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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS2003

Silicon Carbide High Temperature Anemometer and Method for Assembling the Same

A high temperature anemometer includes a pair of substrates. One of the substrates has a plurality of electrodes on a facing surface, while the other of the substrates has a sensor cavity on a facing surface. A sensor is received in the sensor cavity, wherein the sensor has a plurality of bondpads, and wherein the bond pads contact the plurality of electrodes when the facing surfaces are mated with one another. The anemometer further includes a plurality of plug-in pins, wherein the substrate with the cavity has a plurality of trenches with each one receiving a plurality of plug-in pins. The plurality of plug-in pins contact the plurality of electrodes when the substrates are mated with one another. The sensor cavity is at an end of one of the substrates such that the sensor partially extends from the substrate. The sensor and the substrates are preferably made of silicon carbide.

Okojie, Robert S.↗
NASA NTRS2002

Alternative Processing Methods for Ultra High Temperature Ceramics

Ultra High Temperature Ceramics (UHTCs) are being developed for possible use in a number of structural applications including hypersonic vehicles, engines, plasma arc electrodes and high temperature shielding. Alternative methods of processing Ultra High Temperature Ceramics (UHTCs) will be discussed. Techniques that may improve oxidation resistance, strength, and reduce the processing temperature of the UHTCs will be presented. Hot-pressed UHTCs made using either milled/uncoated powders or non-milled coated powders will be compared.

Gusman, Michael↗
NASA NTRS2002

Theory and Simulation of A Novel Viscosity Measurement Method for High Temperature Semiconductor

The properties of molten semiconductors are good indicators for material structure transformation and hysteresis under temperature variations. Viscosity, as one of the most important properties, is difficult to measure because of high temperature, high pressure, and vapor toxicity of melts. Recently, a novel method was developed by applying a rotating magnetic field to the melt sealed in a suspended quartz ampoule, and measuring the transient torque exerted by rotating melt flow on the ampoule wall. The method was designed to measure viscosity in short time period, which is essential for evaluating temperature hysteresis. This paper compares the theoretical prediction of melt flow and ampoule oscillation with the experimental data. A theoretical model was established and the coupled fluid flow and ampoule torsional vibration equations were solved numerically. The simulation results showed a good agreement with experimental data. The results also showed that both electrical conductivity and viscosity could be calculated by fitting the theoretical results to the experimental data. The transient velocity of the melt caused by the rotating magnetic field was found reach equilibrium in about half a minute, and the viscosity of melt could be calculated from the altitude of oscillation. This would allow the measurement of viscosity in a minute or so, in contrast to the existing oscillation cup method, which requires about an hour for one measurement.

Lin, Bochuan↗
NASA NTRS1991

Superelement methods in high temperature metal matrix composites

A study into fiber fracture and debonding in metal matrix composites is conducted using the finite element method. The superelement finite element technique was used to model a metal matrix composite under various loading condition and with varying degrees of fiber debonding. The use of superelement saved many man hours by allowing for alteration of only the primary superelement to manipulate partial bonding for the entire model. The composite's material properties were calculated and the effects of fiber debonding on these properties were noted. The internal stress state of the composite while under various loads was also studied. Special interest was devoted to the change in stress state as a result of increasing fiber debonding.

Trowbridge, Daniel↗
NASA NTRS1983

Application of the Parker flash method to high temperature thermoelectrics

Mathematical aspects of thermal diffusivity measurements are reviewed and applied to develop an experimental setup at JPL. Certain approximations commonly appearing in the literature are examined in some detail and rejected based upon sensitive slope variations having significant impact on the results. The final mathematical formulation used was one developed by Parker et al. (1961), which evaluated the diffusivity in a way that could be simply evaluated by examining an oscilloscope trace. A computer algorithm was written to examine solution sensitivity to the number of terms taken in the infinite series. The mathematical technique is being used at JPL to evaluate diffusivities of graphite, Boron Carbon and Lanthanum Sulphur compounds in the temperature range of 300 K to 1200 K.

Noon, E. L.↗
NASA NTRS1998

Deterministic and Probabilistic Creep and Creep Rupture Enhancement to CARES/Creep: Multiaxial Creep Life Prediction of Ceramic Structures Using Continuum Damage Mechanics and the Finite Element Method

