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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

A methodology for corrosion testing ODS steels in liquid tin under reactor conditions in HFIR

Liquid metal–based divertor concepts have promising attributes for application in fusion reactors. Liquid tin is being considered as one of those liquid metals due to its excellent thermophysical properties. However, tin is extremely corrosive to steels at elevated temperatures, and the coupled effects of corrosion with neutron irradiation for application in fusion reactors have not been quantified. Researchers at Oak Ridge National Laboratory (ORNL) have designed and irradiated a series of capsules in the High Flux Isotope Reactor (HFIR) to help address gaps in the literature with respect to coupled corrosion and neutron irradiation effects. The capsules are filled with solid tin designed to melt due to the gamma heating in HFIR and allow interaction with the specimens. The capsules contain a SiC thermometer for post-irradiation temperature verification. Five capsules were irradiated in HFIR for 10.5 days, accumulating 0.93 dpa in the FeCrAl specimens. Post-irradiation temperature verification was performed on the SiC thermometers, and temperatures were observed to be higher than what was expected from thermal models. An explanation for the model underprediction is given herein. In conclusion, the capsules described within this article are the first to irradiate liquid metal within the HFIR flux trap and demonstrated the safety basis for continued liquid coolant studies in HFIR.

FeCrAl↗

Voltage-temperature charge verification testing of 34 ampere-hour nickel-cadmium cells

This testing was designed to evaluate various voltage-temperature (V-T) charge curves for use in low-Earth-orbit (LEO) applications of nickel-cadmium battery cells. The trends established relating V-T level to utilizable capacity were unexpected. The trends toward lower capacity at higher V-T levels was predominant in this testing. This effect was a function of the V-T level, the temperature, and the cell history. This effect was attributed to changes occurring in the positive plate. The results imply that for some applications, the use of even lower V-T levels may be warranted. The need to limit overcharge, especially in the early phases of missions, is underlined by this test program.

Timmerman, P. J.↗

Shale gas: Geochemical and physical constraints on genesis, storage, and producibility

Our research project on shale gas included two tasks: (1) Testing of different shales’ ability to geocatalytically generate natural gas at low temperatures; verification of geocatalytic methanogenesis would potentially render shale gas a quasi-renewable resource, and (2) quantification and characterization of porosity and permeability in organic-rich rocks with implication for producibility. Adequate porosity is required for geological storage of shale gas. At the same time, pore connectivity is essential for gas producibility.

03 NATURAL GAS↗

A Method for Characterizing PMR-15 Resin

Quantitative analysis technique based on reverse-phase, highperformance liquid chromatography (HPLC) and paired-ion chromatography (PIC) developed for PMR-15 resins. In reverse-phase HPLC experiment, polar solvent containing material to be analyzed passed through column packed with nonpolar substrate. Composition of PMR-15 Resin of 50 weight percent changes as resin ages at room temperature. Verification of proper resin formulation and analysis of changes in resin composition during storage important to manufacturers of PMR-15 polymer matrix composite parts. Technique especially suitable for commercial use by manufacturers of high-performance composite components.

Roberts, G. D.↗

Wide-field Infrared Survey Telescope (WFIRST): Composite Structure Verification for Operational Temperatures

The Wide-Field Infrared Survey Telescope (WFIRST) mission is the next large astrophysics observatory for NASA after the James Webb Space Telescope and is the top priority mission from the 2010 National Academy of Sciences' decadal survey. The WFIRST Optical Telescope Assembly (OTA) includes inherited composite support structures that were originally designed and tested for room temperature operation; however, the WFIRST mission will require operation at colder temperatures to achieve sufficient sensitivity for the infrared wavelengths. We will present the results and conclusions of testing completed at the coupon and engineering model level to verify that the inherited composite structures will maintain mechanical integrity and performance over the required temperature range. The testing included: (1) characterization testing of constituent material coupons, (2) thermal cycling and static load testing of a representative aft metering structure (AMS) and forward metering structure (FMS), and (3) thermal cycling and dynamic testing of a representative secondary mirror assembly (SMA).

