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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

A high transmission tender X-ray monochromator employing a matched pair of multilayer grating and mirror

It is now well established that multilayer coated gratings may offer high diffraction efficiencies over the tender X-ray range, from about 1 keV to 5 keV, covering the gap between single layer coated grating monochromators and crystal monochromators. Nevertheless, few beamlines in the world are using such gratings in their monochromator. The successful implementation of a multilayer grating monochromator requires producing a matched pair of a multilayer grating and a multilayer mirror, and this matching is not straightforward as it must account for different incidence angles and refraction effects on each element. Here we review the realization of the multilayer grating monochromator of the SIRIUS beamline which has been successfully in service for several years. We show how, by alternating computer simulation with our diffraction code and measurements, we could optimize the monochromator transmission on a very wide energy range. After the grating was coated, it was found that the angle of optimal efficiency versus photon energy was significantly different from what was predicted by a simple conformal model of binary layers. Layer interdiffusion and profile smoothing during the deposition process must be added to the multilayer model to reproduce the measured data. The critical adjustment of the mirror multilayer period is achieved by the lateral translation of the mirror, which was given a small transverse period gradient. The monochromator is thus providing high transmission efficiency in the 1 to 5 keV energy range, more than 30% over 2.5 keV and up to 46% at 4.6 keV.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
NASA NTRS1992

Multilayer Monochromator For Hard X Rays And Gamma Rays

Compact monochromator for hard x rays and gamma rays provides high spectral resolution with high throughput. Resembles instruments in "Compact X-Ray and Extreme-Ultraviolet Monochromator" (MFS-28499), "Scanning X-Ray or Extreme-Ultraviolet Monochromator" (MFS-28492), "Ultra-High-Spectral-Resolution X-Ray/EUV Monochromator" (MFS-28500), and "Four-Mirror X-Ray and Extreme-Ultraviolet Monochromator" (MFS-28498). Operates on principle of multilayer Bragg reflector. Used in nuclear, astronomical, and biomedical research, x-ray crystallography, research on processing materials, research in x-ray lasers, and x-ray lithography.

Hoover, Richard B.↗
NASA NTRS1998

On the Use of Monochromators for the Calibration of AXAF

Data acquired, during the AXAF calibration at MSFC's X-Ray Calibration Facility (XRCF), using monochromators requires special analysis owing to potentially large spatial variations in the monochromators' beams and to higher-order contributions to the spectral content. A description of the monochromators -- the Double-Crystal Monochromator (DCM) and the HIgh-Resolution Erect-Field Spectrometer (HIREFS\TM) reflection-grating monochromator --- is given, followed by a discussion of the spectral and spatial content as monitored by Beam-Normalization Detector (BND) flow proportional counters (FPCs). Emphasis is given to the methodology employed in determining the spatial content through fits to Beam Uniformity (BU) measurements made nonsimultaneously, either during calibration or during pre-calibration source characterization. We present an interpolation scheme which adequately represents the beam properties over a wide range of source conditions.

Swartz, Douglas A.↗
NASA NTRS1990

Determination of washout performance of various monochrome displays under simulated flight ambient and solar lighting conditions

The aircraft cockpit ambient lighting simulation system (ACALSS) has been developed to study display readability and associated pilot/vehicle performance effects in a part-task simulator cockpit. In the study reported here, the ACALSS was used to determine the illumination levels at which subjects lose the ability to maintain aircraft states when using three display technologies as display media for primary flight displays: a standard monochrome EL (electroluminescent) flat-panel, a laboratory-class monochrome CRT, and an enhanced-brightness EL flat-panel. The multivariate statistical technique of modified profile analysis was used to test for performance differences between display devices as functions of illumination levels. The standard monochrome EL flat-panel display began to washout after the 2500 foot-candle level of illumination. The monochrome CRT began to washout after the 5500 foot-candle level of illumination. No performance decrements by increased illumination up to the 12,000 foot-candle level were found for the enhanced-brightness EL flat-panel display. What was not anticipated was that half the subjects would subjectively prefer the CRT over the enhanced-brightness EL, even though their performance errors would have indicated the opposite.

