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At least 19 records

Variable temperature pressure cell for polycrystalline X-ray studies down to 2 K - Application to Bi

A variable pressure diamond anvil cell is described for operation at temperatures continuously variable from 300 down to 2 K and controllable within 10 mK. Polycrystalline X-ray data are collected from the pressure cavity by means of either (1) standard photographic techniques, (2) diffractometer measurements, or (3) energy dispersive diffractometry. The facility has been used to examine parts of the phase diagram of Bi. Results from this study indicate that the Bi-I and Bi-III structures are retained to low temperatures; however, there is no evidence to support a structural transition from Bi-V to Bi-VIII.

Skelton, E. F.↗

Contribution of intermediate luminosity X-ray galaxies to the background - Anon 0945-30

Evidence that the galaxy A0945-30 is a new extragalactic X-ray source was found from an analysis of rotating modulation collimator quick-look data collected from the SAS 3 X-ray observatory. A strong piece of evidence was the hydrogen column density of 3 plus or minus 1 times 10 to the 22nd power per sq cm for a power law spectrum extending to about 35 keV inferred from HEAO 1 data. Observations indicate that the galaxy is an early type spiral with a bright nucleus. A faint star alongside the galaxy within the 90% confidence X-ray source error circle is an F dwarf with no indication of emission features. Spectra of the galaxy in the red and blue show sharp, intermediate strength emission lines of forbidden O III, forbidden N II, and H-alpha together with strong Mg, Fe, Ca absorption features characteristic of a normal stellar continuum in the galactic nucleus.

Schnopper, H. W.↗

Trace elemental characteristics of aerosols emitted from municipal incinerators

As part of a continuing investigation of high temperature combustion aerosols, elemental composition of size differentiated aerosols emitted from a local municipal incinerator was studied. Aerosols were aerodynamically separated into eight diameter groups ranging from 0.43 mm to 20 mm, collected, and analyzed by charged particle induced X-ray emission technique. On line data collection and reduction codes generated aerial densities for elements from Na to U with sensitivities in the ng/cu m range for most elements. From the total weights of aerosols collected per stage, their size distribution was determined to be bimodal, with one group centered at a diameter of 0.54 mm and the other at a diameter of 5.6 mm. Measured elemental concentrations in various size ranges indicate that K and S show a strong tendency to concentrate on aerosol surfaces. A weaker trend for surface preference was also observed for Mn and Ni, but other elements show no such trend.

Singh, J. J.↗

The detection of extended X-ray emission surrounding cD galaxies in poor clusters

The paper presents some preliminary results of a survey, performed with an imaging proportional counter, to detect X-ray emission from poor clusters which nevertheless contain dominant D or cD galaxies and could, therefore, be classified as Bautz-Morgan Type I. The data suggest that poor clusters can collect enough gas to become detectable X-ray sources if they are relatively compact, which the presence of dominant galaxies indicates.

Kriss, G. A.↗

Extended X-ray and radio observations of Scorpius X-1.

A 23-day observation reveals temporal variations at energies of 3-10 keV similar to those found in previous optical data. However, there is no evidence of more than one preferred intensity level or of an intensity threshold for flares. We rule out X-ray periodicities containing more than 5 per cent of the mean quiescent-period intensity with periods of from 6 minutes to 4 hours. The X-ray intensity is strongly correlated with hardness but is not correlated with radio data collected over eight days.

Canizares, C. R.↗

Mapping of electrical potential distribution with charged particle beams

Potentials were measured using a beam of soft X-rays in air at 2 x 10 to the -5 power Torr. Ions were detected by a continuous-dynode electron multiplier after they passed through a retarding field. Ultimate resolution depends upon the diameter of the X-ray beam which was 3 mm. When the fields in the region of interest were such to disperse the ions, only a small fraction were detected and the method of measurement was not very reliable. Yet reasonable data could be collected if the ions traveled in parallel paths toward the detector. Development should concentrate on increasing the aperture of the detector from the pinhole which was used to something measured in centimeters. Also increasing the strength of the source would provide a stronger signal and more reliable data. Measurements were made at an estimated ion current to 10 to the -15 power A from a 10 cm length of the X-ray beam, this current being several orders of magnitude below what would have a perturbing effect on the region to be measured. Consequently, the source strength can be increased and prospects for this method of measurement are good.

