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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1992

Thermal Control Surfaces Experiment (TCSE) materials analysis

Materials on the Thermal Control Surfaces Experiment (TCSE) underwent changes in their properties during the 5.8 years of exposure to the combined space environment. The analysis of these materials is continuing and current results are discussed. Some materials were significantly degraded such as silver Teflon, S13GLO, and Z302; while others such as Z93 and YB71 were stable. Time dependent flight data is provided, along with preflight and postflight measurements. Results are compared with other experiments, demonstrating the atomic oxygen (AO) ram effect. Atomic oxygen texturing of silver Teflon varies with incident angle. Even indirect exposure to atomic oxygen appears to be involved with surface texturing on the interior of the TCSE. Localized contamination occurred at discrete locations both inside and on exterior surfaces. Most of the visible deposits were the result of the classical photo-enhanced contamination deposition. The synergism of combined space environmental effects is demonstrated by the specific localization of contamination caused by photo-enhanced deposition versus AO removal. Optical degradation measurements of these contaminated areas, utilizing a new portable reflectometer, are presented.

Wilkes, Donald R.↗
NASA NTRS2009

Modern Material Analysis Instruments Add a New Dimension to Materials Characterization and Failure Analysis

Modern analytical tools can yield invaluable results during materials characterization and failure analysis. Scanning electron microscopes (SEMs) provide significant analytical capabilities, including angstrom-level resolution. These systems can be equipped with a silicon drift detector (SDD) for very fast yet precise analytical mapping of phases, as well as electron back-scattered diffraction (EBSD) units to map grain orientations, chambers that admit large samples, variable pressure for wet samples, and quantitative analysis software to examine phases. Advanced solid-state electronics have also improved surface and bulk analysis instruments: Secondary ion mass spectroscopy (SIMS) can quantitatively determine and map light elements such as hydrogen, lithium, and boron - with their isotopes. Its high sensitivity detects impurities at parts per billion (ppb) levels. X-ray photo-electron spectroscopy (XPS) can determine oxidation states of elements, as well as identifying polymers and measuring film thicknesses on coated composites. This technique is also known as electron spectroscopy for chemical analysis (ESCA). Scanning Auger electron spectroscopy (SAM) combines surface sensitivity, spatial lateral resolution (10 nm), and depth profiling capabilities to describe elemental compositions of near and below surface regions down to the chemical state of an atom.

Panda, Binayak↗
NASA NTRS1972

Surveyor 3 material analysis plan, Appendix B

The Surveyor 3 material analysis plan is composed of a series of comprehensive charts of all science and engineering investigations reported. The plan progresses from left to right on each figure. Each test was designed to ensure that the subsequent tests would not be significantly affected by those that preceded it. Each box represents one or more tasks performed by the individual or firm named at the lower left. The upper-right corner shows the amount and type of material subjected to the test or tests listed within the box.

Nickle, N. L.↗
NASA NTRS1987

Materials analysis by ultrasonics: Metals, ceramics, composites

Research results in analytical ultrasonics for characterizing structural materials from metals and ceramics to composites are presented. General topics covered by the conference included: status and advances in analytical ultrasonics for characterizing material microstructures and mechanical properties; status and prospects for ultrasonic measurements of microdamage, degradation, and underlying morphological factors; status and problems in precision measurements of frequency-dependent velocity and attenuation for materials analysis; procedures and requirements for automated, digital signal acquisition, processing, analysis, and interpretation; incentives for analytical ultrasonics in materials research and materials processing, testing, and inspection; and examples of progress in ultrasonics for interrelating microstructure, mechanical properties, and dynamic response.

