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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2011

Developing Guidelines for Assessing Visual Analytics Environments

Visual analytic systems can be evaluated from a user perspective with quantitative metrics (i.e., time to complete the analysis or the accuracy of the solution found). However, qualitative measures are also useful in a user assessment. These include such measures as the utility of the interactive visualizations in the analysis process and the user's assessment of the efficiency of the analytic process. Quantitative measures can be found if data sets with embedded ground truth are used for analysis. Qualitative measures are more elusive. In this paper we report on an experiment with professional analysts who ranked five of submissions to the VAST 2009 Challenge and provided the rationale for their rankings. Their comments were used in conjunction with a meta-analysis of the 2009 VAST Challenge reviews to produce a set of guidelines for visual analytic systems. As visual analytic software is expected to eventually help in all aspects of analysis, we expect to see future systems provide more help with generating the final report. Hence, researchers also need to have an understanding of what makes a good analytic product. Therefore we asked the analysts to rank the situational assessments of four grand challenge entries and to provide comments on those assessments. We used these comments to produce guidelines for researchers to use in evaluating their analytic reports.

99 GENERAL AND MISCELLANEOUS↗
DOE OSTI2022

Optical variability of quasars with 20-yr photometric light curves

ABSTRACT We study the optical gri photometric variability of a sample of 190 quasars within the SDSS Stripe 82 region that have long-term photometric coverage during ∼1998−2020 with SDSS, PanSTARRS-1, the Dark Energy Survey, and dedicated follow-up monitoring with Blanco 4m/DECam. With on average ∼200 nightly epochs per quasar per filter band, we improve the parameter constraints from a Damped Random Walk (DRW) model fit to the light curves over previous studies with 10–15 yr baselines and ≲ 100 epochs. We find that the average damping time-scale τDRW continues to rise with increased baseline, reaching a median value of ∼750 d (g band) in the rest frame of these quasars using the 20-yr light curves. Some quasars may have gradual, long-term trends in their light curves, suggesting that either the DRW fit requires very long baselines to converge, or that the underlying variability is more complex than a single DRW process for these quasars. Using a subset of quasars with better-constrained τDRW (less than 20 per cent of the baseline), we confirm a weak wavelength dependence of τDRW∝λ0.51 ± 0.20. We further quantify optical variability of these quasars over days to decades time-scales using structure function (SF) and power spectrum density (PSD) analyses. The SF and PSD measurements qualitatively confirm the measured (hundreds of days) damping time-scales from the DRW fits. However, the ensemble PSD is steeper than that of a DRW on time-scales less than ∼ a month for these luminous quasars, and this second break point correlates with the longer DRW damping time-scale.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

Interplay between Terminal and Bridging Diiron Hydrides in Neutral and Oxidized States

This study describes the structural, spectroscopic, and electrochemical properties of electronically unsymmetrical diiron hydrides. The terminal hydride Cp*Fe(pdt)Fe(dppe)(CO)H ([1(t-H)]0, Cp*– = Me5C5 –, pdt2– = CH2(CH2S–)2, dppe = Ph2PC2H4PPh2) was prepared by hydride reduction of [Cp*Fe(pdt)Fe(dppe)(CO)(NCMe)]+. As established by X-ray crystallography, [1(t- H)]0 features a terminal hydride ligand. Unlike previous examples of terminal diiron hydrides, [1(t-H)]0 does not isomerize to the bridging hydride [1(µ-H)]0. Oxidation of [1(t-H)]0 gives [1(t- H)]+, which was also characterized crystallographically as its BF4 – salt. Density functional theory (DFT) calculations indicate that [1(t-H)]+ is best described as containing an Cp*Fe(III) center. In solution, [1(t-H)]+ isomerizes to [1(µ-H)]+ as anticipated by DFT. Reduction of [1(µ- H)]+ by Cp2Co affords the diferrous bridging hydride [1(µ-H)]0. Electrochemical measurements and DFT calculations indicate that the couples [1(t-H)]+/0 and [1(µ-H)]+/0 differ by 210 mV. Qualitative measurements indicate that [1(t-H)]0 and [1(µ-H)]0 are close in free energy. Protonation of [1(t-H)]0 in MeCN solution affords H2 even with weak acids via hydride transfer.

