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At least 19 records

Tensile properties, strain rate sensitivity, and activation volume of additively manufactured 316L stainless steels [Tensile properties of 316L stainless steels made by laser powder-bed-fusion additive manufacturing]

The tensile properties of additively manufactured (AM) metals and alloys are among the most important variables that impact the potential applications of these materials. Here we examine and report on the tensile properties of AM 316L stainless steels fabricated by the laser powder-bed-fusion (L-PBF) technique, via twelve sets of optimized laser processing parameters that produce materials with density >98.8 ± 0.10%. A heterogeneous microstructure is observed in all L-PBF samples, including microscopic features such as dislocations, cellular walls, elemental segregations, local misorientations, impurities, precipitates, and a large fraction of low-angle grain boundaries (2-10°, ~40–60%). The derived average grain size defined by high-angle grain boundaries (>10°) is ~30–50 μm. Tensile testing reveals a yield strength ranging from 552 to 635 MPa and a tensile-elongation-to-failure (TEF) of 0.09–0.42 for directly-printed samples, whereas these values are 592–690 MPa and 0.29–0.50 for samples machined from the as-built rectangular thin plates. In all samples, we observe a variation of tensile yield strength within ~15% but not the TEF, suggesting marginal microstructural changes despite a wide range of laser processing parameters. The large scatter of TEF in directly-printed samples originates from the sensitivity of thin gauge geometry (~2 mm 2 cross-section area) to the built-in flaws. We measured a substantially higher strain rate sensitivity (m~0.02–0.03) of L-PBF 316L compared to the coarse-grained counterparts (~0.006), together with a small activation volume of ~20–30b3 (where b is the Burgers vector of 316L). In conclusion, these deformation kinetics parameters suggest that the tensile plasticity of L-PBF 316L is controlled by a much finer microstructural length scale than the measured grain size, consistent with the high strength and juxtaposed nano- to macro-structures seen in these materials. Strategies to optimize the tensile properties of AM materials are discussed.

36 MATERIALS SCIENCE↗

Low and room temperatures tensile properties of a nanoprecipitate-strengthened (FeCoCr)40Ni40Al10Cu10 high-entropy alloy

Highlights: • We designed a (FeCoCr){sub 40}Ni{sub 40}Al{sub 10}Cu{sub 10} high entropy alloy (HEA) strengthened by exclusive L1{sub 2} nano-precipitates. • The present HEA exhibited excellent combination of tensile strength (~1200MPa) and elongation (~36%) at 233 K. • The coherent nano-precipitates, deformation twinning and immobile LC locks made a joint contribution to the optimal mechanical property. - Abstract: We report the tensile properties and microstructural evolution of a high entropy alloy (FeCoCr){sub 40}Ni{sub 40}Al{sub 10}Cu{sub 10} deformed at low temperature (233K) and room temperature (293 K). The alloy presented a superior combination of tensile strength (~1200 MPa) and elongation (~36%) at 233 K than at 293 K. Transmission electron microscopy revealed that the enhanced tensile properties at low temperature were due to deformation twinning, the formation of immobile Lomer-Cottrell dislocation locks, and the high density coherent nano-precipitates.

36 MATERIALS SCIENCE↗

Investigation of thermal aging effects on the tensile properties of Alloy 617 by in-situ synchrotron wide-angle X-ray scattering