Vary, Alex↗
NASA NTRS2021

5 Inch Thick 2219-T87 Plate Low Ductility Investigation - Material Analysis on Broken 2219 Tensile Samples

2219-T87 material used on a LOX tank baffle support on Artemis-I showed unusually low fracture elongation. Recent material data indicated 5” thick 2219-T87 plate stock had very low ductility (<1%) in the short transverse direction at the half-thickness location. Metallurgical analysis performed to understand the root cause that led to the drastic reduction in tensile ductility. The PowerPoint report details the key findings from material analysis by optical and scanning electron microscopy.

aluminum alloy 2219↗
NASA NTRS2004

Materials Analysis: A Key to Unlocking the Mystery of the Columbia Tragedy

Materials analyses of key forensic evidence helped unlock the mystery of the loss of space shuttle Columbia that disintegrated February 1, 2003 while returning from a 16-day research mission. Following an intensive four-month recovery effort by federal, state, and local emergency management and law officials, Columbia debris was collected, catalogued, and reassembled at the Kennedy Space Center. Engineers and scientists from the Materials and Processes (M&P) team formed by NASA supported Columbia reconstruction efforts, provided factual data through analysis, and conducted experiments to validate the root cause of the accident. Fracture surfaces and thermal effects of selected airframe debris were assessed, and process flows for both nondestructive and destructive sampling and evaluation of debris were developed. The team also assessed left hand (LH) airframe components that were believed to be associated with a structural breach of Columbia. Analytical data collected by the M&P team showed that a significant thermal event occurred at the left wing leading edge in the proximity of LH reinforced carbon carbon (RCC) panels 8 and 9. The analysis also showed exposure to temperatures in excess of 1,649 C, which would severely degrade the support structure, tiles, and RCC panel materials. The integrated failure analysis of wing leading edge debris and deposits strongly supported the hypothesis that a breach occurred at LH RCC panel 8.

Mayeaux, Brian M.↗
DOE OSTI2025

Editorial: Applications of spectroscopy and chemometrics in nuclear materials analysis

Optical analysis techniques, including spectroscopy and image analysis, have many advantages when applied to the study of nuclear materials. They require small sample sizes, can be performed remotely, and can be proceduralized through consistent practice. Most importantly, they provide a wealth of information by generating multivariate data. For example, ultraviolet–visible–near-infrared absorbance spectroscopy of actinides in aqueous and organic solutions is dependent on the oxidation state, anionic complexation, and temperature. These variables are important for solution-based separation processes, and sensitivity to these factors, combined with online monitoring, can drive the efficiency and control of these processes. The morphology and chemical composition of actinide particles can also provide a vital clue to the mechanisms by which the particles were formed, providing forensic information on the origins of the particles.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1979

Utilization of nuclear methods for materials analysis and the determination of concentration gradients

The various types of nuclear chemical analysis methods are discussed. The possibilities of analysis through activation and direct observation of nuclear reactions are described. Such methods make it possible to analyze trace elements and impurities with selectivity, accuracy, and a high degree of sensitivity. Such methods are used in measuring major elements present in materials which are available for analysis only in small quantities. These methods are well suited to superficial analyses and to determination of concentration gradients; provided the nature and energy of the incident particles are chosen judiciously. Typical examples of steels, pure iron and refractory metals are illustrated.

Darras, R.↗
NASA NTRS2004

Material Analysis and Identification

KeyMaster Technologies, Inc., develops and markets specialized, hand-held X-ray fluorescence (XRF) instruments and unique tagging technology used to identify and authenticate materials or processes. NASA first met with this Kennewick, Washington-based company as the Agency began seeking companies to develop a hand-held instrument that would detect data matrix symbols on parts covered by paint and other coatings. Since the Federal Aviation Administration was also searching for methods to detect and eliminate the use of unapproved parts, it recommended that NASA and KeyMaster work together to develop a technology that would benefit both agencies.