Yu, Xin↗
DOE OSTI2019

Characterizing Speed and Scale of Cryptocurrency Discussion Spread on Reddit

Cryptocurrencies are a novel and disruptive technology that has prompted a new approach to how currencies work in the modern economy. As such, online discussions related to cryptocurrencies often go beyond posts about the technology and underlying architecture of the various coins, to subjective speculations of price fluctuations and predictions. Furthermore, online discussions, potentially driven by foreign adversaries, criminals or hackers, can have a significant impact on our economy and national security if spread at scale. This paper is the first to qualitatively measure and contrast discussion growth about three popular cryptocurrencies with key distinctions in motivation, usage, and implementation – Bitcoin, Ethereum, and Monero on Reddit. More specifically, we measure how discussions relevant to these coins spread in online social environments – how deep and how wide they go, how long they last, how many people they reach, etc. More importantly, we compare user behavior patterns between the focused community of the official coin subreddits and the general community across Reddit as a whole. Our Reddit sample covers three years of data between 2015 and 2018 and includes a time period of a record high Bitcoin price rise. Our results demonstrate that while the largest discussions on Reddit are focused on Bitcoin, posts about Monero (a cryptocurrency often used by criminals for illegal transactions on the Dark Web) start discussions that are typically longer and wider. Bitcoin posts trigger subsequent discussion more immediately but Monero posts are more likely to trigger a longer lasting discussion. We find that moderately subjective posts across all three coins trigger larger, longer, and more viral discussion cascades within both focused and general communities on Reddit. Our analysis aims to bring the awareness to online discussion spread relevant to cryptocurrencies in addition to informing models for forecasting cryptocurrency price that rely on discussions in social media.

information spread, social network analysis, reddi↗
DOE OSTI2018

Non-Destructive Characterization of Subsurface Residual Stress Fields and Correlation with Microstructural Conditions in a Shot-Peened Inconel Component

Shot-peening is an important surface treatment used in a preventative way to guard against fatigue failures. The residual stress state imparted by shot-peening deters the formation and propagation of surface cracks. In this paper, we describe the measurement of residual stresses in an Inconel, IN100, sample using lattice strains measured using High Energy X-ray Diffraction (HEXD) and a Bi-Scale Optimization Method (BSOM). HEXD enabled rapid, non-destructive lattice strain measurements over a large region of the sample. Subsurface strains were obtained using a conical slit setup. The BSOM utilizes a macroscale representation of the sample and a spherical harmonic-based crystal scale representation of crystal orientation space at each experimental point (diffraction volume). A roughly biaxial stress state was predicted with a von Mises equivalent stress between 300 MPa and 400 MPa near the surface. The layer of material with high residual stress induced by shot-peening was found to be approximately 1 mm thick. Diffraction peak width, EBSD, and microhardness measurements were also made on the same sample, which rendered more qualitative measures of the plasticity-related effects of the shot-peening induced residual stress field. All of these measurements show a dimishing shot-peening plasticity with the increasing depth.

42 ENGINEERING↗
DOE OSTI2015

SU-E-I-67: Arachnoid Cysts: The Role of the BLADE Technique

Purpose: The purpose of this study is first to show the extent by which BLADE sequences can reduce all the image artifacts and second to verify that the usefulness of this technique in certain pathological conditions is significant. Methods: In this study, fourteen consecutive patients (5 females, 9 males), who routinely underwent MRI brain examination, between 2010–2014, were selected. The applied routine protocols for brain MR examination included the following sequences: 1) T2-W FLAIR axial; 2) T2-W TSE axial; 3) T2*-W axial, 4) T1-W TSE sagittal; 5) DWI-W axial; 6) T1-W TSE axial; 7) T1-W TSE axial+contrast. In cases of cystic tumors, the T2-W FLAIR BLADE sequence was added to the protocol. All the images were evaluated independently at two separate settings with 3 weeks interval by two radiologists. The radiologists also evaluated the presence of image artifacts (motion, flow, chemical shift, Gibbs ringing). To evaluate the size of the cyst, the two radiologists compared the two techniques (conventional and BLADE) by assessing the extent of the divergence in the measurements of the cysts. Results: Regarding the extent of the cyst size, BLADE measurements were found to be more reliable than the conventional ones with the differences being statistically significant (p<0.01). The qualitative measurements indicated that the T2 FLAIR BLADE sequences were superior to the conventional T2 FLAIR with statistically significant differences (p<0.001) in the following characteristics: 1) overall image quality, 2) CSF nulling; 3) contrast at the pathology and its surrounding; 4) limits of the pathology; 5) motion artifacts; 6) flow artifacts; 7) chemical shift artifacts and 8) Gibbs ringing artifacts. Conclusion: BLADE sequence was found to decrease both flow artifacts in the temporal lobes and motion artifacts from the orbits and it is proposed for clinical use.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2019

