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Explore NASA and DOE materials research. Search alloys, composites and material properties, then open the original technical report for test conditions and results.

At least 1,603 records · Page 89

An experimental and analytical investigation of the rail shear-test method as applied to composite materials

This report presents the results from an experimental and analytical investigation of the stress distributions occurring in a rail shear test. The effects of non-uniform stresses induced by differential thermal expansion, rail flexibility and specimen aspect ratio on measured shear modulus and ultimate strength of composite laminates are shown. A two-dimensional linearly elastic finite element model was used to analytically determine how various geometric parameters influenced the magnitude and distribution of inplane normal and shear stresses in a tensile rail shear specimen. Rail shear tests were conducted at room temperature and 589 K (600 F) on selected graphite-polyimide composite laminates using two titanium rail configurations. The analysis and test methods are discussed, and the results of the effects of the various parameters on shear modulus and ultimate strength are presented.

Garcia, R.↗

Thermal expansion and swelling of cured epoxy resin used in graphite/epoxy composite materials

The paper presents results of experiments in which the thermal expansion and swelling behavior of an epoxy resin system and two graphite/epoxy composite systems exposed to water were measured. It was found that the cured epoxy resin swells by an amount slightly less than the volume of the absorbed water and that the swelling efficiency of the water varies with the moisture content of the polymer. Additionally, the thermal expansion of cured epoxy resin that is saturated with water is observed to be more than twice that of dry resin. Results also indicate that cured resin that is saturated with 7.1% water at 95 C will rapidly increase in moisture content to 8.5% when placed in 1 C water. The mechanism for this phenomenon, termed reverse thermal effect, is described in terms of a slightly modified free-volume theory in conjunction with the theory of polar molecule interaction. Nearly identical behavior was observed in two graphite/epoxy composite systems, thus establishing that this behavior may be common to all cured epoxy resins.

Adamson, M. J.↗

Composite-Material Point-Stress Analysis

PSANAL computes composite-laminate elastic and thermal properties and allowable load levels for any combination of applied membrane and bending loads occurring at a point. Basic linear orthotropic stress/ strain relationships and standard composite-laminate theory formulas are utilized.

Spears, F., S.↗

Environmental Exposure Effects on Composite Materials for Commercial Aircraft

This period's activities were highlighted by continued long term and accelerated lab exposure testing, and by completion of all fabrication tasks on the optional material systems, AS1/3501-6 and Kevlar 49/F161-188. Initial baseline testing was performed on the two optional material systems. Long term exposure specimens were returned from three of the four ground rack sites and from two of the three aircraft locations. Test data from specimens returned from Dryden after 2 years exposure do not indicate continuing trends of strength reduction from the 1 year data. Test data from specimens returned from the Wellington, new Zealand ground rack and on Air New Zealand aircraft after 1 year exposure show strength changes fairly typical of other locations.

Hoffman, D. J.↗

Three dimensional finite element analysis of layered fiber-reinforced composite materials

A three-dimensional finite element analysis was performed for a biaxially loaded composite laminate (with a centered hole) consisting of several fiber-reinforced composite layers each with a specified fiber orientation. The detailed stress distribution around the hole was determined. Also, the locations of initial damage zones due to different failure mechanisms were indicated.

Lee, J. D.↗

Application of the cubic polynomial strength criterion to the failure analysis of composite materials

A comparative failure analysis is presented based on the application of quadratic and cubic forms of the tensor polynomial lamina strength criterion to various composite structural configurations in a plane stress state. Failure loads have been predicted for off-angle laminates under simple loading conditions and for symmetric-balanced laminates subject to varying degrees of biaxial tension, including configurations subject to multimode failures. Some experimental data are also provided to support these calculations. From these results, the necessity of employing a cubic strength criterion to accurately predict the failure of composite laminae is demonstrated.

Tennyson, R. C.↗

Environmental effects on defect growth in composite materials

Data for evaluating the effects of moisture and temperature on the integrity of fiber composite components was gathered. In particular, the static and cyclic performance of three composite laminates containing flaws was investigated at room temperature and at 422 K (300 F) in wet and dry conditions.

