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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Direct current magnetic Hall probe technique for measurement of field penetration in thin film superconductors for superconducting radio frequency resonators

Superconducting Radio Frequency (SRF) cavities used in particle accelerators are typically formed from or coated with superconducting materials. Currently, high purity niobium is the material of choice for SRF cavities that have been optimized to operate near their theoretical field limits. This brings about the need for significant R & D efforts to develop next generation superconducting materials that could outperform Nb and keep up with the demands of new accelerator facilities. To achieve high quality factors and accelerating gradients, the cavity material should be able to remain in the superconducting Meissner state under a high RF magnetic field without penetration of quantized magnetic vortices through the cavity wall. Therefore, the magnetic field at which vortices penetrate a superconductor is one of the key parameters of merit of SRF cavities. Techniques to measure the onset of magnetic field penetration on thin film samples need to be developed to mitigate the issues with the conventional magnetometry measurements that are strongly influenced by the film orientation and shape and edge effects. In this work, we report the development of an experimental setup to measure the field of full flux penetration through films and multi-layered superconductors. Our system combines a small superconducting solenoid that can generate a magnetic field of up to 500 mT at the sample surface and three Hall probes to detect the full flux penetration through the superconductor. We report this setup can be used to study alternative materials that could potentially outperform niobium, as well as superconductor–insulator–superconductor (SIS) multilayer coatings on niobium.

47 OTHER INSTRUMENTATION↗
DOE OSTI2022

Magnetic field mapping of superconducting radio frequency cavities

Superconducting radio frequency (SRF) cavities are the fundamental building blocks of modern particle accelerators. Niobium is the material of choice to build such cavities. These cavities require a cryogenic cool-down to ~2 ? 4 K for optimum performance minimizing RF losses on the inner cavity surface. However, temperature-independent residual losses in SRF cavities cannot be prevented entirely. One of the major sources of residual losses is trapped magnetic flux. The flux trapping mechanism depends on different factors, such as surface preparations and cool-down conditions. We have developed a diagnostic magnetic field scanning system (MFSS) using Hall probes and anisotropic magneto-resistance sensors to study the spatial distribution of trapped flux in 1.3 GHz single-cell cavities. The first result from this newly commissioned system revealed that the trapped flux on the cavity surface might redistribute with increasing RF power. The MFSS was also able to capture significant magnetic field enhancement at specific cavity locations after a quench.

Parajuli, Ishwari↗
DOE OSTI2022

High resolution diagnostic tools for superconducting radio frequency cavities

Superconducting radio-frequency (SRF) cavities are one of the fundamental building blocks of modern particle accelerators. To achieve the highest quality factors (10 10 –10 11 ), SRF cavities are operated at liquid helium temperatures. Magnetic flux trapped on the surface of SRF cavities during cool-down below the critical temperature is one of the leading sources of residual RF losses. Instruments capable of detecting the distribution of trapped flux on the cavity surface are in high demand in order to better understand its relation to the cavity material, surface treatments and environmental conditions. We have designed, developed, and commissioned two high-resolution diagnostic tools to measure the distribution of trapped flux at the surface of SRF cavities. One is a magnetic field scanning system, which uses cryogenic Hall probes and anisotropic magnetoresistance sensors that fit the contour of a 1.3 GHz cavity. This setup has a spatial resolution of ~ 13 μm in the azimuthal direction and ~ 1 cm along the cavity contour. The second setup is a stationary, combined magnetic and temperature mapping system, which uses anisotropic magnetoresistance sensors and carbon resistor temperature sensors, covering the surface of a 3 GHz SRF cavity. This system has a spatial resolution of 5 mm close to the iris and 11 mm at the equator. Initial results show a non-uniform distribution of trapped flux on the cavities’ surfaces, dependent on the magnitude of the applied magnetic field during field-cooling below the critical temperature.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2021

Magnetic field sensors for detection of trapped flux in superconducting radio frequency cavities