Robinson, J. W.↗

Remote sensing data applied to the evaluation of soil erosion caused by land-use. Ribeirao Anhumas Basin Area: A case study

Formerly covered by a tropical forest, the study area was deforested in the early 40's for coffee plantation and cattle raising, which caused intense gully erosion problems. To develop a method to analyze the relationship between land use and soil erosion, visual interpretations of aerial photographs (scale 1:25.000), MSS-LANDSAT imagery (scale 1:250,000), as well as automatic interpretation of computer compatible tapes by IMAGE-100 system were carried out. From visual interpretation the following data were obtained: land use and cover tapes, slope classes, ravine frequency, and a texture sketch map. During field work, soil samples were collected for texture and X-ray analysis. The texture sketch map indicate that the areas with higher slope angles have a higher susceptibilty to the development of gullies. Also, the over carriage of pastureland, together with very friable lithologies (mainly sandstone) occuring in that area, seem to be the main factors influencing the catastrophic extension of ravines in the study site.

Dejesusparada, N.↗

Stardust.

Rocket experiments were conducted to collect particles from noctilucent clouds at Kiruna, Sweden. The Pandora II inflight shadowing technique considered by Hallgren and Hemenway (1971) was used in the experiments. This technique makes it possible to study the collected particles as a function of time and altitude intervals. The particles observed consisted of an irregular electron-opaque core surrounded by a rounded, low density material. X-ray and electron opacity data suggest that the abundances of the heavy elements, such as Hf and Ta, in the particles are comparable to those of the light elements, such as Al and Si.

Hemenway, C. L.↗

Determination of volume fraction in multiphase systems using incomplete pole figures

The determination of the volume fraction of a second phase in a multiphase sample by X-ray diffraction becomes more difficult if the diffracting planes have a preferred orientation. Lopata and Kula have described a method of treating this problem using complete pole figures for each of the phases. With some samples, it is not always possible or convenient to obtain data over the full hemisphere. Equations and an example are given which require X-ray data over a limited range of approximately 0 to 75 deg. This can be obtained by reflection without a specially cut sample or transmission data. A series of Legendre polynomials are fitted to data collected while spinning the sample about its normal. An extrapolation is made possible by introducing two conditions on the end points which must be satisfied if the extrapolation functions are to be valid.

Houska, C. R.↗

High temperature cyclic oxidation furnace testing at NASA Lewis Research Center

A standardized method of testing the cyclic oxidation resistance of various alloys in static air up to 1200 C has been developed and routinely used at the NASA Lewis Research Center. Test samples are automatically raised and lowered into a resistance wound furnace for a series of fixed-interval heating and cooling cycles. Spall catchers collect the accumulated spall from each sample. The samples are weighed intermittently to generate specific weight change with time data. At various test times the samples and the accumulated spall are analyzed by X-ray diffraction. A computer program is used to print out the specific weight change versus time data and the X-ray data in tabular form and to plot the specific weight change versus time data in a publishable format. The data are also organized and indexed. So far several hundred Fe-, Ni-, and Co-base alloys have been tested using this basic procedure and will form the basis of a series of cyclic oxidation handbooks to be published by NASA. Such specific weight change/time data have been used to estimate the oxidative metal consumption by several computer modeling techniques both to rank alloys and to estimate life.

Barrett, C. A.↗

A gamma ray monitor for the OSO-7 spacecraft

A 3 in. x 3 in. NaI(Tl) gamma ray (0.3 to 10 MeV) spectrometer with a CsI(Na) charged particle and anti-Compton shield has been developed for the Orbiting Solar Observatory (OSO-7) which was launched September 30, 1971. The instrument, designed for a rotating wheel compartment, utilizes a 377 channel quadratic PHA with accumulation times of 3, 1, or 0.5 minutes. Quick look and calibration data obtained via a direct data link to a minicomputer allows near real time monitoring and control of the experiment. Various commands changing the operating mode can be executed. The functions which can be commanded include: rotation of the quadrants in which data is collected by 90 deg; gain adjustment of the central detector over a 6:1 range; manual or automatic sequencing of calibrations; variations of accumulation times by telemetering selected channels; and selection of reference directions. A small X-ray detector covering the range 7.5 to 120 keV is also included.

