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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2016

Identifying and discriminating phase transitions along decaying shocks with line imaging Doppler interferometric velocimetry and streaked optical pyrometry [Identify phase transition along decaying shocks with line imaging VISAR and streaked optical pyrometry]

Ultrafast line-imaging velocity interferometer system for any reflector and streaked optical pyrometry are now commonly used to obtain high precision equation of state and electronic transport data under dynamic compression at major high energy density science facilities. In this work, we describe a simple way to improve distinguishing phase transformation signatures from other signals when monitoring decaying shock waves. The line-imaging capability of these optical diagnostics offers additional supporting evidence to the assignment of particular anomalies—such as plateaus or reversals—to the occurrence of a phase transition along the Hugoniot. Finally, we illustrate the discussion with two example datasets collected during laser driven shock compression of quartz and stishovite.

47 OTHER INSTRUMENTATION↗
DOE OSTI2019

Dynamic absorption in optical pyrometry of hot spots in plastic-bonded triaminotrinitrobenzene [Optical Pyrometry of Shock-induced Hot Spots in Plastic-bonded Triaminotrinitrobenzene]

Herein we demonstrate a methodology for measuring optical pyrometry in environments which are disadvantageous for typical pyrometery applications by introducing additional fit parameters to account for absorption or emission which convolutes the thermal spectrum. Emission spectra from a plastic-bonded formulation of triaminotrinitrobenzene (TATB) shocked by 2-4 km s -1 impacts with Al flyer plates show significant deviations from graybody behavior. To extract reliable temperatures via optical pyrometry, we fit the spectra to a combination of a graybody and either a Gaussian absorption or emission spectrum. We found that the absorption needed to fit the data corresponds well with the known pressure-dependent absorption of TATB, and that the absorption model gives temperatures and emissivities in line with other explosives. By contrast, emission gives temperatures too low and emissivities that decrease as more material reacts. We conclude the nonthermal part of the spectrum is dominated by the absorption of unreacted TATB, and accurate pyrometry of TATB must use either our graybody plus absorption model or must limit the spectral range of observation to above 650 nm.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

Combined x-ray scattering, radiography, and velocity interferometry/streaked optical pyrometry measurements of warm dense carbon using a novel technique of shock-and-release

This work focused on a new application of the shock-and-release technique for equation of state (EOS) measurements. Warm dense matter states at near normal solid density and at temperatures close to 10 eV in diamond and graphite samples were created using a deep release from a laser-driven shock at the OMEGA laser facility. Independent temperature, density, and pressure measurements that do not depend on any theoretical models or simulations were obtained using imaging x-ray Thomson scattering, radiography, velocity interferometry, and streaked optical pyrometry. The experimental results were reproduced by the 2-D FLASH radiation hydrodynamics simulations finding a good agreement. The final EOS measurement was then compared with widely used SESAME EOS models as well as quantum molecular dynamics simulation results for carbon, which were very consistent with the experimental data.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2004

Thin-Filament Pyrometry Developed for Measuring Temperatures in Flames

Many valuable advances in combustion science have come from observations of microgravity flames. This research is contributing to the improved efficiency and reduced emissions of practical combustors and is benefiting terrestrial and spacecraft fire safety. Unfortunately, difficulties associated with microgravity have prevented many types of measurements in microgravity flames. In particular, temperature measurements in flames are extremely important but have been limited in microgravity. A novel method of measuring temperatures in microgravity flames is being developed in-house at the National Center for Microgravity Research and the NASA Glenn Research Center and is described here. Called thin-filament pyrometry, it involves using a camera to determine the local gas temperature from the intensity of inserted fibers glowing in a flame. It is demonstrated here to provide accurate measurements of gas temperatures in a flame simultaneously at many locations. The experiment is shown. The flame is a laminar gas jet diffusion flame fueled by methane (CH4) flowing from a 14-mm round burner at a pressure of 1 atm. A coflowing stream of air is used to prevent flame flicker. Nine glowing fibers are visible. These fibers are made of silicon carbide (SiC) and have a diameter of 15 m (for comparison, the average human hair is 75 m in diameter). Because the fibers are so thin, they do little to disturb the flame and their temperature remains close to that of the local gas. The flame and glowing filaments were imaged with a digital black-and-white video camera. This camera has an imaging area of 1000 by 1000 pixels and a wide dynamic range of 12 bits. The resolution of the camera and optics was 0.1 mm. Optical filters were placed in front of the camera to limit incoming light to 750, 850, 950, and 1050 nm. Temperatures were measured in the same flame in the absence of fibers using 50-m Btype thermocouples. These thermocouples provide very accurate temperatures, but they generally are not useful in microgravity tests because they measure temperature at only one location at a time. Thermocouple measurements at a height of 11 mm above the burner were used to calibrate the thin-filament pyrometry system at all four wavelengths. This calibration was used to perform thin-filament pyrometry at other heights above the burner. One such profile is shown in this graph; this is for a height of 21 mm. The agreement between the pyrometry measurements and thermocouple results at this height is excellent in the range of 1000 to 2000 K, with an estimated uncertainty of 50 K and an estimated upper limit of 2500 K. Neither the thermocouple nor the thin-filament pyrometry temperatures have been corrected for radiation, but the correction is expected to be nearly the same for both methods. We anticipate that thin-filament pyrometry similar to that developed here will become an important diagnostic for studies of microgravity flames owing to its accuracy and its ability to simultaneously measure finely spaced temperatures.