The nickel-base Alloy 617 has been considered as the lead candidate structural material for the intermediate heat exchanger (IHX) of the Very-High-Temperature Reactor (VHTR). In order to assess the long-term performance of Alloy 617, thermal aging experiments up to 10,000 h in duration were performed at 1000 degrees C. Subsequently, in-situ synchrotron wide-angle X-ray scattering (WAXS) tensile tests were carried out at ambient temperature. M23C6 carbides were identified as the primary precipitates, while a smaller amount of M6C was also observed. The aging effects were quantified in several aspects: (1) macroscopic tensile properties, (2) volume fraction of the M23C6 Phase, (3) the lattice strain evolution of both the matrix and the M23C6 precipitates, and (4) the dislocation density evolution during plastic deformation. The property-microstructure relationship is described with a focus on the evolution of the M23C6 phase. For aging up to 3000 h, the yield strength (YS) and ultimate tensile strength (UTS) showed little variation, with average values being 454 MPa and 787 MPa, respectively. At 10,000 h, the YS and UTS reduced to 380 MPa and 720 MPa, respectively. The reduction in YS and UTS is mainly due to the coarsening of the M23C6 Precipitates. After long term aging, the volume fraction of the M23C6 phase reached a plateau and its maximum internal stress was reduced, implying that under large internal stresses the carbides were more susceptible to fracture or decohesion from the matrix. Finally, the calculated dislocation densities were in good agreement with transmission electron microscopy (TEM) measurements. The square roots of the dislocation densities and the true stresses displayed typical linear behavior and no significant change was observed in the alloys in different aging conditions.

Alloy 617↗

Interlaboratory round robin study on axial tensile properties of SiC-SiC CMC tubular test specimens [Interlaboratory round robin study on axial tensile properties of SiC/SiC tubes]

An interlaboratory round robin study was conducted on the tensile strength of SiC–SiC ceramic matrix composite (CMC) tubular test specimens at room temperature with the objective of expanding the database of mechanical properties of nuclear grade SiC–SiC and establishing the precision and bias statement for standard test method ASTM C1773. The mechanical properties statistics from the round robin study and the precision statistics and precision statement are presented herein. The data show reasonable consistency across the laboratories, indicating that the current C1773–13 ASTM standard is adequate for testing ceramic fiber reinforced ceramic matrix composite tubular test specimen. Furthermore, it was found that the distribution of ultimate tensile strength data was best described with a two–parameter Weibull distribution, while a lognormal distribution provided a good description of the distribution of proportional limit stress data.

36 MATERIALS SCIENCE↗

Exploring biofiber properties and their influence on biocomposite tensile properties

Biofibers serve as effective reinforcements for neat polylactic acid (PLA) in biocomposites, offering an attractive opportunity to decarbonize the manufacturing sector of the United States by displacing fossil-based reinforcement fibers such as carbon fibers. Also, biofiber production can stimulate economic growth in rural economies, fueling sustainable development. PLA resins are commonly compounded with biofibers to create biocomposites suitable for additive manufacturing. PLA-biofiber composites often exhibit better overall material properties than neat (pure) PLA, but the associations between biofiber properties and the material properties of their biocomposites remain largely unexplored. Hence, this research delves into a comprehensive exploration of diverse biofibers, scrutinizing their physical and chemical attributes, including size, shape, ash content and biochemical composition. The study meticulously analyzes the flow properties of each biofiber and elucidates the ultimate tensile strengths and Young's modulus of corresponding biocomposite samples. Noteworthy correlations between biofiber and biocomposite tensile properties are uncovered, shedding light on critical interrelationships. The study introduces an approach employing regression models to predict the ultimate tensile strength and Young's modulus of biocomposites. These models, validated with a cross-validation technique, exhibit remarkable predictive accuracy, particularly in estimating ultimate tensile strength. © 2024 Oak Ridge National Laboratory managed by UT-Battelle, LLC and The Author(s). Polymer International published by John Wiley & Sons Ltd on behalf of Society of Chemical Industry.

