense condenser discharge sparks having fifty time this energy. (author)

Randolph, D W↗

NASA NTRS1951

Spark Ignition of Flowing Gases. 2: Effect of Electrode Parameters on Energy Required to Ignite a Propane-Air Mixture

Research was conducted to determine the effect of the electrode parameters of spacing, configuration, and material' on the energy required for ignition of a flowing propane-air mixture. In addition, the data were used to indicate the energy distribution along the spark length and to confirm previous observations concerning the effect of spark duration on ignition energy requirements. The data were obtained with a mixture at a fuel-air ratio of 0.0835 (by weight), a pressure of 3 inches of mercury absolute, a temperature of 80 F, and a mixture velocity of 5 feet per second. Results showed that the energy required for ignition decreased as the electrode spacing was increased; a minimum energy occurred at. a spacing of 0.65 inch for large electrodes. For small electrodes, the spacing for minimum energy was not sharply defined. Small-diameter electrodes required less energy than large-diameter electrodes if the spacing was less than the optimum distance of 0.65 inch; at a spacing equal to the optimum distance, no difference was noted. Significant effects of electrode material on ignition energy were ascribed to differences in the type of spark discharges produced; glow discharges required higher energy than the arc-glow discharges. With pure glow discharges, the ignition energy was substantially constant for lead, cadmium, brass, aluminum, and tungsten electrodes. A method is described for determining the energy distribution along a glow discharge. It was found that one-third to one-half of the energy in the spark was concentrated in a small region near the cathode electrode, and the remainder was uniformly distributed across the spark gap. It was impossible to ascertain the dependence of ignition on. this distribution. It was also observed that long-duration (600 microsec) sparks required much less energy for ignition than did short-duration (1 microsec) sparks.

Swett, Clyde. C., Jr.↗

NASA NTRS1974

Dicarboxylic acids from electric discharge

An investigation was conducted concerning the possible synthesis of a suite of dicarboxylic acids similar to that found in the Murchison meteorite. The investigation included the conduction of a chemical evolution experiment which simulated electric discharge through the primitive atmosphere of the earth. The suite of dicarboxylic acids obtained in the electric discharge experiment is similar to that of the Murchison meteorite, except for the fact that 2-chlorosuccinic acid is present in the spark discharge.

Zeitman, B.↗

NASA NTRS2008

Making Superconducting Welds between Superconducting Wires

A technique for making superconducting joints between wires made of dissimilar superconducting metals has been devised. The technique is especially suitable for fabrication of superconducting circuits needed to support persistent electric currents in electromagnets in diverse cryogenic applications. Examples of such electromagnets include those in nuclear magnetic resonance (NMR) and magnetic resonance imaging (MRI) systems and in superconducting quantum interference devices (SQUIDs). Sometimes, it is desirable to fabricate different parts of a persistent-current-supporting superconducting loop from different metals. For example, a sensory coil in a SQUID might be made of Pb, a Pb/Sn alloy, or a Cu wire plated with Pb/Sn, while the connections to the sensory coil might be made via Nb or Nb/Ti wires. Conventional wire-bonding techniques, including resistance spot welding and pressed contact, are not workable because of large differences between the hardnesses and melting temperatures of the different metals. The present technique is not subject to this limitation. The present technique involves the use (1) of a cheap, miniature, easy-to-operate, capacitor-discharging welding apparatus that has an Nb or Nb/Ti tip and operates with a continuous local flow of gaseous helium and (2) preparation of a joint in a special spark-discharge welding geometry. In a typical application, a piece of Nb foil about 25 m thick is rolled to form a tube, into which is inserted a wire that one seeks to weld to the tube (see figure). The tube can be slightly crimped for mechanical stability. Then a spark weld is made by use of the aforementioned apparatus with energy and time settings chosen to melt a small section of the niobium foil. The energy setting corresponds to the setting of a voltage to which the capacitor is charged. In an experiment, the technique was used to weld an Nb foil to a copper wire coated with a Pb/Sn soft solder, which is superconducting. The joint was evaluated as part of a persistent-current circuit having an inductance of 1 mH. A current was induced in a loop, and no attenuation of the current after a time interval 1,000 s was discernible in a measurement having a fractional accuracy of 10(exp -4): This observation supports the conclusion that the weld had an electrical resistance <10(exp -10) omega.

Penanen, Konstantin I.↗

NASA NTRS1993

Low power arcjet system spacecraft impacts

Potential plume contamination of spacecraft surfaces was investigated by positioning spacecraft material samples relative to an arcjet thruster. Samples in the simulated solar array region were exposed to the cold gas arcjet plume for 40 hrs to address concerns about contamination by backstreaming diffusion pump oil. Except for one sample, no significant changes were measured in absorptance and emittance within experimental error. Concerns about surface property degradation due to electrostatic discharges led to the investigation of the discharge phenomenon of charged samples during arcjet ignition. Short duration exposure of charged samples demonstrated that potential differences are consistently and completely eliminated within the first second of exposure to a weakly ionized plume. The spark discharge mechanism was not the discharge phenomenon. The results suggest that the arcjet could act as a charge control device on spacecraft.

Pencil, Eric J.↗

NASA NTRS2011

Exploring the Fate of Nitrogen Heterocycles in Complex Prebiotic Mixtures

A long standing question in the field of prebiotic chemistry is the origin of the genetic macromolecules DNA and RNA. DNA and RNA have very complex structures with repeating subunits of nucleotides, which are composed of nucleobases (nitrogen heterocycles) connected to sugar-phosphate. Due to the instability of some nucleobases (e.g. cytosine), difficulty of synthesis and instability of D-ribose, and the likely scarcity of polyphosphates necessary for the modern nucleotides, alternative nucleotides have been proposed for constructing the first genetic material. Thus, we have begun to investigate the chemistry of nitrogen heterocycles in plausible, complex prebiotic mixtures in an effort to identify robust reactions and potential alternative nucleotides. We have taken a complex prebiotic mixture produced by a spark discharge acting on a gas mixture of N2, CO2, CH4, and H2, and reacted it with four nitrogen heterocycles: uracil, 5-hydroxymethyluracil, guanine, and isoxanthopterin (2-amino-4,7-dihydroxypteridine). The products of the reaction between the spark mixture and each nitrogen heterocycle were characterized by liquid chromatography coupled to UV spectroscopy and Orbitrap mass spectrometry. We found that the reaction between the spark mixtUl'e and isoxanthopterin formed one major product, which was a cyanide adduct. 5-hydroxymethyluracil also reacted with the spark mixture to form a cyanide adduct, uracil-5-acetonitrile, which has been synthesized previously by reacting HCN with S-hydroxymethyluracil. Unlike isoxanthopterin, the chromatogram of the 5-hydroxymethyluracil reaction was much more complex with multiple products including spark-modified dimers. Additionally, we observed that HMU readily self-polymerizes in solution to a variety of oligomers consistent with those suggested by Cleaves. Guanine and uracil, the biological nucleobases, did not react with the spark mixture, even at high temperature (100 C). This suggests that there are alternative nucleobases which are more reactive under prebiotic conditions and may have been involved in producing precursor nucleotides.

Smith, Karen E.↗