Sunderland, Peter B.↗
DOE OSTI2019

Fully automated calibration for acoustic pyrometry

A method of calibrating transceiver positions inside an acoustic pyrometry measuring vessel that contains a plurality of transceivers, includes determining (40) a speed of sound in the acoustic pyrometry measuring vessel from a temperature and gas composition of a gas inside the acoustic pyrometry measuring vessel, acquiring (41) time-of-flight (TOFs) Δti,j measurements from a plurality of pairs i,j of transceivers inside the acoustic pyrometry measuring vessel, estimating (42) a radius of the acoustic pyrometry measuring vessel from an average of the acquired TOF measurements, and using (43) an estimated radius of the acoustic pyrometry measuring vessel to estimate errors Δθj of displacement angles of the transceivers.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2019

Two-color pyrometry system to eliminate optical errors for spatially resolved measurements in flames

Two color (2C) pyrometry has long been used to measure flame temperature and soot concentration from radiative emission in flames. While 2C pyrometry is not an absolute measurement in non-axisymmetric flames (such as diesel spray combustion) it is a desirable diagnostic for semi-quantitative or qualitative measurements since it requires minimal optical access and can utilize high-speed imaging to attain exceptional temporal and spatial resolution. In this work, an improved optical configuration of 2C pyrometry is presented that 1) eliminates optical errors inherent in other designs, and 2) uses off-the-shelf optics and a single camera . In particular, this work analyzes the impact of parallax and path length differences on the 2C pyrometry measurement and exemplifies how the present design eliminates associated errors by design rather than in post-processing. Finally, the theoretical range of measurements were generated a priori and overlaid with experimental data to illustrate the dynamic range over which 2C pyrometry can determine the soot concentration and temperature in theory and in practice.

47 OTHER INSTRUMENTATION↗
DOE OSTI2019

Linking pyrometry to porosity in additively manufactured metals

Porosity in additively manufactured metals can reduce material strength which is generally considered undesirable. Although studies have shown relationships between process parameters and porosity, monitoring strategies for defect detection and pore formation are still needed. In this paper, instantaneous anomalous conditions are detected in-situ via pyrometry during laser powder bed fusion additive manufacturing and correlated with voids observed using post-build micro-computed tomography. Large two-color pyrometry data sets were used to estimate instantaneous temperatures, melt pool orientations and aspect ratios. Machine learning algorithms were then applied to processed pyrometry data to detect outlier images and conditions. It is shown that melt pool outliers are good predictors of voids observed post-build. With this approach, real time process monitoring can be incorporated into systems to detect defect and void formation. Alternatively, using the methodology presented here, pyrometry data can be post processed for porosity assessment.

36 MATERIALS SCIENCE↗
DOE OSTI2021

A comparison of Raman and pyrometry dynamic temperature measurements of shocked cyclohexane

Optical pyrometry is a well-developed, broadly applicable method to determine temperature in dynamic compression experiments. However, it measures radiation from only the skin depth of the radiant material, is highly susceptible to spurious backgrounds, and requires an often-unmeasurable free parameter—the sample dynamic emissivity. Raman spectroscopy offers a method to determine temperature directly from fundamental theory, but it is practically limited in applications to a small subset of shock experiments. In this work, we describe an experiment allowing simultaneous application of Raman and pyrometric temperature techniques to benchmark a specific instance of pyrometry. We attempted both measurements on multiple experiments and compare the successful temperature results between the separate but highly repeatable shots. Here, we find that dynamic shock temperatures inferred from Raman spectroscopy and pyrometry generally agree within the uncertainties of each measurement, although those uncertainties are larger than typical for a specially designed pyrometry experiment on a shocked metal sample.