36 MATERIALS SCIENCE↗

Microstructure, Tensile Properties, and Corrosion Behavior of Die-Cast Mg-7Al-1Ca-xSn Alloys

The microstructure, tensile properties, and corrosion behavior of die-cast Mg-7Al-1Ca-xSn (x = 0, 0.5, 1.0, and 2.0 wt.%) alloys were studied using OM, SEM/EDS, tensile test, weight loss test, and electrochemical test. The experimental results showed that Sn addition effectively refined grains and intermetallic phases and increased the amount of intermetallic phases. Meanwhile, Sn addition to the alloys suppressed the formation of the (Mg,Al){sub 2}Ca phase and resulted in the formation of the ternary CaMgSn phase and the binary Mg{sub 2}Sn phase. The Mg-7Al-1Ca-0.5Sn alloy exhibited best tensile properties at room temperature, while Mg-7Al-1Ca-1.0Sn alloy exhibited best tensile properties at elevated temperature. The corrosion resistance of studied alloys was improved by the Sn addition, and the Mg-7Al-1Ca-0.5Sn alloy presented the best corrosion resistance.

36 MATERIALS SCIENCE↗

Effect of aging treatment on microstructures, tensile properties and intergranular corrosion behavior of Al–Cu–Li alloy

Highlights: • T8 duplex aging greatly promoted the precipitation of strengthening phases. • Heavy precipitation of strengthening phases led to enhancing of tensile properties. • Intergranular corrosion sensibility can be reduced by T8 duplex aging greatly. - Abstract: The influence of aging treatment on microstructures, tensile properties and corrosion properties of Al–Cu–Li alloy was investigated. The results show that the T8 duplex aging treatment was more effective than T6 and T8 single aging treatment in enhancing the tensile properties and improving the intergranular corrosion (IGC) resistance. Based on the microstructure observation, tensile test, electrochemical experiment and IGC measurement, the factors which affect the microstructures, tensile properties and IGC behavior changing of Al–Cu–Li alloy during aging treatments were discussed in detail.

36 MATERIALS SCIENCE↗

Effects of Laser Energies on Wear and Tensile Properties of Biomimetic 7075 Aluminum Alloy

Inspired by the non-smooth surface of certain animals, a biomimetic coupling unit with various sizes, microstructure, and hardness was prepared on the surface of 7075 aluminum alloy. Following experimental studies were conducted to investigate the wear and tensile properties with various laser energy inputs. The results demonstrated that the non-smooth surface with biomimetic coupling units had a positive effect on both the wear resistance and tensile property of 7075 aluminum alloy. In addition, the sample with the unit fabricated by the laser energy of 420.1 J/cm{sup 2} exhibited the most significant improvement on the wear and tensile properties owing to the minimum grain size and the highest microhardness. Also, the weight loss of the sample was one-third of the untreated one’s, and the yield strength, the ultimate tensile strength, and the elongation improved by 20, 20, and 34% respectively. Moreover, the mechanisms of wear and tensile properties improvement were also analyzed.

36 MATERIALS SCIENCE↗

Evolutions of the Micro- and Macrostructure and Tensile Property of Cu-15Ni-8Sn Alloy During Electromagnetic Stirring-Assisted Horizontal Continuous Casting

The present study investigates the evolution of the micro- and macrostructure and tensile property of the Cu-15Ni-8Sn (weight percent) alloy prepared by horizontal continuous casting and electromagnetic stirring (EMS). The results show that the application of EMS is beneficial for grain refinement and for microstructure transformation from the dendrite to the rosette structure and that it leads to a significant improvement in the tensile property. The forced flow induced by EMS homogenizes the temperature field ahead of the solid-liquid interface, disturbing the heat flow direction and resulting in the columnar to equiaxed transition. The grain refinement under different electromagnetic stirring frequencies is mainly derived from the homogenization of the temperature and the remelting of dendritic arms. In addition, the evolution of the tensile property with and without EMS is discussed from the perspective of fracture mode and fine-grain strengthening.