Higbie, P. R.↗

HEAO-B and -C engineering design and scientific objectives

The HEAO-B observatory will be launched in late 1978 for a one-year mission to analyze individual X-ray objects and extended sources in detail using a high precision X-ray telescope. The energy range of the telescope is 0.1 keV to 4 keV. Four interchangeable instruments are at the focal plane; a high resolution imaging instrument, an imaging proportional counter, a focal plane crystal spectrometer, and a solid state spectrometer. A monitor proportional counter will collect data independently of the telescope. The HEAO-C observatory is a scanning mission and will be launched in 1979 for six months operation. It will contain two cosmic ray experiments and a gamma ray spectrometer.

Dailey, C. C.↗

Apollo Telescope Mount experiments technology

The Skylab Apollo Telescope Mount (ATM) experiments, consisting of a white light coronagraph, four ultraviolet instruments, two X-ray telescopes and two hydrogen-alpha telescopes, observed the sun daily for nine solar rotations. The ATM instruments were individually larger, more complex, and provided better spatial resolution than previous solar satellite instruments. An additional major advantage of the telescope complex was its ability to simultaneously collect multispectral data of specific solar phenomena. To maximize the scientific benefits of the orbiting observatory, a coordinated observing program involving worldwide ground-based observatories was conducted. A description of the Skylab, the ATM, and the ATM experiments is given, and the daily process of flight planning and execution is described.

Keathley, W. C.↗

Apollo Telescope Mount experiments technology

The Skylab Apollo Telescope Mount (ATM) experiments, consisting of a white light coronagraph, four ultraviolet instruments, two X-ray telescopes and two hydrogen-alpha telescopes, observed the sun daily for nine solar rotations. The results have only begun to be evaluated, but is is already apparent that many theories of solar physics will undergo significant revisions as results are further developed. The ATM instruments were individually larger, more complex, and provided better spatial resolution than previous solar satellite instruments. An additional major advantage of the telescope complex was its ability to simultaneously collect multispectral data for specific experiments. A description of the Skylab, the ATM and the ATM experiments will be given. The daily process of flight planning and execution will be described. Examples of scientific data and some preliminary findings will be presented.