metering↗

T0TEM - T0 Test Evaluation Module Development and Verification

Transition temperature testing of ferritic steels evaluates the ductile to brittle transition temperature, where the behavior of the steel changes from controlled ductile tearing to uncontrollable brittle fracture. This testing is governed by ASTM (American Society of Testing and Materials) E1921 standard. The calculations and plots required by this standard are iterative in nature and require significant effort to produce by standard hand calculations. In addition to analysis of a complete data set, intermediate analysis during testing is beneficial to determine optimal test temperatures. Given the exhaustive nature of calculating the transition temperature, being able to quickly update target temperatures is a significant benefit to not only the quality of tests, but the number of required tests as well. T0 Test Evaluation Module (T0TEM) v1.5 is a software application created under the Layered Pressure Vessel (LPV) certification effort. To reduce the analysis time of transition temperature test data sets producedfor this effort, T0TEM was created to calculate the E1921 Master Curve along with all required data and validity checks. By creating this program, hundreds of hours of analysis time were saved. In addition, the creation of a standard program provided a significant improvement in the consistency with which results were reported. T0TEM also calculates the results and plots required for the E1921 inhomogeneity annex to determine whether a material behaves in a homogenous manner. This program was created by Levi Shelton and Cameron Bosley at NASA, with input and review from the E1921 committee. The results generated by T0TEM were compared to the validation data sets provided by ASTM with good concurrence. ASTM committee members have reviewed and applied T0TEM to other data sets with satisfactory results. T0TEM was originally released to the NASA Software Repository and publicly via SourceForge in May of 2020. Version 1.5 was released in April of 2021 with minor functionality updates and additional statistical analysis methods.

Levi Shelton↗

Investigating Temperature Uniformity and Accuracy in PV Module Lamination: A Verification Study

This study investigates the temperature uniformity and accuracy of a photovoltaic (PV) module lamination process by addressing inconsistencies identified in 2017 data where irregular temperature changes were observed across setpoints. The 2017 data showed a notable drop in temperature upon bladder initiation, except for the 145 degrees Celsius profile. This inconsistency indicated potential inaccuracies in manual data recording methods. To address this concern, a verification experiment was conducted to evaluate temperature uniformity across the 2014 Bent River SPL2828 laminator platen and within test samples. Thermocouples, paired with Omega data acquisition software, were deployed to measure temperatures at multiple platen locations and within test samples. The experiment compared lamination temperatures of polyethylene-co-vinyl acetate (EVA) encapsulant when paired with solite glass or TPE backsheets. The methodology included verifying temperature uniformity directly on the platen and by using a large glass/EVA/glass sample using multiple thermocouples. Smaller samples were built with glass/EVA/glass and glass/EVA/backsheet configurations with one centered thermocouple to verify and compare sample temperatures. This verification aims to refine lamination temperature profiles, enhance data accuracy and provide insights into optimal process control for uniform module lamination. Ensuring consistent and uniform lamination may improve the accuracy and reliability of research outcomes.

14 SOLAR ENERGY↗

Challenges and opportunities in verification and validation of low temperature plasma simulations and experiments

This paper describes the verification and validation (V&V) framework developed for the stochastic Particle-in-Cell, Direct Simulation Monte Carlo code Aleph. An ideal framework for V&V from the viewpoint of the authors is described where a physics problem is defined, and relevant physics models and parameters to the defined problem are assessed and captured in a Phenomena Identification and Ranking Table (PIRT). Furthermore, numerous V&V examples guided by the PIRT for a simple gas discharge are shown to demonstrate the V&V process applied to a real-world simulation tool with the overall goal to demonstrably increase the confidence in the results for the simulation tool and its predictive capability. Although many examples are provided here to demonstrate elements of the framework, the primary goal of this work is to introduce this framework and not to provide a fully complete implementation, which would be a much longer document. Comparisons and contrasts are made to more usual approaches to V&V, and techniques new to the low-temperature plasma community are introduced. Specific challenges relating to the sufficiency of available data (e.g., cross sections), the limits of ad hoc validation approaches, the additional difficulty of utilizing a stochastic simulation tool, and the extreme cost of formal validation are discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Development and Performance Verification of Fiber Optic Temperature Sensors in High Temperature Engine Environments