Two-color pyrometry system to eliminate optical errors for spatially resolved measurements in flames

Two color (2C) pyrometry has long been used to measure flame temperature and soot concentration from radiative emission in flames. While 2C pyrometry is not an absolute measurement in non-axisymmetric flames (such as diesel spray combustion) it is a desirable diagnostic for semi-quantitative or qualitative measurements since it requires minimal optical access and can utilize high-speed imaging to attain exceptional temporal and spatial resolution. In this work, an improved optical configuration of 2C pyrometry is presented that 1) eliminates optical errors inherent in other designs, and 2) uses off-the-shelf optics and a single camera . In particular, this work analyzes the impact of parallax and path length differences on the 2C pyrometry measurement and exemplifies how the present design eliminates associated errors by design rather than in post-processing. Finally, the theoretical range of measurements were generated a priori and overlaid with experimental data to illustrate the dynamic range over which 2C pyrometry can determine the soot concentration and temperature in theory and in practice.

47 OTHER INSTRUMENTATION↗
DOE OSTI2015

Detecting carbon uptake and cellular allocation by individual algae in multispecies assemblages: Tracking carbon into single algal cells

Algal species vary in carbon (C) need and uptake rates. Understanding differences in C uptake and cellular allocation among species from natural communities will bring new insight into many ecosystem process questions including how species changes will alter energy availability and C sequestration in aquatic ecosystems. A major limitation of current methods that measure algal C incorporation is the inability to separate the response of individual species from mixed-species assemblages. I used Fourier-transform infrared microspectroscopy to qualitatively measure inorganic 13 C isotope incorporation into individual algal cells in single species, two species, and natural phytoplankton assemblages. Lateral shifts in spectral peaks from 13 C treatments were observed in all species. Comparison of peaks associated with carbohydrates, proteins, and lipids allowed for the detection of which individuals took in C, and which macromolecules the C was used to make. For example, shifts in Spirogyra spectral peaks showed substantial C incorporation in carbohydrates. Further, shifts in peaks at 1160 cm -1 , 1108 cm -1 , 1080 cm -1 , 1048 cm -1 , and 1030 cm -1 suggested C was being allocated into cellulose. The natural phytoplankton assemblage demonstrated how C could be tracked into co-occurring species. A diatom had large shifts in protein and carbohydrate peaks, while a green alga and euglenoid had only a few shifts in protein related peaks. Fourier-transform infrared microspectroscopy is an established, label free method for measuring the chemical composition of algal cells. However, adding a label such as 13 C isotope can greatly expand the technique's capabilities by qualitatively tracking C movement between inorganic and organic states within single cells.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2021

Ultrasonic Characterization of Ethylene Vinyl Acetate (EVA) Crosslinking for Quality Assurance and Lamination Process Control (US-Xlink)