74 ATOMIC AND MOLECULAR PHYSICS↗
DOE OSTI2019

Comparison of Simultaneous Shock Temperature Measurements from Three Different Pyrometry Systems

Pyrometry is one of the most prevalent techniques for measuring temperature in shock physics experiments. However, the challenges of applying pyrometry in such highly dynamic environments produces multiple sources of uncertainty that require investigation. An outstanding question is the degree of agreement between different pyrometers and different experiments. Here we report a series of novel plate impact experiments with simultaneous thermal radiance measurements using three different multi-wavelength optical pyrometry systems, each with different spatial and temporal resolutions, on samples shocked to identical states. We compare the temperatures measured by each system and their associated uncertainties using a number of emissivity assumptions. The results shown that the measurements from all three systems agree within uncertainty. Furthermore, some non-thermal light contamination was observed despite a number of prevention measures.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Sensor fusion of pyrometry and acoustic measurements for localized keyhole pore identification in laser powder bed fusion

We report in-situ process monitoring as an aid to part qualification for laser powder-bed fusion (L-PBF) technology is a topic of increasing interest to the additive manufacturing community. In this work, airborne acoustic and inline pyrometry measurements were recorded simultaneously with the laser position. X-ray radiography imaging was used to spatio-temporally register keyhole pore locations to the pyrometry and acoustic signals, enabling binary labeling of data partitions based on pore formation. These labeled partitions were subsequently featurized using a highly comparative time-series analysis toolbox. Acoustic data was found to be much more effective than the pyrometry data for keyhole pore identification. However, when the information contained in both sensing modalities was combined in a sensor fusion strategy, the error rates of the top performing models were significantly reduced.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Experiments at TA-55 have used optical pyrometry to measure temperatures of shocked plutonium on the 40mm gun

Researchers at LANL, along with collaborators from MSTS, have worked for more than a decade to develop and implement an optical pyrometry method to measure the temperature of metals shocked to the high pressures and temperatures. Because traditional shock wave measurements only provide information on the mechanical state of the material, temperature measurements are required to validate and improve equation-of-state (EOS) models for materials. The conditions sampled are complex; commenserate with those found in planetary impacts, and accressed by conventional and nuclear weapons. Optical pyrometry is currently the best available method for inferring the temperature of shocked metals, by careful measurement of the calibrated radiance emitted by a surface at finite temperature. These measurements are difficult often complicated by the short time scales associated with shock wave experiments (<1 µs) coupled with the many sources of non-thermal light (impact flash, fracture light, etc.) that pollutes the radiant light measured from the sample.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2020

Detecting keyhole porosity and monitoring process signatures in additive manufacturing: an in situ pyrometry and ex situ X-ray radiography correlation

Creation of pores and defects during laser powder bed fusion (LPBF) can lead to poor mechanical properties and thus must be minimized. Post-build inspection is required to ensure the printed parts contain acceptably low defect concentrations. These inspections are time consuming and costly, especially for large or complex parts. As a potential solution, in situ process monitoring can be used to detect the creation of defects, characterize local material behavior and predict expected component properties. However, the precise relationship between pore creation and in situ process monitoring still needs to be understood. In this work, high-speed infrared diode-based pyrometry and high-speed optical imaging signals were used to monitor LPBF printing of 446 stainless steel 316 L single tracks with varying laser power and velocity. Results indicate an increase in pyrometer signal and melt pool dimensions with increasing laser power and decreasing velocity in agreement with previous work. In addition, careful analysis of pyrometer signal reveals a distinct signature of the conduction-to-keyhole mode transition which was confirmed by metallography. Critically, pore defect initiation as characterized by ex situ X-ray radiography was correlated with in situ thermal monitoring signals to derive the probability of defect creation. Our results show that, in principle, a probabilistic prediction of pore formation can be achieved based on in situ high-speed pyrometry monitoring of the LPBF melt pool.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Two-color pyrometry based flame to fuel surface radiative heat flux diagnostic using flamelets

In this study, a non-intrusive two-color pyrometry based radiative heat flux diagnostic is presented that accounts for the self-absorption effects. This diagnostic relies on looking up the flame temperature and soot volume fraction using the ratio of color intensities obtained from digital cameras and numerical solutions of 1D steady-state diffusion flames. Virtual two color pyrometry of computed flame show a unique one-to-one mapping of strained flames with intensity ratio; thereby allowing flames to be indexed and creation of a two-color flamelet manifold (TCFM). The TCFM is a function of two variables; the ratio of red to green intensities (flame index) and physical distance to the stoichiometric surface defined using a level-set function. The developed diagnostic is used in upward flame spread experiments where an approximate flame hull reconstruction method is applied to provide the 3D level-set function and intensity ratio for use of TCFM to provide radiative absorption properties for 3D ray tracing. Accounting for self- absorption effects provide improved soot volume fraction estimates. In conclusion, the radiative heat flux estimates are found to be in very good agreement with literature and improved results are obtained near the flame base.