36 MATERIALS SCIENCE↗

The Effect of Boron and Zirconium on the Structure and Tensile Properties of the Cast Nickel-Based Superalloy ATI 718Plus

The effects of boron and zirconium on cast structure, hardness, and tensile properties of the nickel-based superalloy 718Plus were investigated. For this purpose, five alloys with different contents of boron and zirconium were cast via vacuum induction melting and then purified via vacuum arc remelting. Microstructural analysis by light-optical microscope and scanning electron microscope equipped with energy-dispersive x-ray spectroscopy and phase studies by x-ray diffraction analysis were performed. The results showed that boron and zirconium tend to significantly reduce dendritic arm spacing and increase the amount of Laves, Laves/gamma eutectic, and carbide phases. It was also found that boron led to the formation of B{sub 4}C and (Cr, Fe, Mo, Ni, Ti){sub 3}B{sub 2} phases and zirconium led to the formation of intermetallic phases and ZrC carbide. In the presence of boron and zirconium, the hardness and its difference between dendritic branches and inter-dendritic spaces increased by concentrating such phases as Laves in the inter-dendritic spaces. These elements had a negative effect on tensile properties of the alloy, including ductility and strength, mainly because of the increase in the Laves phase. It should be noted that the largest degradation of the tensile properties occurred in the alloys containing the maximum amount of zirconium.

36 MATERIALS SCIENCE↗

The Effect of Carboxyl Group Content on Water Uptake Capacity and Tensile Properties of Functionalized Soy Protein-Based Superabsorbent Plastics

This manuscript studies the relation between macroscopic properties of the soy protein isolate (SPI)-based superabsorbent polymers (SAP) (e.g., water uptake capacity and tensile properties) and the extent of chemical modification conducted on the protein. The increase in the carboxyl group content, obtained from electrometric titrations, for acylated systems compared to native SPI brings with it an improvement in the protein hydrophilic character, as revealed by the determination of the water imbibing capacity. SEM images show that larger porous regions were developed in the acylated plastics. As for their mechanical properties, static tensile measurements indicated that acylated plastics with greater water uptake values display higher extensibility, compared to the reference sample. These natural-based SAP materials could be appropriate for applications in which maintaining the dimensional stability during service is not crucial (e.g. in agriculture and horticulture).

36 MATERIALS SCIENCE↗

Geometric Limitation and Tensile Properties of Wire and Arc Additive Manufacturing 5A06 Aluminum Alloy Parts

Wire and arc additive manufacture (WAAM), as an emerging and promising technology of metal additive manufacturing, it lacks of experimental works to clarify the feature of geometrical configuration, microstructure and tensile properties, which can be used for further evaluating whether the as-deposited part can be used directly, and providing design reference for structure optimization. Taking 5A06 aluminum alloy additive manufacturing for example, in this paper, the geometric limitation and tensile property criteria are characterized using experimental method. The minimum angle and curvature radius that can be made by WAAM are 20° and 10 mm when the layer width is 7.2 mm. It shows isotropy when loading in build direction and perpendicular one. When loading in the direction of parallel and perpendicular to texture orientation, the tensile properties are anisotropic. The difference between them is 22 MPa.

36 MATERIALS SCIENCE↗

Dataset of tensile properties for sub-sized specimens of nuclear structural materials

Mechanical testing with sub-sized specimens plays an important role in the nuclear industry, facilitating tests in confined experimental spaces with lower irradiation levels and accelerating the qualification of new materials. The reduced size of specimens results in different material behavior at the microscale, mesoscale, and macroscale, in comparison to standard-sized specimens, which is referred to as the “specimen size effect.” Although analytical models have been proposed to correlate the properties of sub-sized specimens to standard-sized specimens, these models lack broad applicability across different materials and testing conditions. The objective of this study is to create the first large public dataset of tensile properties for sub-sized specimens used in nuclear structural materials. We performed an extensive literature review of relevant publications and extracted over 1,000 tensile testing records comprising 55 columns including material type and composition, manufacturing information, irradiation conditions, specimen dimensions, and tensile properties. The dataset can serve as a valuable resource to investigate the specimen size effect and develop computational methods to correlate the tensile properties of sub-sized specimens.

36 MATERIALS SCIENCE↗