Module makers strive to cut lamination processing times to enhance production throughput and reduce costs. If overdone, this might lead to poor EVA quality due to incomplete EVA crosslinking and a large concentration of potentially harmful reactants. Those deficiencies are frequently missed during production quality testing as initially their impact on power output is small. Additionally, the crosslinking agent is frequently inhomogeneously dispersed across the EVA foils such that local destructive characterization procedures such as differential scanning calorimetry (DSC), Soxhlet extraction, swelling methods, or mechanical tests provide only a limited amount of information. However, these defects and inhomogeneities can become considerably more important during field operation, dramatically reducing long-term power yield, and increasing LCOE. Examples of typical long-term module degradation modes relating to poor lamination process conditions include cell breakage, corrosion of the metallization, delamination, and local quality deficiencies. To provide reliable material characterization in a manufacturing setting, we devised a non-destructive technology that uses ultrasound to evaluate the quality of interface adhesion and the degree of crosslinking. As a calibration reference, DSC measurements were employed. Although the potential of ultrasonic approaches for this purpose has already been noted, those previous methods were generally limited to local qualitative measurements. Furthermore, variations in EVA thickness and temperature had a substantial impact on them. The solution we propose solves these limitations by employing ultrasonic absorption rather than relying solely on sound velocity data.

14 SOLAR ENERGY↗
DOE OSTI2017

Graded approach for assessing digital system failure susceptibilities - 305

Owner/operators of nuclear plants must be able to identify and assess susceptibilities to digital system failures and unintended behaviors that could lead to plant system malfunctions, including common-cause failures (CCFs) of multiple controlled components that may impact overall plant safety. Nuclear plant designers and regulators often assess and manage potential failure modes by assuming the failure occurs and showing by analysis that the results are acceptable. In 2016 EPRI published a guideline on Methods for Assuring Safety and Dependability when Applying Digital Instrumentation and Control Systems (EPRI 3002005326), which takes a more holistic approach that considers digital system failure modes from the perspective of their impact on plant risk and includes a graded approach based on safety significance. This paper describes that graded approach. The methodology in EPRI 3002005326 systematically identifies potential I and C vulnerabilities that could lead to significant malfunctions of controlled components and systems, including common-cause failures (CCF), and discusses in detail methods to protect against them. It considers both preventive measures that reduce the likelihood of failures, and plant systems and features that mitigate the effects of component failures and misbehaviors. Coping analysis is then performed as appropriate to provide additional assurance of protection. The safety significance based graded approach is an important feature in that it can help users focus attention on overall plant safety, including potentially risk-significant scenarios that might not be considered in traditional safety analyses. The purpose is to help the user ensure that modifications to the I and C that could potentially be safety significant are treated appropriately and at the same time not waste valuable resources on excessive protection against changes that have little or no impact on safety. The graded approach allows the design engineer to tailor the rigor of the preventive, limiting, and mitigative measures commensurately with the effects the I and C modification has on overall plant safety. The graded approach focuses on safety significance impact, which is effectively a qualitative measure of the potential change in safety (or risk) caused by a proposed I and C modification, as compared to the I and C that is being replaced. Safety significance impact should not be confused with importance to safety or risk significance. It is possible that an upgrade to safety-related and/or risk-significant I and C systems may have little or no safety significant impact and vice versa. The approach considers three factors that influence the impact on safety significance of a proposed I and C modification: context, likelihood of failure, and consequences of failure. The most significant of the three factors is context - what the I and C is connected to, both directly and indirectly, including its potential effects on plant systems that respond to transients or accidents. The graded approach is particularly helpful in assessing potential CCFs resulting from digital I and C failures, and shows why the most problematic CCFs will be those that can affect multiple plant systems. (authors)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

Blade Designs For Improved Multi-Phase Performance In sCO 2 Compressors; Part II - Optical Diagnostics In sCO 2 And Experimental Evaluation With Particle Image Velocimetry

This paper presents the second part of a study in which the leading-edge and suction surface of a compressor blade was modified to delay onset of phase change for sCO 2 compressors operating near the critical point. Using a first-of-its-kind apparatus for the measurement of sCO 2 flow fields, Particle Image Velocimetry (PIV) is used for local flow field measurements of two compressor blade geometries: the modified “biased-wedge,” and a conventional constant thickness blade. Utilizing the developed hardware, the feasibility of a simple, laser-based diagnostic for qualitatively measuring liquid phase regions, is also presented. The design of the optical diagnostics rig, a discussion of numerous challenges, and necessary considerations involved in performing optical-based measurements like PIV, in sCO 2 , are discussed. Velocity field measurements for the modified compressor profile show a much lower suction peak compared to a conventional blade. Furthermore, these results validate numerical results at the tested conditions, where the suction side profile of the biased wedge works to minimize the local pressure gradient.