Superconducting radio-frequency (SRF) cavities are fundamental building block of modern particle accelerators. They operate at liquid helium temperatures 2-4 K to achieve very high quality factors 1e10-1e11. Trapping of magnetic flux within the superconductor is a significant contribution to the residual RF losses which limit the achievable quality factor. Suitable diagnostic tools are in high demand to understand the mechanisms of flux trapping in technical superconductors and the fundamental components of such diagnostic tool are magnetic field sensors. We have studied the performance of commercially available Hall probes, anisotropic magnetoresistive sensors and flux-gate magnetometers with respect to their sensitivity and capability to detect localized, low magnetic flux amplitudes, of the order of few tens of magnetic flux quantum at liquid helium temperature. Although Hall probes have the lowest magnetic field sensitivity (~96$ nV$/microT at 2 K), their physical dimensions are such that they have the ability to detect the lowest number of trapped vortices among the three type of sensors. Hall probes and anisotropic magnetoresistive sensors have been selected to be used in a setup to map regions of trapped flux on the surface of a single-cell SRF cavity.

47 OTHER INSTRUMENTATION↗
DOE OSTI2022

Key directions for research and development of superconducting radio frequency cavities

Radio frequency superconductivity is a cornerstone technology for many future HEP particle accelerators and experiments from colliders to proton drivers for neutrino facilities to searches for dark matter. While the performance of superconducting RF (SRF) cavities has improved significantly over the last decades, and the SRF technology has enabled new applications, the proposed HEP facilities and experiments pose new challenges. To address these challenges, the field continues to generate new ideas and there seems to be a vast room for improvements. In this paper we discuss the key research directions that are aligned with and address the future HEP needs.

43 PARTICLE ACCELERATORS↗
DOE OSTI2024

Role of microstructure on flux expulsion of superconducting radio frequency cavities

The trapped residual magnetic flux during the cool-down due to the incomplete Meissner state is a significant source of radio frequency losses in superconducting radio frequency cavities. Here, in this study, we clearly correlate the niobium microstructure in elliptical cavity geometry and flux expulsion behavior. In particular, a traditionally fabricated Nb cavity half-cell from an annealed poly-crystalline Nb sheet after an 800 °C heat treatment leads to a bi-modal microstructure that ties in with flux trapping and inefficient flux expulsion. This non-uniform microstructure is related to varying strain profiles along the cavity shape. A novel approach to prevent this non-uniform microstructure is presented by fabricating a 1.3 GHz single cell Nb cavity with a cold-worked sheet and subsequent heat treatment leading to better flux expulsion after 800 °C/3 h. Microstructural evolution by electron backscattered diffraction-orientation imaging microscopy on cavity cutouts, and flux pinning behavior by dc-magnetization on coupon samples confirms a reduction in flux pinning centers with increased heat treatment temperature. The heat treatment temperature-dependent mechanical properties and thermal conductivity are reported. The significant impact of cold work in this study demonstrates clear evidence for the importance of the microstructure required for high-performance superconducting cavities with reduced losses caused by magnetic flux trapping.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2023

Electropolishing parameters study for surface smoothening of low-$\beta$650 MHz five-cell niobium superconducting radio frequency cavity

Electropolishing (EP) is applied to niobium (Nb) superconducting radio frequency (SRF) cavities, which are used in particle accelerators for their surface treatment. The EP process for 1.3 GHz cavities has been extensively studied earlier. In this work, a parametric study on EP of low-β (0.61) 650 MHz Nb SRF cavities (LB650), which will be used in pre-production cryomodule for proton improvement plan-II (PIP-II) linear accelerator, was conducted to determine adequate EP conditions for attaining a smooth surface of the cavities. EP performed with the standard parameters and an initial cathode (cathode-I) having a cathode surface area of ~5% of the cavity surface area yielded a rough equator surface of the cavity. The grain step height on the equator weld position was measured to be ~ 32 μm. The rough surface was attributed to preferential grain etching confirmed by a polarization curve showing a linear relationship between the EP current and voltage and the absence of the current plateau region. The cathode was modified to make its surface area twice that of cathode-I. The modified cathode (cathode-M) provided a current plateau region in the corresponding I-V curves measured at different cavity temperatures. The onset voltage for the plateau was found to be higher at higher cavity temperatures. Here this study revealed that even with cathode-M, the standard 18 V was low for EP of such large-sized cavities when the cavity temperature was 18 °C. EP performed at a higher voltage of 22–24.5 V with cathode-M yielded a smooth surface with a grain step height of only 0.6 μm. The applied EP conditions also improved removal uniformity along the cavity length. In contrast to the cavity treated with cathode-I, the cavities treated with cathode-M achieved a significantly higher accelerating gradient (E acc ) in vertical tests conducted in a cryostat at 2 K. The modified EP was found efficient to produce the cavities that achieved E acc of 22.4 MV/m, required by PIP II project in the baseline RF tests, to qualify for further surface processing used to enhance their quality factors.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2022