High temperature and long duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. A previous model advanced by the authors described a methodology by which the creep rupture life of a loaded component can be predicted. That model was based on the life fraction damage accumulation rule in association with the modified Monkman-Grant creep ripture criterion However, that model did not take into account the deteriorating state of the material due to creep damage (e.g., cavitation) as time elapsed. In addition, the material creep parameters used in that life prediction methodology, were based on uniaxial creep curves displaying primary and secondary creep behavior, with no tertiary regime. The objective of this paper is to present a creep life prediction methodology based on a modified form of the Kachanov-Rabotnov continuum damage mechanics (CDM) theory. In this theory, the uniaxial creep rate is described in terms of stress, temperature, time, and the current state of material damage. This scalar damage state parameter is basically an abstract measure of the current state of material damage due to creep deformation. The damage rate is assumed to vary with stress, temperature, time, and the current state of damage itself. Multiaxial creep and creep rupture formulations of the CDM approach are presented in this paper. Parameter estimation methodologies based on nonlinear regression analysis are also described for both, isothermal constant stress states and anisothermal variable stress conditions This creep life prediction methodology was preliminarily added to the integrated design code CARES/Creep (Ceramics Analysis and Reliability Evaluation of Structures/Creep), which is a postprocessor program to commercially available finite element analysis (FEA) packages. Two examples, showing comparisons between experimental and predicted creep lives of ceramic specimens, are used to demonstrate the viability of this methodology and the CARES/Creep program.

Jadaan, Osama M.↗
NASA NTRS1985

Test method development for structural characterization of fiber composites at high temperatures

Test methods used for structural characterization of polymer matrix composites can be applied to glass and ceramic matrix composites only at low temperatures. New test methods are required for tensile, compressive, and shear properties of fiber composites at high temperatures. A tensile test which should be useful to at least 1000 C has been developed and used to characterize the properties of a Nicalon/glass composite up to the matrix limiting temperature of 600 C. Longitudinal and transverse unidirectional composite data are presented and discussed.

Mandell, J. F.↗
NASA NTRS2014

Methods for Producing High-Performance Silicon Carbide Fibers, Architectural Preforms, and High-Temperature Composite Structures

Methods are disclosed for producing architectural preforms and high-temperature composite structures containing high-strength ceramic fibers with reduced preforming stresses within each fiber, with an in-situ grown coating on each fiber surface, with reduced boron within the bulk of each fiber, and with improved tensile creep and rupture resistance properties tier each fiber. The methods include the steps of preparing an original sample of a preform formed from a pre-selected high-strength silicon carbide ceramic fiber type, placing the original sample in a processing furnace under a pre-selected preforming stress state and thermally treating the sample in the processing furnace at a pre-selected processing temperature and hold time in a processing gas having a pre-selected composition, pressure, and flow rate. For the high-temperature composite structures, the method includes additional steps of depositing a thin interphase coating on the surface of each fiber and forming a ceramic or carbon-based matrix within the sample.

DiCarlo, James A.↗
NASA NTRS2016

Systems and Methods for Implementing High-Temperature Tolerant Supercapacitors

Systems and methods in accordance with embodiments of the invention implement high-temperature tolerant supercapacitors. In one embodiment, a high-temperature tolerant super capacitor includes a first electrode that is thermally stable between at least approximately 80C and approximately 300C; a second electrode that is thermally stable between at least approximately 80C and approximately 300C; an ionically conductive separator that is thermally stable between at least approximately 80C and 300C; an electrolyte that is thermally stable between approximately at least 80C and approximately 300C; where the first electrode and second electrode are separated by the separator such that the first electrode and second electrode are not in physical contact; and where each of the first electrode and second electrode is at least partially immersed in the electrolyte solution.

Brandon, Erik J.↗
NASA NTRS1988

Computational Methods For Composite Structures

Selected methods of computation for simulation of mechanical behavior of fiber/matrix composite materials described in report. For each method, report describes significance of behavior to be simulated, procedure for simulation, and representative results. Following applications discussed: effects of progressive degradation of interply layers on responses of composite structures, dynamic responses of notched and unnotched specimens, interlaminar fracture toughness, progressive fracture, thermal distortions of sandwich composite structure, and metal-matrix composite structures for use at high temperatures. Methods demonstrate effectiveness of computational simulation as applied to complex composite structures in general and aerospace-propulsion structural components in particular.

Chamis, Christos C.↗
NASA NTRS1988

Reaction kinetics between fiber and matrix

Interdiffusion and interdiffusion controlled intermediate phase formation in metal matrix composites can be of interest for the prolonged application of these systems at high temperatures. Methods are discussed that address the kinetics of interdiffusion in systems that exhibit solid solution intermixing or the formation of a third intermediate phase at the fiber/matrix interface, or both. The tungsten fiber reinforced niobium and tungsten fiber reinforced superalloy systems are employed as model systems for experimentation and discussion. In an effort to impede interdiffusion, the concept of ion implanted diffusion barriers have been examined. Preliminary results on the feasibility and effectiveness of ion implanted diffusion barriers are presented.