Batson, Vernon M.↗
NASA NTRS2005

High-Resolution Electron Energy-Loss Spectroscopy (HREELS) Using a Monochromated TEM/STEM

A 200 keV FEI TF20 XT monochromated (scanning) transmission electron microscope funded by NASA's SRLIDAP program is undergoing installation at Lawrence Livermore National Laboratory. Instrument specifications in STEM mode are Cs =1.0 mm, Cc =1.2 mm, image resolution =0.18 nm, and in TEM mode Cs =1.3 mm, Cc =1.3 mm, information limit =0.14 nm. Key features of the instrument are a voltage-stabilized high tension (HT) supply, a monochromator, a high-resolution electron energy-loss spectrometer/energy filter, a high-resolution annular darkfield detector, and a solid-state x-ray energy-dispersive spectrometer. The high-tension tank contains additional sections for 60Hz and high frequency filtering, resulting in an operating voltage of 200 kV plus or minus 0.005V, a greater than 10-fold improvement over earlier systems. The monochromator is a single Wien filter design. The energy filter is a Gatan model 866 Tridiem-ERS high resolution GIF spec d for less than or equal to 0.15 eV energy resolution with 29 pA of current in a 2 nm diameter probe. 0.13 eV has already been achieved during early installation. The x-ray detector (EDAX/Genesis 4000) has a take-off angle of 20 degrees, an active area of 30 square millimeters, and a solid angle of 0.3 steradians. The higher solid angle is possible because the objective pole-piece allows the detector to be positioned as close as 9.47 mm from the specimen. The voltage-stabilized HT supply, monochromator and GIF enable high-resolution electron energy-loss spectroscopy (HREELS) with energy resolution comparable to synchrotron XANES, but with approximately 100X better spatial resolution. The region between 0 and 100 eV is called the low-loss or valence electron energy-loss spectroscopy (VEELS) region where features due to collective plasma oscillations and single electron transitions of valence electrons are observed. Most of the low-loss VEELS features we are detecting are being observed for the first time in IDPs. A major focus of our research is to understand the origin and significance of these features and how they might be exploited to gain insight about IDPs and other meteoritic materials.

Sai, Z. R.↗
NASA NTRS1988

A monochromator based on W/C multilayers of 40 A layer spacing

The design and preliminary performance data are presented for a monochromator based on two multilayer X-ray mirrors. The monochromator is based on mirrors with a d-spacing of 40 A and is designed to operate in the 5-75 A wavelength regime which can be varied by interchanging the mirrors with ones of different d-spacing. The multilayer mirrors are fabricated using sputter deposition and typically consist of 40 layer pairs of W and C. Except for W/Si, which shows 1-2 percent better reflectivities over the 7-40 A range but 4-10 percent poorer reflectivities for wavelengths longer than 40 A and shorter than 7 A, calculations performed using other combinations of materials generally show poorer reflectivities over the wavelength range of interest. Plans for a four-mirror version of the monochromator that will have increased resolution are also presented.

Smith, A.↗
NASA NTRS1991

Four-Mirror X-Ray And Extreme-Ultraviolet Monochromator

More mirrors provide additional wavelength selectivity. Four-mirror x-ray and extreme-ultraviolet monochromator provides narrower wavelength passband than devices described in "Compact X-Ray and Extreme Ultraviolet Monochromator" (MFS-28499) and "Scanning X-Ray or Extreme Ultraviolet Monochromator" (MFS-28492). Relies on Bragg reflection from two identical parallel multilayer mirrors to extract narrow-spectrum x-ray or extreme-ultraviolet beam from broad-spectrum input beam.

Hoover, Richard B.↗
NASA NTRS1972

Helium window for shock-tube monochromators

Technique for coupling vacuum ultraviolet monochromator to shock tube to avoid loss of high energy ultraviolet light during quantitative measurements is described. System consists of helium gas window pumping through small aperture in entrance pupil of monochromator. Diagram of equipment and principles of operation are presented.

Thomas, G. M.↗
NASA NTRS1978

Tunable VUV photofragment monochromator

A versatile tunable VUV photofragment monochromator is described. The instrument uses a unique flashlamp and a single slit monochromator to produce the photofragments. A tunable dye laser is used to detect these fragments via laser induced fluorescence. The results of preliminary design parameter measurements are presented along with the first photofragment spectra obtained with this instrument. It is shown that the SNR is adequate to assign single quantum state photofragment distributions.