Source record↗
NASA NTRS1993

The continuing materials analysis of the thermal control surfaces experiment (S0069)

The long term effects of the natural and induced space environment on spacecraft surfaces are critically important to future spacecraft - including Space Station Freedom. The damaging constituents of this environment include thermal vacuum, solar ultraviolet radiation, atomic oxygen, particulate radiation, and the spacecraft induced environment. The behavior of materials and coatings in the space environment continues to be a limiting technology for spacecraft and experiments. The Thermal Control Surfaces Experiment (TCSE) was flown on the National Aeronautics and Space Administration (NASA) Long Duration Exposure Facility (LDEF) to study these environmental effects on surfaces-particularly on thermal control surfaces. The TCSE was a comprehensive experiment that combined in-space measurements with extensive pre- and post-flight analyses of thermal control surfaces to determine the effects of exposure to the low Earth orbit space environment. The TCSE is the first space experiment to directly measure the total hemispherical reflectance of thermal control surfaces in the same way they are routinely measured in the laboratory. The trend analyses of selected coatings performed as part of the continuing post-flight analysis of the TCSE are described. A brief description of the TCSE and its mission on LDEF are presented. There are several publications available that describe the TCSE, it's mission on LDEF, and initial results in greater detail. These are listed in the TCSE Bibliography.

Wilkes, Donald R.↗
NASA NTRS2003

Surface Material Analysis of the S-type Asteroids: Removing the Space Weathering Effect from Reflectance Spectrum

Recent years, many researchers have been observing a lot of asteroid reflectance spectra in the UV, visible to NIR at wavelength region. Reflectance spectroscopy of asteroid at this range should bring us a lot of information about its surface materials. Pyroxene and olivine have characteristic absorption bands in this wavelength range. Low-Ca pyroxene has two absorption bands around 0.9 microns and 1.9 microns. The more Ca and Fe content, the longer both absorption band centers. On the other hand, reflectance spectrum of olivine has three complicated absorption bands around 1 m, and no absorption feature around 2 microns. In general, reflectance spectra of many asteroids that are considered to be silicate rich (i.e., S- and A type asteroids) show redder slope and more subdued absorption bands than those of terrestrial minerals and meteorites. These features are now believed to be caused by the space weathering effect, which is probably caused by micrometeorite bombardment and/or solar wind. This process causes nanophase reduced iron (npFe(sup 0)) particles near the surface of mineral grains, which leads the optical change. Therefore, the space weathering effect should be removed from asteroid reflectance spectra to compare with those of meteorite and terrestrial minerals. In this report, we will apply the expanded modified Gaussian model (MGM) to the reflectance spectra of S-type asteroids 7 Iris and 532 Herculina and compare them with those of meteorites.

Ueda, Y.↗
NASA NTRS2017

Material Analysis and System Design for Exploration Life Support Systems 2017

Advanced Environmental Control and Life Support System (ECLSS) design is critical for manned space flight beyond Earth. Current systems enable extended missions in low-Earth orbit, but for deep-space missions, not only will astronauts be outside the reach of resupply operations from Earth but they will also need to handle malfunctions and compensate for the degradation of materials. These two daunting challenges must be overcome for long-term independent space flight. In order to solve the first, separation and recycling of onboard atmosphere is required. Current systems utilize space vacuum to fully regenerate CO2 sorbent beds, but this is not sustainable. The second challenge stems from material and performance degradation due to operational cycling and on-board contaminants. This report will review the recent work by the ECLSS team at Marshall Space Flight Center towards overcoming these challenges by characterizing materials via novel methods and by assessing new air revitalization systems.

Knox, Jim↗
NASA NTRS1999

C/SiC Component & Material Analysis, Attachment Verification, & Blisk Turbopump Testing

Ceramic composite blisk components constructed of carbon fibers & silicon carbide ceramic matrix have been fabricated and tested. Room and cryogenic torque testing have verified the attachment configuration. The polar and quasi-isotropic blisks have been proof spun, balanced, and tested in the Simplex turbopump. Foreign particle impact analysis was conducted for C/SiC. Data and manufacturing lessons learned are significantly benefiting the development of the Reusable Launch Vehicle's ceramic matrix composite integrally bladed disk.

Effinger, Michael R.↗