Porter, T. R.↗

Tribological evaluation of composite materials made from a partially fluorinated polyimide

Preliminary tribological studies on a new polyimide formulated from the diamine 2,2-bis 4-(4-aminophenoxy) phenyl hexafluoropane (4-BDAF) indicates polyimides made from this diamine have excellent potential for high temperature applications. Two different polyimides were formulated from the diamine, and five different composites were formulated using one of the polyimides. Composites were made using 10 weight percent (w/o) graphite fluoride powder, 20 w/o PTFE powder, 30 w/o silver powder, or 50 w/o carbon fibers, both graphitic and nongraphitic types. The powder additions did not improve the tribological properties as much as the carbon fibers, and the graphitic fibers produced better results than did the nongraphitic fibers. Results also indicated that improved high temperature stability and tribological properties may be obtained with a polyimide made from the dianhydride pyromellitic acid (PMDA) rather than the dianhydride benzophenonetetracarboxylic acid (BTDA).

Fusaro, R. L.↗

Attaching Strain Gages to Composite Materials

Polyurethane adhesive bonds strain gages reliably to graphite/epoxy composites. Adhesive easy to apply, used over wide temperature range (ambient to cryogenic), and applied in short time. Tests on gages bonded to composite with adhesive demonstrated reliability of attachment.

Penn, B.↗

Space Radiation Effects on Graphite-Epoxy Composite Materials

Radiation effects on engineering properties, dimensional stability, and chemistry on state of the art composite systems were characterized. T300/934 graphite-epoxy composite was subjected to 1.0 MeV electron radiation for a total dose of 1.0 x 10(10) rads at a rate of 5.0 x 10(7) rads/hour. This simulates a worst case exposure equivalent to 30 years in space. Mechanical testing was performed on he 4-ply unidirectional laminates over the temperature range of -250 F (116K) to +250 F (394K). A complete set of in-plane tensile elastic and strength properties were obtained (E sub 1, E sub 2, nu sub 12, G sub 12, X sub T, Y sub T, and S). In addition electron microscopy was used to study and analyze the fracture surfaces of all specimens tested. Results indicate that little difference in properties is noted at room temperature, but significant differences are observed at both low and elevated temperatures.

Milkovich, S. M.↗

Fracture toughness of fibrous composite materials

Laminates with various proportions of 0 deg, 45 deg, and 90 deg plies were fabricated from T300/5208 and T300/BP-907 graphite/epoxy prepreg tape material. The fracture toughness of each laminate orientation or lay-up was determined by testing center-cracked specimens, and it was also predicted with the general fracture-toughness parameter. The predictions were good except when crack-tip splitting was large, at which time the toughness and strengths tended to be underpredicted. By using predictions, a parametric study was also made of factors that influence fracture toughness. Fiber and matrix properties as well as lay-up were investigated. Without crack-tip splitting, fracture toughness increases in proportion to fiber strength and fiber volume fraction, increases linearly with E(22)/E(11), is largest when the modulus for non-0 deg fibers is greater than that of 0 deg fibers, and is smallest for 0(m)/90(p)(s) lay-ups. (The E(11) and E(22) are Young's moduli of the lamina parallel to and normal to the direction of the fibers, respectively). For a given proportion of 0 deg plies, the most notch-sensitive lay-ups are 0(m)/90(p)(s) and the least sensitive are 0(m)/45(n)(s) and alpha(s). Notch sensitivity increases with the proportion of 0 deg plies and decreases with alpha. Strong, tough matrix materials, which inhibit crack-tip splitting, generally lead to minimum fracture toughness.

Poe, C. C., Jr.↗

A study of the stress wave factor technique for the characterization of composite materials

This study has investigated the potential of the Stress Wave Factor as an NDT technique for thin composite laminates. The conventional SWF and an alternate method for quantifying the SWF were investigated. Agreement between the initial SWF number, ultrasonic C-scan, inplane displacements as obtained by full field moire interferometry, and the failure location have been observed. The SWF number was observed to be the highest when measured along the fiber direction and the lowest when measured across the fibers. The alternate method for quantifying the SWF used square root of the zeroth moment (square root of M sub o) of the frequency spectrum of the received signal as a quantitative parameter. From this study it therefore appears that the stress wave factor has an excellent potential to monitor damage development in thin composite laminates.