MAGNETIC FIELD MAPPING OF 1.3 GHz SUPERCONDUCTING RADIO FREQUENCY NIOBIUM CAVITIES

Niobium is the material of choice to build superconducting radio frequency (SRF) cavities, which are fundamental building blocks of modern particle accelerators. These cavities require a cryogenic cool-down to ~2 - 4 K for optimum performance minimizing RF losses on the inner cavity surface. However, temperature-independent residual losses in SRF cavities cannot be prevented entirely. One of the significant contributor to residual losses is trapped magnetic flux. The flux trapping mechanism depends on different factors, such as surface preparations and cool-down conditions. We have developed a diagnostic magnetic field scanning system (MFSS) using Hall probes and anisotropic magneto-resistance sensors to study the spatial distribution of trapped flux in 1.3 GHz single-cell cavities. The first result from this newly commissioned system revealed that the trapped flux on the cavity surface might redistribute with increasing RF power. The MFSS was also able to capture significant magnetic field enhancement at specific cavity locations after a quench.

Parajuli, I. P.↗
DOE OSTI2024

Field, frequency, and temperature dependencies of the surface resistance of nitrogen diffused niobium superconducting radio frequency cavities

We investigate the rf performance of several single-cell superconducting radio-frequency cavities subjected to low temperature heat treatment in nitrogen environment. The cavities were treated at temperature 120 – 165 ° C for an extended period of time (24–48 h) either in high vacuum or in a low partial pressure of ultrapure nitrogen. The improvement in Q 0 with a Q rise was observed when nitrogen gas was injected at ∼ 300 ° C during the cavity cooldown from 800 ° C and held at 165 ° C , without any degradation in accelerating gradient over the baseline performance. The treatment was applied to several elliptical cavities with frequency ranging from 0.75 to 3.0 GHz, showing an improved quality factor as a result of low temperature nitrogen treatments. The Q rise feature is similar to that achieved by nitrogen alloying Nb cavities at higher temperature, followed by material removal by electropolishing. The surface modification was confirmed by the change in electronic mean free path and tuned with the temperature and duration of heat treatment. The decrease of the temperature-dependent surface resistance with increasing rf field, resulting in a Q rise, becomes stronger with increasing frequency and decreasing temperature. The data suggest a crossover frequency of ∼ 0.95 GHz above that the Q rise phenomenon occurs at 2 K. Some of these results can be explained qualitatively with an existing model of intrinsic field-dependence of the surface resistance with both equilibrium and nonequilibrium quasiparticle distribution functions. The change in the Q slope below 0.95 GHz may result from masking contribution of trapped magnetic flux to the residual surface resistance. Published by the American Physical Society 2024

43 PARTICLE ACCELERATORS↗
DOE OSTI2022

Experiments On A Conduction Cooled Superconducting Radio Frequency Cavity With Field Emission Cathode

To achieve Ampere-class electron beam accelerators the pulse delivery rate need to be much higher than the typical photo injector repetition rate of the order of a few kilohertz. We propose here an injector which can, in principle, generate electron bunches at the same rate as the operating RF frequency. A conduction-cooled superconducting radio frequency (SRF) cavity operating in the CW mode and housing a field emission element at its region of high axial electric field can be a viable method of generating high-repetition-rate electron bunches. In this paper, we report the development and experiments on a conduction-cooled Nb3Sn cavity with a niobium rod intended as a field emitter support. The initial experiments demonstrate 0.4 MV/m average accelerating gradient, which is equivalent of peak gradient of 3.2 MV/m. The measured RF cavity quality factor is 1.4 x 10$^8$ slightly above our goal. The achieved field gradient is limited by the relatively low input RF power and by the poor coupling between the external power supply and the RF cavity. With ideal coupling the field gradient can be as high as 0.6 MV/m still below our goal of about 1 MV/m.