42 ENGINEERING↗
DOE OSTI2017

Study of aluminum particle combustion in solid propellant plumes using digital in-line holography and imaging pyrometry

The combustion of molten metals is an important area of study with applications ranging from solid aluminized rocket propellants to fireworks displays. Our work uses digital in-line holography (DIH) to experimentally quantify the three-dimensional position, size, and velocity of aluminum particles during combustion of ammonium perchlorate (AP) based solid-rocket propellants. Additionally, spatially resolved particle temperatures are simultaneously measured using two-color imaging pyrometry. To allow for fast characterization of the properties of tens of thousands of particles, automated data processing routines are proposed. In using these methods, statistics from aluminum particles with diameters ranging from 15 to 900 µm are collected at an ambient pressure of 83 kPa. In the first set of DIH experiments, increasing initial propellant temperature is shown to enhance the agglomeration of nascent aluminum at the burning surface, resulting in ejection of large molten aluminum particles into the exhaust plume. The resulting particle number and volume distributions are quantified. In the second set of simultaneous DIH and pyrometry experiments, particle size and velocity relationships as well as temperature statistics are explored. The average measured temperatures are found to be 2640 ± 282 K, which compares well with previous estimates of the range of particle and gas-phase temperatures. The novel methods proposed here represent new capabilities for simultaneous quantification of the joint size, velocity, and temperature statistics during the combustion of molten metal particles. The proposed techniques are expected to be useful for detailed performance assessment of metalized solid-rocket propellants.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Predicting melt pool depth and grain length using multiple signatures from in-situ single camera two-wavelength imaging pyrometry for laser powder bed fusion

In laser powder bed fusion (LPBF), the in-situ process signatures are known to have a direct correlation with the microstructural properties of the solidified melt pool (MP). It is known that the MP cooling and heating rates, and laser processing parameters can critically determine the grain structure and thereby affect the part properties. The objective of this work is to study the feasibility of using in-process, high-speed imaging pyrometry for evaluating the solidified MP properties “below” the surface, such as depth and microstructural properties. To accomplish this, we employ an in-house single camera-based two-wavelength imaging pyrometry (STWIP) system for monitoring the printing of single-scan tracks with Inconel 718 on a commercial LPBF printer (EOS M290). Further, the lab designed STWIP system is a coaxial high-speed (>10,000 fps) imaging system capable of monitoring MP temperature, morphology, and intensity profiles. The temperature measurements from STWIP are emissivity independent. The STWIP measured MP signatures of the printed tracks are correlated with the ex-situ microscopy characterized MP depth and the average grain lengths. From the data analysis, using support vector machine (SVM)-based regression models, we found that the MP temperature signatures are crucial for an accurate prediction of MP depth and the grain length, thus validating the novelty and necessity of the developed in-situ monitoring methods and analysis.

36 MATERIALS SCIENCE↗
DOE OSTI2014

2D surface temperature measurement of plasma facing components with modulated active pyrometry

In nuclear fusion devices, such as Tore Supra, the plasma facing components (PFC) are in carbon. Such components are exposed to very high heat flux and the surface temperature measurement is mandatory for the safety of the device and also for efficient plasma scenario development. Besides this measurement is essential to evaluate these heat fluxes for a better knowledge of the physics of plasma-wall interaction, it is also required to monitor the fatigue of PFCs. Infrared system (IR) is used to manage to measure surface temperature in real time. For carbon PFCs, the emissivity is high and known (ε ~ 0.8), therefore the contribution of the reflected flux from environment and collected by the IR cameras can be neglected. However, the future tokamaks such as WEST and ITER will be equipped with PFCs in metal (W and Be/W, respectively) with low and variable emissivities (ε ~ 0.1–0.4). Consequently, the reflected flux will contribute significantly in the collected flux by IR camera. The modulated active pyrometry, using a bicolor camera, proposed in this paper allows a 2D surface temperature measurement independently of the reflected fluxes and the emissivity. Experimental results with Tungsten sample are reported and compared with simultaneous measurement performed with classical pyrometry (monochromatic and bichromatic) with and without reflective flux demonstrating the efficiency of this method for surface temperature measurement independently of the reflected flux and the emissivity.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