Govada, A. K.↗

The compositions of chondrules in unequilibrated chondrites An evaluation of models for the formation of chondrules and their precursor materials

Recent progress toward the resolution of the problem of chondrule composition is reviewed. Special attention is given to studies of both the chemical and textural properties of chondrules. The characteristic variations of the composition of carbonaceous chondrite chrondules are discussed within the framework of current theories of chondrule evolution. Consideration is also given to the possible mechanisms for chondrule melts, and the relationship between chondrules and other chondrite components.

Grossman, J. N.↗

Mechanical properties testing of candidate polymer matrix materials for use in high performance composites

The mechanical properties of four candidate neat resin systems for use in graphite/epoxy composites are characterized. This includes tensile and shear stiffnesses and strengths, coefficients of thermal and moisture expansion, and fracture toughness. Tests are conducted on specimens in the dry state and moisture-saturated, at temperatures of 23C, 82C and 121C. The neat resins tested are Hexcel HX-1504, Narmco 5245-C, American Cyanamid CYCOM 907, and Union Carbide ERX-4901A (MDA). Results are compared with those obtained for four other epoxy resins tested in a prior program, i.e., Hercules 3502, 2220-1, and 2220-3, and Ciba-Geigy Fibredux 914, as well as with available Hercules 3501-6 data. Scanning electron microscopic examination of fracture surfaces is performed to permit the correlation of observed failure modes with the environmental test conditions. A finite element micromechanics analysis is used to predict unidirectional composite response under various test conditions, using the measured neat resin properties as input data.

Zimmerman, R. S.↗

The effect of low velocity impact on the strength characteristics of composite materials laminates

The nonlinear and dynamic response of composite structures to impact loading conditions was investigated. The convergence of both finite element and finite difference solution procedures was investigated with this configuration. The response of composite beams and plates to impact were examined. Fundamental data on the indentation and flexural response of both plate and beam geometry were collected. Numerical analyses were extended to the study of circular plates subjected to impact loading. Further work was done in modeling the response to simulated impact loading through careful modeling of the momentum transfer from impactor to target. The modeling methodology and solution procedures were well tested and verified. A computer program for the solution of circular plate problems was developed and is under testing.

Liebowitz, H.↗

A parametric study of fracture toughness of fibrous composite materials

Impacts to fibrous composite laminates by objects with low velocities can break fibers giving crack-like damage. The damage may not extend completely through a thick laminate. The tension strength of these damage laminates is reduced much like that of cracked metals. The fracture toughness depends on fiber and matrix properties, fiber orientations, and stacking sequence. Accordingly, a parametric study was made to determine how fiber and matrix properties and fiber orientations affect fracture toughness and notch sensitivity. The values of fracture toughness were predicted from the elastic constants of the laminate and the failing strain of the fibers using a general fracture toughness parameter developed previously. For a variety of laminates, values of fracture toughness from tests of center-cracked specimens and values of residual strength from tests of thick laminates with surface cracks were compared to the predictions to give credibility to the study. In contrast to the usual behavior of metals, it is shown that both ultimate tensile strength and fracture toughness of composites can be increased without increasing notch sensitivity.

Poe, C. C., Jr.↗

Analysis of woven fabrics for reinforced composite materials

The use of woven fabrics as reinforcements for composites is considered. Methods of analysis of properties are reviewed and extended, with particular attention paid to three-dimensional constructions having through-the-thickness reinforcements. Methodology developed is used parametrically to evaluate the performance potential of a wide variety of reinforcement constructions including hybrids. Comparisons are made of predicted and measured properties of representative composites having biaxial and triaxial woven, and laminated tape lay-up reinforcements. Overall results are incorporated in advanced weave designs.

Dow, Norris F.↗