Miller, G. E.↗
NASA NTRS1979

Portable high-resolution laser monochromator-interferometer with multichannel electronic readout

A high-resolution 0.4-m monochromator is described for use in wavelength diagnosis of tunable pulsed and CW laser sources in the 3000-10,000-A region. The f/20 design uses an echelle grating in an over-and-under Ebert configuration with a scanned photodiode array to provide a real-time multichannel display of spectral output. Absolute wavelength may be determined to 0.1 A with the monochromator, and a Fabry-Perot interferometer attachment extends linewidth measurement capability to 0.01 A or better. Spectra are displayed on a storage oscilloscope, and calculation of laser parameters is explained. The instrument measures 70 cm long x 15 cm wide x 20 cm high.

Morris, M. B.↗
NASA NTRS1991

Scanning X-Ray Or Extreme-Ultraviolet Monochromator

Wavelength of peak transmission of proposed high-throughput, narrow-band-pass x-ray or extreme-ultraviolet monochromator continuously adjustable. Essential filtering and reflecting components designed according to principles described in "Compact X-Ray and Extreme-Ultraviolet Monochromator" (MFS-28499). However, angle of incidence varied to change wavelength of Bragg reflection.

Hoover, Richard↗
DOE OSTI2025

Reducing heat load density with asymmetric and inclined double-crystal monochromators: principles and requirements revisited

Asymmetric double-crystal monochromators (aDCMs) and inclined DCMs (iDCMs) can significantly expand the X-ray beam footprint and consequently reduce the heat load density and gradient. Based on rigorous dynamical theory calculations, the major principles and properties of aDCMs and iDCMs are presented to guide their design and development, particularly for fourth-generation synchrotrons. In addition to the large beam footprint, aDCMs have very large bandwidths (up to ∼10 eV) and angular acceptance, but the narrow angular acceptance of the second crystal requires precise control of the relative orientations and strains. Based on Fourier coupled-wave diffraction theory calculations, it is rigorously proved that the iDCM has almost the same properties as the conventional symmetric DCM, including the efficiency, angular acceptance, bandwidth, tuning energy range and sensitivity to misalignment. The exception is that, for the extremely inclined geometry that can achieve very large footprint expansion, the iDCM has (beneficially) a larger bandwidth and wider angular acceptance. Inclined diffraction has the `rho-kick effect' that can be cancelled by the second reflection of the iDCM (even with misalignment), except that inhomogeneous strains may cause non-uniform rho-kick angles. At present, fabrication/mounting-induced strains pose low risk since they can be controlled to <0.5 µrad over large areas. The only uncertain challenge is the thermally induced strains, yet it is estimated that these strains are naturally lowered by the large footprint and may be further mitigated by optimized cryogenic cooling to the 1–2 µrad level. Overall, aDCMs and iDCMs have more stringent requirements than normal DCMs, but they are feasible schemes in practice.

asymmetric monochromator↗
DOE OSTI2026

Twist-Angle-Dependent Excitons in Moiré MoTe 2 Visualized by Cryogenic STEM and Monochromated EELS

van der Waals twisted bilayers of transition-metal dichalcogenides exhibit diverse excitonic phenomena arising from moiré superlattices and lattice reconstruction. While interlayer strain and relaxation reshape their electronic bands, their nanoscale influence on the excitonic fine structure remains poorly understood. Here, we study the interplay between spin–orbit coupling (SOC) and the moiré lattice by probing excitons in H-type twisted (∼8-layer × 8-layer) MoTe 2 using atomic-resolution scanning transmission electron microscopy (STEM) combined with monochromated electron energy loss spectroscopy (EELS) at cryogenic temperature. Spatially resolved spectra reveal moiré-site-dependent variations in excitonic absorption, including modulation of the X B exciton across the moiré unit cell. We find that SOC in MoTe 2 increases with the twist angle within the studied range (2–4.5°), with the largest value observed at 4°. Furthermore, these findings establish the twist angle as a tunable parameter for SOC via moiré engineering and link local structural relaxation to excitonic fine structure in twisted MoTe 2 .

cryogenic STEM/EELS↗