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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Radiation Damage Studies on Titanium Alloys as High Intensity Proton Accelerator Beam Window Materials

A high-strength dual a+ß phase titanium alloy Ti–6Al–4V is utilized as a material for beam windows in several accelerator target facilities. However, relatively little is known about how material properties of this alloy are affected by high-intensity proton beam irradiation. With plans to upgrade neutrino facilities at J-PARC and Fermilab to over 1 MW beam power, the radiation damage in the window material will reach a few displacements per atom (dpa) per year, significantly above the ~0.3 dpa level of existing data. The international RaDIATE collaboration, Radiation Damage In Accelerator Target Environments, has conducted a high intensity proton beam irradiation of various target and window material specimens at Brookhaven Linac Isotope Producer (BLIP) facility, including a variety of titanium alloys. Post-Irradiation Examination (PIE) of the specimens in the 1st capsule, irradiated at up to 0.25 dpa, is in progress. Tensile tests in a hot cell at Pacific Northwest National Laboratory (PNNL) exhibited a clear signature of radiation hardening and loss of ductility for Ti–6Al–4V, while Ti–3Al–2.5V, with less ß phase, exhibited less severe hardening. Microstructural investigations will follow to study the cause of the difference in tensile behavior between these alloys. High-cycle fatigue (HCF) performance is critical to the lifetime estimation of beam windows exposed to a periodic thermal stress from a pulsed proton beam. The first HCF data on irradiated titanium alloys are to be obtained by a conventional bend fatigue test at Fermilab and by an ultrasonic mesoscale fatigue test at Culham Laboratory. Specimens in the 2nd capsule, irradiated at up to ~1 dpa, cover typical titanium alloy grades, including possible radiation-resistant candidates. These systematic studies on the effects of radiation damage of titanium alloy materials are intended to enable us not only to predict realistic lifetimes of current beam windows made of Ti–6Al–4V, but also to extend the lifetime by choosing a more radiation and thermal shock tolerant alloy with a preferable heat treatment, or even by developing new materials.

Titanium Alloy, Beam Window, Proton Beam, Radiatio↗
DOE OSTI2016

Assessment of candidates for target window material in accelerator-driven molybdenum-99 production

NorthStar Medical Technologies is pursuing production of an important medical isotope, Mo-99, through a photo-nuclear reaction of a Mo-100 target using a high-power electron accelerator. The current target utilizes an Inconel 718 window. The purpose of this study was to evaluate other candidate materials for the target window, which separates the high-pressure helium gas inside the target from the vacuum inside the accelerator beamline and is subjected to significant stress. Our initial analysis assessed the properties (density, thermal conductivity, maximum stress, minimum window thickness, maximum temperature, and figure of merit) for a range of materials, from which the three most promising were chosen: Inconel 718, 250 maraging steel, and standard-grade beryllium. These materials were subjected to further analysis to determine the effects of thermal and mechanical strain versus beam power at varying thicknesses. Both beryllium and the maraging steel were calculated to withstand more than twice as high beam power than Inconel 718.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Two dimensional meta-material windows

Conductive nanoshells are oriented so as to redirect incident radiation as a function of wavelength. Nanoshells can be formed on templates such as nanospheres or gratings and embedded in an elastomeric layer. In some examples, conductive nanoshells are coupled to a layer that is configured to unbuckle and buckle as a function of temperature, so that radiation in one or more wavelength ranges is directed differently at different temperatures. Building windows can include such layers to that infrared radiation is reflected on warm days and directed into a building on cool days. Such layers can also direct incident visible radiation to a room ceiling so as to enhance interior lighting.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2019

Effects of Electron Irradiation on Candidate Materials for Target Window in Accelerator-Driven Molybdenum-99 Production

NorthStar Medical technologies is planning to produce Mo-99 through the photo-nuclear reaction Mo-100 (γ,n) Mo-99 utilizing multiple high-power electron accelerators. In this approach, the production target consists of multiple thin disks of metal Mo-100 cooled by helium gas at high (300–400 psi) pressure [4]. The cost of enriched Mo-100 is on the order of $500 - 1,000 per gram, which makes a smaller target desirable and requires achieving the highest possible electron flux on the target. The heat deposition in the entrance window limits the maximum flux because the window separates the vacuum in the accelerator beam line from the high-pressure helium in the target and is only cooled on one side by the helium flow. Because the window is continuously under stress from the helium pressure and the heat from the electron beam, it is desirable to estimate a lifetime for the window and develop a replacement schedule for the target holder. Such an estimate requires the ability to predict changes in the window material properties under electron irradiation. Candidate materials for the Mo-99 production target window are Inconel 718, 250 maraging steel, and beryllium. These materials encompass a wide range of thermal conductivity, thermal expansion coefficients, Young’s modulus, tensile strength and tensile ductility. The Mo-99 target window is subjected to internal pressure from the helium coolant and thermal stresses. The operating conditions and relative advantages of each material have been described previously [1]. The current work investigates the effects of electron irradiation on the tensile properties of these materials. Axial tensile tests were conducted with electron-irradiated samples and results were compared to baseline results generated for as-fabricated materials.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Innovative Glazing Materials

