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Testing and Qualification of Molybdenum Subcapsule Welds for MiniFuel Experiments

This report documents the testing and qualification efforts for welding molybdenum components to support MiniFuel irradiation campaigns. Other details such as general weld parameters, weld joint geometries, and performance limits are also provided in this report. The American Welding Society’s specifications were used to select the nondestructive and destructive tests, which include: gross and fine leak testing, internal pressure proof testing, and creating metallographic mounts of welds. Leak testing and metallographic mounts provide qualitative information about the weld integrity, while the proof testing indicated pressure/usage limits of the molybdenum subcapsule. Based on the testing results provided in the is report, the capsule can be exposed to an internal pressure of at least 20.7 MPa (3000 psi). A sealed capsules is also capable of withstanding the 3.2 MPa (468 psi) external hydrostatic operating pressure of the High Flux Isotope Reactor.

42 ENGINEERING↗

Lifetime extension drop-test of real-world corroded 5 Quart Hagan nuclear material storage container

A 5Qt Hagan container with a 20-year history of nuclear material storage was challenged with three successive drop tests at a height of 3.7 meters. The total mass of the test package was 12.1 kg. The 1st and 2nd drop tests (center of gravity over the container bottom corner but 180 degrees apart on the container bottom face) passed the pre- and post- impact helium leak criterion at less than 1.00E-6 atm-cc/sec (ambient cubic centimeters per second). The 3rd and final test (center of gravity over top corner) failed with a post-impact gross leak of 1.1E-1 atmcc/sec. The RRFMC (Respirable Release Fraction Measurement Chamber) is a drop tower test system that is critical for the sustainability of the SAVY-4000™ series and Hagan-type (NFT Inc. Golden CO) nuclear material storage containers. These are the primary in-use nuclear material storage container types at the Los Alamos National Laboratory TA-55 facility. Results are presented to expand the technical knowledge basis for container lifetime, regarding actual exposure to corrosive gas species on the container inner surfaces. The primary source of general corrosion throughout the container is gaseous hydrogen chloride (HCl). This gas is generated by the degradation of the polyvinylchloride (PVC) bag-out bag. Additionally, in most cases, the nuclear material itself also releases HCl gas (due to residual chemical components associated with the material formation). The RRFMC drop tower gives the end-user the ability record and analyze high-speed video and photography and if needed aerosol mass release measurements. In this report the principal issue is the physical deformation of the 5Qt Hagan container. There were no mass release experiments of test aerosol mass in the present study.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