A High Temperature Fiber Optic Sensor (HTFOS) has been developed at NASA Glenn Research Center for aircraft engine applications. After fabrication and preliminary in-house performance evaluation, the HTFOS was tested in an engine environment at NASA Armstrong Flight Research Center. The engine tests enabled the performance of the HTFOS in real engine environments to be evaluated along with the ability of the sensor to respond to changes in the engine's operating condition. Data were collected prior, during, and after each test in order to observe the change in temperature from ambient to each of the various test point levels. An adequate amount of data was collected and analyzed to satisfy the research team that HTFOS operates properly while the engine was running. Temperature measurements made by HTFOS while the engine was running agreed with those anticipated.

Adamovsky, Grigory↗

High temperature furnace modeling and performance verifications

Analytical, numerical and experimental studies were performed on two classes of high temperature materials processing furnaces. The research concentrates on a commercially available high temperature furnace using zirconia as the heating element and an arc furnace based on a ST International tube welder. The zirconia furnace was delivered and work is progressing on schedule. The work on the arc furnace was initially stalled due to the unavailability of the NASA prototype, which is actively being tested aboard the KC-135 experimental aircraft. A proposal was written and funded to purchase an additional arc welder to alleviate this problem. The ST International weld head and power supply were received and testing will begin in early November. The first 6 months of the grant are covered.

Smith, James E., Jr.↗

High temperature furnace modeling and performance verifications

Analytical, numerical, and experimental studies were performed on two classes of high temperature materials processing sources for their potential use as directional solidification furnaces. The research concentrated on a commercially available high temperature furnace using a zirconia ceramic tube as the heating element and an Arc Furnace based on a tube welder. The first objective was to assemble the zirconia furnace and construct parts needed to successfully perform experiments. The 2nd objective was to evaluate the zirconia furnace performance as a directional solidification furnace element. The 3rd objective was to establish a data base on materials used in the furnace construction, with particular emphasis on emissivities, transmissivities, and absorptivities as functions of wavelength and temperature. A 1-D and 2-D spectral radiation heat transfer model was developed for comparison with standard modeling techniques, and were used to predict wall and crucible temperatures. The 4th objective addressed the development of a SINDA model for the Arc Furnace and was used to design sample holders and to estimate cooling media temperatures for the steady state operation of the furnace. And, the 5th objective addressed the initial performance evaluation of the Arc Furnace and associated equipment for directional solidification. Results of these objectives are presented.

Smith, James E., Jr.↗

METCAN updates for high temperature composite behavior: Simulation/verification

The continued verification (comparisons with experimental data) of the METCAN (Metal Matrix Composite Analyzer) computer code is updated. Verification includes comparisons at room and high temperatures for two composites, SiC/Ti-15-3 and SiC/Ti-6-4. Specifically, verification of the SiC/Ti-15-3 composite includes comparisons of strength, modulus, and Poisson's ratio as well as stress-strain curves for four laminates at room temperature. High temperature verification includes comparisons of strength and stress-strain curves for two laminates. Verification of SiC/Ti-6-4 is for a transverse room temperature stress-strain curve and comparisons for transverse strength at three temperatures. Results of the verification indicates that METCAN can be used with confidence to simulate the high temperature nonlinear behavior of metal matrix composites.