Windows have the unique capability of being able to achieve a net zero energy impact by admitting solar gains in the winter to offset thermal losses and admitting daylight to offset electric lighting. If rejection or admission of solar heat gains and daylight are appropriately timed, then heating, cooling and lighting energy use at the perimeter zone can be reduced to net zero energy levels. Nano-scale switchable coatings on glass have been developed to actively modulate solar intensity and spectral transmission. We provide a brief overview of these switchable glazing materials, discuss the desired performance objectives for such materials, and present results from recently completed monitored studies of state-of-the-art switchable windows, particularly with respect to occupant response and market factors. Careful application of state-of-the-art switchable windows and new material science developments on the horizon can deliver the desired net zero energy performance while meeting critical human factors and market related requirements.

Building energy efficiency↗
DOE OSTI2018

Effect of Window-Layer Materials on p-n Junction Location in Cu(In,Ga)Se 2 Solar Cells

We report on measurements of junction location in Cu(In,Ga)Se $_{2}$ (CIGS) solar cells with different window-layer materials by nm-resolution electrical potential/field profiling across the junction using Kelvin probe force microscopy imaging on cross-section of the devices. The results illustrate that the device with a CdS window layer (CdS/CIGS) has a buried homojunction located inside the CIGS absorber with ~40-nm junction depth, whereas the ZnOS/CIGS devices with and without partial electrolyte treatment prior to the window-layer deposition are similar, exhibiting a heterointerface junction. This junction location may contribute in part to the highest efficiency of the CdS/CIGS device among the three devices.

14 SOLAR ENERGY↗
DOE OSTI2023

Insights into radiation resistance of titanium alloys from displacement cascade simulations

Radiation damage in beam window materials limits the use of high power proton beams in high energy physics research. The alloy Ti-6Al-4V is presently used as a beam window material but a prospective alternative, Ti-15V-3Cr-3Sn-3Al has been proposed. Since both these alloys contain dual phases at room temperature, we compare the radiation damage in the α and ß-phases of these two materials via primary knock-on atom (PKA) cascade simulations in the 10-40keV energy range. At PKA energies 30 and 40keV, the number of Frenkel pairs in the ballistic stage is higher in the ß-phase of Ti-6Al-4V than that in the ß-phase of Ti-15V-3Cr-3Sn-3Al almost by a factor of 2. The α-phase, of both these alloys, by far outperforms the ß-phases of the two alloys, both in terms of damage during the ballistic stage and in terms of the surviving defects. The average displacement threshold energy (E d ) in the α-phase of both alloys was found to be 66eV while that in the ß-phase of Ti-15-3 was 55 eV and in the ß-phase of Ti-6-4 was 46. Further, while the number of surviving defects is almost equal in both alloys, the vacancy and interstitial clustering mechanisms differ notably, which can impact the degree of radiation hardening and loss of ductility. Our simulations show larger vacancy and interstitial clusters form in Ti-6Al-4V as compared to that in Ti-15-3-3-3 alloy. These results indicate that Ti-15-3-3-3 alloys may be a promising candidate for next generation beam window material with a higher radiation tolerance than the existing Ti-6-4 alloy.

36 MATERIALS SCIENCE↗
DOE OSTI2015

High-temperature strain cell for tomographic imaging

This disclosure provides systems, methods, and apparatus related to the high temperature mechanical testing of materials. In one aspect, a method includes providing an apparatus. The apparatus may include a chamber. The chamber may comprise a top portion and a bottom portion, with the top portion and the bottom portion each joined to a window material. A first cooled fixture and a second cooled fixture may be mounted to the chamber and configured to hold the sample in the chamber. A plurality of heating lamps may be mounted to the chamber and positioned to heat the sample. The sample may be placed in the first and the second cooled fixtures. The sample may be heated to a specific temperature using the heating lamps. Radiation may be directed though the window material, the radiation thereafter interacting with the sample and exiting the chamber through the window material.

42 ENGINEERING↗
DOE OSTI2020

Tensile behavior of dual-phase titanium alloys under high-intensity proton beam exposure: radiation-induced omega phase transformation in Ti-6Al-4V

A high-intensity proton beam exposure with 181 MeV energy has been conducted at Brookhaven Linac Isotope Producer facility on various material specimens for accelerator targetry applications, including titanium alloys as a beam window material. The radiation damage level of the analyzed capsule was 0.25 dpa at the beam center region with an irradiation temperature around 120 oC. Tensile tests showed increased hardness and a large decrease in ductility for the dual a+ß-phase Ti-6Al-4V Grade-5 and Grade-23 extra low interstitial alloys, with the near a-phase Ti-3Al-2.5V Grade-9 alloy still exhibiting uniform elongation of a few % after irradiation. Transmission Electron Microscope analyses on Ti-6Al-4V indicated clear evidence of a high-density of defect clusters with size less than 2 nm in each a-phase grain. The ß-phase grains did not contain any visible defects such as loops or black dots, while the diffraction patterns clearly indicated ?-phase precipitation in an advanced formation stage. The radiation-induced ?-phase transformation in the ß-phase could lead to greater loss of ductility in Ti-6Al-4V alloys in comparison with Ti-3Al-2.5V alloy with less ß-phase.google scho