14 SOLAR ENERGY↗
DOE OSTI2021

A Method for Assessing Effectiveness and Technical Capabilities Required for Integrated Deterrence (NSLP-Final Report-Draft2022)

The United States faces an ever-increasingly multi-polar security environment dominated by great power competition with China and a lingering Russian threat as well as from would-be regional hegemons led by ambitions from Iran and North Korea. Our adversaries are pursuing and expanding the strategic means by-which they have an asymmetric offset (e.g., cyber, space, and other modes below the level of armed conflict). To combat and deter against the widening range of hostile actions, the U.S. must have additional capabilities with-which to deter. All of which drives us towards a more thoughtful integrated approach to deterrence, attempting to best align deterrent tools with the adversary actions in order to maximize the credibility of our deterrent. Such an approach complicates our deterrence strategy and demands a methodology to assess whether the U.S. has the deterrent tools necessary to deter the adversarial actions most costly to the U.S. To address this complexity, we create a framework to comprehensively and systematically assess our deterrent tools as qualitatively measured against the adversarial actions we wish to deter. Deterrence is ultimately an operation in the cognitive domain and at the heart of the framework presented here is the fundamental deterrence calculus which we use as the defining measure of whether a tool will credibly deter a given action. We describe the eight levers of the deterrence calculus and distill these levers to four products that are used to qualitatively assess the overall effectiveness of deterrence tools against adversarial actions. Credibility is determined by two principal variables: the technical credibility of the deterrent tool, and the principle of proportionality. Technical credibility of realized deterrence products is assessed through development of key mission requirements and hardware (e.g., components) that will impose costs, deny benefits, or encourage restraint. The principle of proportionality qualitatively asserts that for a deterrent tool to be cognitively credible, the costs imposed against, or benefits denied by, an action are commensurate to the magnitude of costs received from the adversarial action. By basing this framework on these two fundamentals, it is possible to compare deterrent tools in a systematic approach across the broad spectrum of hostile actions.

42 ENGINEERING↗
DOE OSTI2012

Radiochromic film measurement of spatial uniformity for a laser generated x-ray environment

n existing x-ray source application (XRSA) test cassette was modified to hold multiple x-ray filter materials followed by two radiochromic film types (FWT-60 and HD-810 Gafchromic® film) to qualitatively characterize the spectral-spatial uniformity over the XRSA sample field of view. Multiple sets of film were examined and nominal set was determined. These initial, qualitative measurements suggest a low-energy regime (E < 3 keV) spatial anisotropy and spatial isotropy at higher energies (E > 3 keV).

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2019

Use of In Situ Acoustic Backscatter Systems to Characterize Spent Nuclear Fuel and its Separation in a Thickener - 19288

To aid in the transportation, dewatering and storage of radioactive UK legacy waste sludges at Sellafield Ltd., the application of an Acoustic Backscatter System (ABS) was investigated in this study, as a method for monitoring suspended solids concentration and consolidation of cohesive and aggregated sludges (that form the basis of many wastes at Sellafield). An ABS represents a particularly promising technology, as they can be used with minimal intrusion, to measure both particle size and concentration depending on prior system knowledge, through inversion of the return echo voltage response of pulse-echo signals in the MHz range. To assess the application for continuous, high concentration (∼30 % v/v) thickened wastes, an ABS was utilised to characterise a pseudo-steady state laboratory thickener over hours, using flocculated calcite as a representative test material. Measurements were taken both horizontally through a consolidated bed using a 1 MHz transducer and vertically downwards with a 2 MHz transducer to measure sediment concentration above the settled bed and track bed height via the interface reflection. Characterisation of flocculated aggregate diameters was initially determined to be ∼510 μm, using an in-line Focussed Beam Reflectance Measurement (FBRM) device. The submerged 2 MHz probe indicated that there were only limited changes to the dispersion concentration or size over time. Changes in settled bed density, due to increasing bed height and changes in the underflow flow rate, were qualitatively measured via differences to the acoustic signal attenuation over time. An initial increase in attenuation with bed height was observed as the bed densified due to local compression. Once an equilibrium bed height was reached, the acoustic attenuation remained fairly constant with time, although the bulk underflow density was reduced with the increase in underflow rate. The solids residence time in the bed, determined from a transitive volume-balance model, was found to be ∼3200 s for pseudo-steady state operation at a maintained bed height of ∼0.175 m. Results of the study highlight the potential the ABS as a remote process monitoring tool for both relatively dilute suspensions and concentrated thickened mineral sludges, with potential applications across waste processing sites at Sellafield. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2016