Lee, H.-J.↗

METCAN updates for high temperature composite behavior - Simulation/verification

The continued verification (comparisons with experimental data) of the METCAN (Metal Matrix Composite Analyzer) computer code is updated. Verification includes comparisons at room and high temperatures for two composites, SiC/Ti-15-3 and SiC/Ti-6-4. Specifically, verification of the SiC/Ti-15-3 composite includes comparisons of strength, modulus, and Poisson's ratio as well as stress-strain curves for four laminates at room temperatures. High temperature verification includes comparisons of strength and stress-strain curves for two laminates. Verification of SiC/Ti-6-4 is for a transverse room temperature stress-strain curve and comparisons for transverse strength at three temperatures. Results of the verification indicates that METCAN can be used with confidence to simulate the high temperature nonlinear behavior of metal matrix composites.

Lee, H.-J.↗

International Space Station Temperature and Humidity Control Subsystem Verification for Node 1

The International Space Station (ISS) Node 1 Environmental Control and Life Support (ECLS) System is comprised of five subsystems: Atmosphere Control and Supply (ACS), Atmosphere Revitalization (AR), Fire Detection and Suppression (FDS), Temperature and Humidity Control (THC), and Water Recovery and Management (WRM). This paper provides a summary of the nominal operation of the Node 1 THC subsystem design. The paper will also provide a discussion of the detailed Element Verification methodologies for nominal operation of the Node 1 THC subsystem operations utilized during the Qualification phase.

Williams, David E.↗

High temperature furnace modeling and performance verifications

A two dimensional conduction/radiation problem for an alumina crucible in a zirconia heater/muffle tube enclosing a liquid iron sample was solved numerically. Variations in the crucible wall thickness were numerically examined. The results showed that the temperature profiles within the liquid iron sample were significantly affected by the crucible wall thicknesses. New zirconia heating elements are under development that will permit continued experimental investigations of the zirconia furnace. These elements have been designed to work with the existing furnace and have been shown to have longer lifetimes than commercially available zirconia heating elements. The first element has been constructed and tested successfully.

Smith, James E., Jr.↗

Proportional and Integral Thermal Control System for Large Scale Heating Tests

The National Aeronautics and Space Administration Armstrong Flight Research Center (Edwards, California) Flight Loads Laboratory is a unique national laboratory that supports thermal, mechanical, thermal/mechanical, and structural dynamics research and testing. A Proportional Integral thermal control system was designed and implemented to support thermal tests. A thermal control algorithm supporting a quartz lamp heater was developed based on the Proportional Integral control concept and a linearized heating process. The thermal control equations were derived and expressed in terms of power levels, integral gain, proportional gain, and differences between thermal setpoints and skin temperatures. Besides the derived equations, user's predefined thermal test information generated in the form of thermal maps was used to implement the thermal control system capabilities. Graphite heater closed-loop thermal control and graphite heater open-loop power level were added later to fulfill the demand for higher temperature tests. Verification and validation tests were performed to ensure that the thermal control system requirements were achieved. This thermal control system has successfully supported many milestone thermal and thermal/mechanical tests for almost a decade with temperatures ranging from 50 F to 3000 F and temperature rise rates from -10 F/s to 70 F/s for a variety of test articles having unique thermal profiles and test setups.

Thermal Control System↗

Modified Laser Flash Method for Thermal Properties Measurements and the Influence of Heat Convection

The study examined the effect of natural convection in applying the modified laser flash method to measure thermal properties of semiconductor melts. Common laser flash method uses a laser pulse to heat one side of a thin circular sample and measures the temperature response of the other side. Thermal diffusivity can be calculations based on a heat conduction analysis. For semiconductor melt, the sample is contained in a specially designed quartz cell with optical windows on both sides. When laser heats the vertical melt surface, the resulting natural convection can introduce errors in calculation based on heat conduction model alone. The effect of natural convection was studied by CFD simulations with experimental verification by temperature measurement. The CFD results indicated that natural convection would decrease the time needed for the rear side to reach its peak temperature, and also decrease the peak temperature slightly in our experimental configuration. Using the experimental data, the calculation using only heat conduction model resulted in a thermal diffusivity value is about 7.7% lower than that from the model with natural convection. Specific heat capacity was about the same, and the difference is within 1.6%, regardless of heat transfer models.

Lin, Bochuan↗