43 PARTICLE ACCELERATORS↗
DOE OSTI2023

QUENCH DETECTION IN A SUPERCONDUCTING RADIO FREQUENCY CAVITY WITH COMBINED TEMPERATURE AND MAGNETIC FIELD MAPPING

Local dissipation of RF power in superconducting radio frequency cavities create so called "hot-spots", primary precursors of cavity quench driven by either thermal or magnetic instability. These hot-spots are detected by a temperature mapping system, and a large increase in temperature on the outer surface is detected during cavity quench events. Here, we have used combined magnetic and temperature mapping systems using anisotropic magneto-resistance (AMR) sensors and carbon resisters to locate the hot spots and areas with high trapped flux on a 3.0 GHz single-cell Nb cavity during the RF tests at 2.0 K. The quench location and hot spots were detected near the equator when the residual magnetic field in the Dewar is kept < 1 mG. The hot spots and quench locations moved when the magnetic field is trapped locally, as detected by T-mapping system. No significant dynamics of trapped flux is detected by AMR sensors, however change in magnetic flux during cavity quench is detected by a flux gate magnetometer, close to the quench location. The result provide the direct evidence of hot spots and quench events due to localized trapped vortices.

Ciovati, Gianluigi↗
DOE OSTI2022

Effect of duration of 120 oC baking on the performance on superconducting radio frequency niobium cavities

Over the last decade much attention was given in increasing the quality factor of superconducting radio frequency (SRF) cavities by impurity doping. Prior to the era of doping, the final cavity processing technique to achieve the high accelerating gradient includes the ?in situ? low temperature baking of SRF cavities at temperature ~ 120 oC for several hours. Here, we present the results of a series of measurements on 1.3 GHz TESLA shape single-cell cavities with successive low temperature baking at 120 oC up to 96 hours. The experimental data were analyzed with available theory of superconductivity to elucidate the effect of the duration of low temperature baking on the superconducting properties of cavity materials as well as the rf performance. In addition, the rf loss related to the trapping of residual magnetic field refereed as flux trapping sensitivity was measured with respect to the duration of 120 oC bake.

Khanal, B. D.↗
DOE OSTI2023

Analysis of furnace contamination on superconducting radio frequency niobium using secondary-ion mass spectrometry

Detection of surface contamination on niobium materials used in superconducting radio frequency (SRF) applications is difficult due to quantitative sensitivity and near-atomic depth resolution needed. Inspection of samples known to have experienced surface contamination was found to have inconsistent nitride coverage after high-temperature nitrogen gas exposure (“doping”). Here we compare contaminating species found on samples treated in several different vacuum furnaces, both “exposed” directly in the chamber and “protected” by containment shielding from evaporative sources with “furnace caps.” Typically, furnace caps are used to impede contamination from reaching the interior surface of cavities during the high-temperature vacuum bake that immediately precedes exposure to nitrogen gas. Although, to date, little is known about the effectiveness of these caps, SIMS results showed that they were effective in limiting contamination arising from the furnace environment. Inspection of sample surfaces by SEM showed a lack of nitrides present on contaminated specimens. TEM with energy dispersive spectroscopy performed on these samples revealed that a carbon-rich layer now existed, indicating that a relatively high contaminant load prevents the nucleation and growth of surface nitrides, while thus inhibiting interstitial nitrogen uptake. Except in extreme cases, subsequent removal of the top several micrometers of the surface via electropolishing appears to effectively eliminate any strong influence on the subsequent SRF cavity performance. With the absence of furnace cleaning, carbon contamination was found to be nearly 10× higher for protected nitrogen-doped and electropolished samples, with minimal metallic contamination detected for both processes. SIMS analysis was also performed to compare the cleanliness of samples fully prepared by such nitrogen “doping” with those prepared by a related process, involving the dissolution of niobium surface oxide and diffusion of oxygen into the surface. This oxygen doping or alloying process offers attractive advantages.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2022