Tensile Test, titanium, acclerator, proton beam↗
DOE OSTI2014

Nanostructured electrochromic smart windows: traditional materials and NIR-selective plasmonic nanocrystals

Electrochromic devices, which dynamically change colour under applied potential, are widely studied for use in energy-efficient smart windows. To improve the viability of smart windows, many researchers are utilizing nanomaterials, which can provide electrochromic devices with improved colouration efficiencies, faster switching times, longer cycle lives, and potentially reduced costs. In an effort to demonstrate a new type of electrochromic device that goes beyond the capabilities of commonly used electrochromic materials, researchers have turned to plasmonic transparent conductive oxide (TCO) nanocrystals. Electrochemical injection of electrons into plasmonic TCO nanocrystal films induces a shift in the plasmon frequency and gives rise to the new functionality of selective optical modulation in the near-infrared region of the solar spectrum. These nanocrystals can be used as building blocks to enable creation of advanced electrochromic devices containing mesoporous electrodes or nanocrystal-in-glass composites. Such devices have been important in advancing the field towards achieving the ideal smart window with independent control over visible and NIR transmittance.

Runnerstrom, EL↗
DOE OSTI2016

Development of Gen-II LAPPD TM Systems For Nuclear Physics Experiments

The technical objectives of this Phase I program were to; Demonstrate proof of concept of a pin-free pixelated readout using an inside-out approach. “Inside-out” is a novel approach for having the ground plane on the inside (floor of the anode facing the MCP stack-up) and anode pads on the outside of the LAPPD. The goal is a demonstration of capacitive coupling through the bottom anode plate (9.02 x 8.66”), using ceramic, and, optionally, glass tile components; Develop a ceramic package or Lower Tile Assembly (LTA) consisting of hermetically sealing a ceramic sidewall to a ceramic anode producing a single unit capable of housing the MCP stack up enabling development of a Gen II LAPPDTM having low loss, high bandwidth and mechanical robustness. The ceramic bodies used in this Task will be the same as in Task 1 and Task 3. Our goal was to work with commercial suppliers to economically fabricate the ceramic components; Evaluate alternative LAPPD top window materials to determine compatibility in sealing to the ceramic sidewall described in Task 2. Concurrently we will specify and select an alloy seal material suitable for sealing the top window to the sidewall, and we will perform sealing trials of these components; Demonstrate electrical characteristics of the inside-out anode in the detector context, the seal integrity of the bonded two-piece ceramic lower tile assembly (LTA) as well as the hermetic seal quality of the window to the sidewall; and Secure at least one specific NP, HEP or commercial application for a Gen II LAPPDTM enabled by this technology to be developed in Phase II.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2021

Lasergate: A windowless gas target for enhanced laser preheat in magnetized liner inertial fusion

At the Z Facility at Sandia National Laboratories, the magnetized liner inertial fusion (MagLIF) program aims to study the inertial confinement fusion in deuterium-filled gas cells by implementing a three-step process on the fuel: premagnetization, laser preheat, and Z-pinch compression. In the laser preheat stage, the Z-Beamlet laser focuses through a thin polyimide window to enter the gas cell and heat the fusion fuel. However, it is known that the presence of the few μm thick window reduces the amount of laser energy that enters the gas and causes window material to mix into the fuel. These effects are detrimental to achieving fusion; therefore, a windowless target is desired. The Lasergate concept is designed to accomplish this by “cutting” the window and allowing the interior gas pressure to push the window material out of the beam path just before the heating laser arrives. In this work, we present the proof-of-principle experiments to evaluate a laser-cutting approach to Lasergate and explore the subsequent window and gas dynamics. Further, an experimental comparison of gas preheat with and without Lasergate gives clear indications of an energy deposition advantage using the Lasergate concept, as well as other observed and hypothesized benefits. While Lasergate was conceived with MagLIF in mind, the method is applicable to any laser or diagnostic application requiring direct line of sight to the interior of gas cell targets.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Detectivity enhancement in THz electrooptical sampling

We demonstrate and discuss a simple scheme that significantly enhances the detectivity of THz electro-optical sampling by introducing a sequence of Brewster windows that increases the ellipticity of the probe beam. By varying the window material or the number of Brewster windows, the enhancement factor can be adjusted; we demonstrate an enhancement factor of ≈20 with four ZnSe Brewster windows. The scheme is particularly useful when very small THz fields are to be measured in connection with low-repetition rate amplified Ti:S laser systems.

43 PARTICLE ACCELERATORS↗