TH-AB-BRA-11: Using 3D Dosimeters for the Investigation of the Electron Return Effect (ERE) in MR-Guided Radiation Therapy: A Feasibility Study

Purpose: To demonstrate the capability of 3D radiochromic PRESAGE and Fricke-type dosimeters to measure the influence of magnetic fields on dose distribution, including the electron return effect (ERE), for MR-guided radiation therapy applications. Methods: Short cylindrical 3D dosimeters with PRESAGE and Fricke-type formulations were created in-house prior to irradiations in a 1.5T/7MV MR-linac. Each dosimeter was prepared with a concentric cylindrical air cavity with diameters of 1.5 cm and 2.5 cm, and the diameters of the dosimeters were 7.2 cm and 8.8 cm for PRESAGE and Fricke-type respectively. The dosimeters were irradiated within the bore of the MR-linac with the flat face of the dosimeters perpendicular to the magnetic field. Dosimeters were irradiated to approximately 9 Gy and 29 Gy to the center of dosimeters with a 15×15 cm{sup 2} field. The PRESAGE dosimeter was scanned using an optical-CT 2 hours post-irradiation; the Fricke-type dosimeter was immediately imaged with the MR component of the MR-linac post-irradiation. Results: Axial slices of the dose distributions show a clear demonstration of the dose enhancement due to the ERE above the cavity and the region of reduced dose below the cavity. The regions of increased and reduced dose are rotated with respect to the radiation beam axis due to the average directional change of the electrons. Measurements from line profiles show the dose enhanced up to ∼0.5 cm around the cavity by up to a factor of 1.3 and 1.4 for PRESAGE and Fricke-type dosimeters respectively. Conclusion: PRESAGE and Fricke-type dosimeters are able to qualitatively measure the ERE with good agreement with previously published simulation and 2D dosimetry demonstrations of the ERE. Further investigation of these 3D dosimeters as promising candidates for quality assurance of MR-guided radiation therapy systems is encouraged to assess changes in response and measurement accuracy due to the magnetic field.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2022

Diagnosing the pedestal magnetic field and magnetohydrodynamics radial structure with pedestal–scrape of layer electron cyclotron emission radiation inversion in H-mode plasma (invited)

Forward modeling is used to interpret inversion patterns of the pedestal–Scrape of Layer (SOL) Electron Cyclotron Emission (ECE) in DIII-D H-mode experiments. The modeling not only significantly improves the ECE data interpretation quality but also leads to the potential measurements of (1) the magnetic field strength |B| at the separatrix, (2) the pedestal |B| evolution during an inter-Edge Localized Mode (ELM) period, and (3) the pedestal Magnetohydrodynamics (MHD) radial structure. The ECE shine-through effect leads to three types of pedestal–SOL radiation inversions that are discussed in this paper. The first type of inversion is the non-monotonic T e,rad profile with respect to the major radius. Using the ECE frequency at the minimum T e,rad , the inversion can be applied to measure the magnetic field |B| at the separatrix and calibrate the mapping of the ECE channels with respect to the separatrix. The second type of inversion refers to the opposite phase between the radiation fluctuations δT e,rad at the pedestal and SOL. This δT e,rad phase inversion is sensitive to density and temperature fluctuations at the pedestal foot and, thus, can be used to qualitatively measure the MHD radial structure. The third type of inversion appears when the pedestal and SOL T e,rad evolve in an opposite trend, which can be used to infer the pedestal |B| field change during an inter-ELM period. Finally, the bandwidth effect on measuring δT e,rad due to pedestal MHD is also investigated in the radiation modeling.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