Higgs-Energy LEptoN (HELEN) Collider based on advanced superconducting radio frequency technology

This Snowmass 2021 contributed paper discusses a Higgs-Energy LEptoN (HELEN) e⁺e⁻ linear collider based on advances superconducting radio frequency technology. The proposed collider offers cost and AC power savings, smaller footprint (relative to the ILC), and could be built at Fermilab with an Interaction Region within the site boundaries. After the initial physics run at 250 GeV, the collider could be upgraded either to higher luminosity or to higher (up to 500 GeV) energies. If the ILC could not be realized in Japan in a timely fashion, the HELEN collider would be a viable option to build a Higgs factory in the U.S.

43 PARTICLE ACCELERATORS↗
DOE OSTI2023

Superconducting radio frequency linear collider HELEN

This article discusses a proposed Higgs-Energy LEptoN (HELEN) $e^+e^-$ linear collider based on advanced traveling wave superconducting radio frequency technology. Here, the proposed collider offers cost and AC power savings, smaller footprint (relative to the ILC), and could be built at Fermilab. After the initial physics run at 250 GeV, the collider could be upgraded either to higher luminosity or to higher, up to 500 GeV, energies.

43 PARTICLE ACCELERATORS↗
DOE OSTI2022

Effect of successive heat treatment on the performance of superconducting radio frequency niobium cavities

One of the primary sources of radio frequency residual losses leading to lower quality factor is trapped residual magnetic field during the cooldown of superconducting radio frequency cavities. It has been reported that non-uniform recrystallization of niobium cavities after the post fabrication heat treatment leads to higher flux trapping during the cooldown, and hence the lower quality factor. Here, we fabricated two 1.3 GHz single cell cavities from high purity fine grain niobium and processed with successive heat treatments in the range 800-1000 ?C to measure the flux expulsion and flux trapping sensitivity. The results show the improved flux expulsion with increase in heat treatment temperature and flux trapping sensitivity depends on the final surface preparation prior to the rf test.

Khanal, Bashu↗
DOE OSTI2024

Method and apparatus for removal of microscopic contaminant particulates from superconducting radio frequency cavities and cavity strings

A method and apparatus for removing microscopic contaminant particulates by high pressure liquid nitrogen jet cleaning from the inner surface of a superconducting radio frequency cavity or a string of multiple cavities and transporting the removed particulates out of the inner space enclosed by the cleaned surfaces. The cleaning method of the invention suppresses field emission, resulting in an increase of the usable accelerating gradient of the cavities and a reduction of the activated radioactivity in accelerator components around cavities.

Geng, Rongli↗
DOE OSTI2023

Evaluation of predictive correlation between flux expulsion and grain growth for superconducting radio frequency cavities

Abstract A series of experiments were carried out in an effort to develop a simple method for predicting the magnetic flux expulsion behavior of high purity niobium used to fabricate superconducting radio frequency (SRF) cavities. Using conventional metallographic characterizations in conjunction with high spatial resolution electron backscattered diffraction-orientation imaging microscopy, we find that the flux expulsion behavior of 1.3 GHz single cell SRF Nb cavities is significantly associated with the grain growth of the Nb material during heat treatment. Most of the Nb grains rapidly grew during 900 °C heat treatment, and were likely full-recrystallized with 1000 °C HT. When compared to the magnetic flux expulsion ratio ( B sc / B nc ) at Δ T = 5 K, the flux expulsion efficiency of the cavities increases with the increase of grain size. Most interestingly, 900 °C HT shows a roughly linear trend that suggests that this criterion could be used to predict the appropriate heat treatment temperature for sufficient flux expulsion behavior in SRF-grade Nb. This result can be used to see if flux expulsion can be predicted by examining the materials coming from Nb vendors, prior to cavity fabrication.

43 PARTICLE ACCELERATORS↗