Keathley, W. C.↗

Phosphate Textural Diversity in CI Chondrites and C-Type Asteroids

Introduction: Apatite, Ca 5 (PO 4 ) 3 (CL/F/OH-), is a ubiquitous phosphate found throughout the solar system, including the most primitive solids, CI-chondrites [1,2] and related samples of carbonaceous asteroids Ryugu [3] and Bennu [4], returned by JAXA’s Hayabusa2 and NASA’s OSIRIS-REx missions, respectively. Apatite in these primitive solids is found as individual grains or mineral clusters and has been inferred to form from the hydrothermal sequence during cooling of their respective parent body or bodies. To better understand the formation history and reworking of these early phosphates we have undertaken a highly coordinated study of phosphate microstructures, geochemistry and U/Pb geochronology from a suite of CI meteorites and carbonaceous asteroid samples. These data have identified novel phosphate microstructures and complex relationships across a suite of apatite grains from the early solar system, indicating multiple episodes of growth and modification on the CI parent body(ies). Methods: Samples of CI chondrites, Alais, Ivuna, Orgueil, Oued Chebeika 002, Yamato (Y) 82162, Y980115, Y980134, and two chips of Hayabusa2 Ryugu particles (A0262 and C0263) have been acquired for analysis. The bulk texture of the samples were first scanned by X-ray Computed Tomography (XCT) using the Nikon XT H 320 within the XFACT facility at NASA JSC or the Xradia 620 Versa at the UTCT facility. Based on the identification of petrofabrics or features of interest from the XCT data, samples were chipped, oriented, potted in epoxy and thick sections were prepared. After anhydrously polishing the samples with silicon carbide and dry diamond powder down to 1 µm, the samples were ion polished using a Hitachi ArBlade. Energy dispersive Xray spectrometry (EDS) maps were collected to ID phosphates of interest using a JEOL 7900F SEM. The internal microstructures of identified phosphates were then mapped by electron backscatter diffraction (EBSD) using the JEOL 7900F. Based on the EDS and EBSD data, domains of interest were targeted for quantitative chemical analyses using a JEOL 8530 EPMA. Subsequently, in situ U-Pb and 207 Pb/ 206 Pb ages will be collected using a Cameca ims1290 secondary ion mass spectrometer at UCLA across a range of microstructures. Results: Apatite grains are ubiquitous throughout the CI chondrites and carbonaceous asteroid materials, found as individual grains, disseminated clusters or grain aggregates. Apatite grains are associated with serpentine, magnet-ite, and/or carbonate. Of particular interest, we have identified individual and aggregate polycrystalline grains ex-hibiting an internal ‘honeycomb’ texture (Fig. 1). Some of these grains appear overprinted by subsequent alteration while others remain unaltered. Apatite halogen sites are dominated by the missing component, assumed to be OH, and F, comparable to published values from Bennu, Ryugu and CM-chondrites [3-5]. However, the Yamato CI-like meteorites show a broader range of Cl values, and one grain from Alais is dominated by CL. Summary: Apatite growth features indicate a protracted and complex growth history, consistent with precipitation from an evolving fluid system. The ‘honeycomb’ texture identified in some CI meteorites is, to the best of our knowledge, the first report of such a microstructure in meteoritic phosphate. The microtextures and zoning will guide subsequent age analyses, to better constrain the formation and reworking of phosphate in CI(-like) materials. Acknowledgments: We thank the National Institute of Polar Research, Japan for samples of Y82162, 980115 and 980134 meteorites, ASU’s Buseck Center for Meteorite Studies for samples of Ivuna and Alais meteorites, and JAXA curation for chips of Ryugu material. This work was funded by NASA ROSES LARS grant 24-LARS24-0014. References: [1] Morlok et al., 2016, GCA 70:5371-5394. [2] Alfin g et al., 2019, Geochemistry 79:125532. [3] Nakamura et al. (2022) Science 379:1-15. [4] Seifert et al. (2026) MAPS 61:504-521. [5] Piralla et al. (2021) MAPS 56:809-828.

CI chondrites↗

Atmospheric, Non-Combusting Droplet Sizing and Spray Imaging Results From a Non-Proprietary Aero Gas Turbine Engine Pressure Swirl Atomizer using Shadowgraphy and Planar Laser Scatter

Members from industry and federal agencies of the United States have developed a collaborating group focused on improving the understanding of the atomization processes common to gas turbine engines. The group is aimed on providing high quality data using x-ray diagnostics in the internal geometry and the near-field dense spray as well as optical diagnostics in the visible spectrum, downstream of the nozzle. This paper reports results from one of the two non-proprietary injectors designs from the group: the primary-secondary injector. In particular, we characterize the spray from only the primary, pressure-swirl atomizing circuit using water through the nozzle. We observed Sauter mean diameter decreased with increased water pressure drop across the nozzle. SMD was also collected at three axial distances and showed decreased size with distance from the nozzle. Planar laser sheet droplet scattering provided qualitative assessment of the spray. Higher water pressure drops provided better atomization than lower pressure drops. The addition of swirling air flow through the injector alleviates and improves the atomization quality, particularly at the lower water pressure drops.

optical diagnostics↗

Evaluation of zirconia, thoria and zirconium diboride for advanced resistojet use

A literature survey was conducted to collect material properties data on all advanced high temperature materials. Three of these, Y2O3-stabilized ZrO2, ThO2, and ZrB2 with additives of C and SiC were selected for further study. Stabilized ZrO2 and ThO2 were found to have higher temperature oxidation resistance than any metal and great potential for use in advanced biowaste resistojets. ZrO2 has a lower electrical resistivity and sublimation and a higher creep endurance strength. ZrO2 and ThO2 tubular heat exchangers, electrically heated indirectly, were evaluated in short tests to about 1900 K in flowing CO2. ZrO2 was subjected to N2, H2, H2O and vacuum as well. X-ray diffraction and fluorescence analyses were made. The metal-to-ceramic seal technology for ZrO2 and ThO2 was developed using chemical vapor deposition of tantalum for metallizing and 82 Au - 18 Ni filler braze.

Page, R. J.↗