Kopp, M. W.↗
NASA NTRS1999

On the Use of Accelerated Aging Methods for Screening High Temperature Polymeric Composite Materials

A rational approach to the problem of accelerated testing of high temperature polymeric composites is discussed. The methods provided are considered tools useful in the screening of new materials systems for long-term application to extreme environments that include elevated temperature, moisture, oxygen, and mechanical load. The need for reproducible mechanisms, indicator properties, and real-time data are outlined as well as the methodologies for specific aging mechanisms.

Gates, Thomas S.↗
NASA NTRSDate not supplied

High-Temperature Mechanical Tensile Testing of Unidirectional Sic/Sic Composites Using A Versatile Lamp Furnace

Silicon carbide (SiC) based ceramic matrix composites (CMCs) are of interest for high-temperature structural applications, including use in turbine engine components. To understand damage mechanisms and predict durability of these systems, in-depth knowledge of their behavior at ambient and high temperatures is necessary. A method for high temperature testing of SiC/SiC minicomposite specimens up to 1500oC in both tensile fast fracture and creep conditions to investigate their thermomechanical behavior will be presented. This method utilizes a novel radiation heat furnace, equipped with infrared lamps with ellipsoidal reflectors, to heat the specimen at the furnace center in user-defined atmospheres. The housing structure of the lamps allows for observation of the specimen during testing using optical methods and for conducting other experimental studies. The goal is to employ nondestructive health monitoring techniques in-situ, including acoustic emission (AE), electrical resistance (ER), and digital image correlation (DIC) to evaluate damage initiation and evolution in the minicomposite specimens during tensile testing. Results from mechanical testing and nondestructive techniques will be presented. Electron microscopy and X-ray micro-computed tomography were used to further characterize specimen damage after testing.

Aeronautics↗
NASA NTRS1998

Single-Transducer, Ultrasonic Imaging Method for High-Temperature Structural Materials Eliminates the Effect of Thickness Variation in the Image

NASA Lewis Research Center's Life Prediction Branch, in partnership with Sonix, Inc., and Cleveland State University, recently advanced the development of, refined, and commercialized an advanced nondestructive evaluation (NDE) inspection method entitled the Single Transducer Thickness-Independent Ultrasonic Imaging Method. Selected by R&D Magazine as one of the 100 most technologically significant new products of 1996, the method uses a single transducer to eliminate the superimposing effects of thickness variation in the ultrasonic images of materials. As a result, any variation seen in the image is due solely to microstructural variation. This nondestructive method precisely and accurately characterizes material gradients (pore fraction, density, or chemical) that affect the uniformity of a material's physical performance (mechanical, thermal, or electrical). Advantages of the method over conventional ultrasonic imaging include (1) elimination of machining costs (for precision thickness control) during the quality control stages of material processing and development and (2) elimination of labor costs and subjectivity involved in further image processing and image interpretation. At NASA Lewis, the method has been used primarily for accurate inspections of high temperature structural materials including monolithic ceramics, metal matrix composites, and polymer matrix composites. Data were published this year for platelike samples, and current research is focusing on applying the method to tubular components. The initial publicity regarding the development of the method generated 150 requests for further information from a wide variety of institutions and individuals including the Federal Bureau of Investigation (FBI), Lockheed Martin Corporation, Rockwell International, Hewlett Packard Company, and Procter & Gamble Company. In addition, NASA has been solicited by the 3M Company and Allison Abrasives to use this method to inspect composite materials that are manufactured by these companies.

Roth, Don J.↗
NASA NTRS2016

Optical Method for Detecting Displacements and Strains at Ultra-High Temperatures During Thermo-Mechanical Testing

An ultra-high temperature optical method incorporates speckle optics for sensing displacement and strain measurements well above conventional measurement techniques. High temperature pattern materials are used which can endure experimental high temperature environments while simultaneously having a minimum optical aberration. A purge medium is used to reduce or eliminate optical distortions and to reduce, and/or eliminate oxidation of the target specimen.

Smith, Russell W.↗
NASA NTRS1983

Method and technique for installing light-weight, fragile, high-temperature fiber insulation

A method of installing fragile, light weight, high temperature fiber insulation, particularly where the insulation is to be used as a seal strip providing a high order of thermal barrier insulation is discussed. The process is based on provision of a strip of the mineral batting cut oversize by a predetermined amount, saturated in a fugitive polymer solution, compressed in a mold, dried and cured to form a rigidized batting material which is machined to required shape. The machine dimensions would normally be at least nominally less than the dimensions of the cavity to be sealed. After insertion in the cavity, which may be a wire-mesh seal enclosure, the apparatus is subjected to baking at a temperature sufficiently high to cause the resin to burn off cleanly, leaving the batting substantially in its original condition and expanded into the cavity or seal enclosure.

Patel, B. C.↗