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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

H-Canyon Jumper Gasket Sealing Evaluation

H-Canyon Documented Safety Analysis approved December 2019 credits the leak integrity of H-Canyon (HCA) process tanks, piping, and jumpers in preventing the release of radioactive material in a post seismic environment. Demonstration of leak tightness capability for this equipment was achieved through substantial analytical effort. However, one potential weak point that affects leak integrity exists at the gasketed joint between Hanford Connectors (HC) and nozzles. Review of the HCA Crane Log over a three-year period indicates the HCs periodically leak. Savannah River National Laboratory (SRNL) was requested to perform gasket compression tests that evaluate gasket relaxation characteristics, i.e., creep, and provide improvements to the HC installation process that can reduce or eliminate the frequency of leaks at HCs. A HC torque value of 312 ft-lbf is the target value used because it is the minimum torque value, with 95% confidence, when an unlubricated HC is impacted for standard sealing period of 9 seconds. In the HCA pipe-jumper connections are installed remotely by using HCs. HCs inherently add to the uncertainty of a gasketed joint because a calibrated torque value cannot be applied. The gasket material is a special material made of asbestos-fiber impregnated with Teflon. This material has been used for decades and generally performs well but does leak intermittently as gaskets creep and preloaded torque is lost. Gasket types are either snap-ring (SR) or lampshade (LS). Both gasket types cover the same seating area. The SR gasket is designed to remain with the jumper when the jumper is removed leaving the nozzle faces clean of any debris. SR gaskets are initially installed when the jumper is fabricated. Changing gaskets is time consuming and the radioactive environment presents risks to personnel. When jumpers are removed LS gaskets could be used to better seal the connection to reduce down time and ALARA concerns. That is, an LS gasket would be remotely positioned over the nozzle and the HC reinstalled. Testing also included two situations not typical of plant operation. One situation was the use of the non-standard double-layered gaskets (DG), and the other situation was the use of a LS without removal of the installed SR gasket. The DG was used when the supply of LS gaskets ended, so that testing could continue. It was of interest to demonstrate this gasket’s creep response because the DG, which was two gaskets glued together, was thicker than the LS gasket and the thicker material was expected to elicit a greater creep characteristics. The second situation of using two gaskets together by installing an LS gasket without removing the installed gasket is not allowed by the ASME Codes. However, by demonstrating the creep history of such a gasket arrangement it could be considered as an option that could possibly seal a connection while significantly reducing operational down time and personnel risk. Forty tests were conducted, and the overall results demonstrate the initial applied force and how the gasket changes with time. The change in sealing force, in terms of torque, was then measured to obtain a force history as the gaskets creep. This report documents the results of those tests as well as the method used to perform the tests.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS2000

Gasket Assembly for Sealing Mating Surfaces

A gasket assembly for securing a pair of surface together wherein an electrically conductive gasket base having a central opening is provided with a pair of layers secured to opposite sides of the gasket base, with the layers being a fusible alloy, a brazing alloy or a synthetic, thermoplastic material which will melt, without degrading, when the gasket base is heated. The surfaces may be secured to each other by a plurality of bolts to squeeze the gasket assembly there between or by some other clamping means. An electrical current is passed through the gasket base to heat it to a temperature sufficient to melt the layers to seal the surfaces to opposite sides of the gasket base.

Bryant, Melvin A., III↗
DOE OSTI2022

Sealability Qualification of Material Extruded Zytel Gaskets at Extreme Temperatures

In this work, an in-depth qualification of additively manufactured Zytel for gasketing proton exchange membrane fuel cells (PEMFC’s) subject to extreme temperature conditions. The temperature cycling of the PEMFC from 55°C to 100°C accelerates the deterioration of these gaskets compared to that of conventional operation. The additive manufacturing process employed to print these gaskets is material extrusion using Zytel filament. In order to see the effects of the temperature of interest on the printed specimen, each specimen was thermally soaked and then charactered and tested according to ASTM standard F37B. ASTM F37B tests a materials ability to seal and maintain it while bearing both a compressive load and internal pressure load to simulate being in static operation. This process of thermally soaking and sealability testing is shown to show the validity of both this material and additive manufactured components for other applications as well. It is observed that soaking the gaskets at 100°C corrects some of the defects that are present after printing such as missing layers and small voids on the surface of the samples. This allowed for the hot soaked materials to perform better than the samples at room temperature and cold soaked.

Sealability↗
NASA NTRS2007

Development and Evaluation of High Temperature Gaskets for Hypersonic and Reentry Applications

A wide variety of flexible gasket compositions were developed and tested at high temperatures. The gasket material system has high temperature capability. GRABER sealants were very effective in sealing machined ACC-4 composite surfaces. The gasket composition do not bond strongly with the ACC-4 substrate materials. The density of gasket materials can be tailored to show appropriate compressibility.

Singh, Mrityunjay↗
DOE OSTI2023

The Qualification of Sealability and Creep Relaxation of Additively Manufactured Zytel Gaskets for PEM Fuel Cells

The purpose of this thesis is to study the feasibility of low-cost additive manufacturing of gaskets for proton exchange membrane fuel cells exposed to extreme temperature conditions ranging from -55°C to 100°C. With the growing popularity and decreasing costs of additive manufacturing technologies, specifically Material Extrusion (ME), research is being conducted to determine the feasibility of ME components. Thermally cycled PEMFCs may exhibit accelerated gasket deterioration, therefore, the mechanical stability of material extruded gaskets following a harsh thermal cycle must be assessed. The feasibility of the material extruded gaskets will be proven by manufacturing optimization and mechanical testing. The target material for this study is Zytel by DuPont Chemical. The mechanical stability will be assessed via sealability and creep relaxation testing according to ASTM F37B and ASTM F38B respectively. Because the capabilities to conduct sealability testing at temperature were not available, each specimen was thermally soaked and allowed to return to room temperature prior to testing. As a result of sealability experiments, the 100°C-soaked specimens resulted in lower leak rates with a higher precision when compared to specimens soaked at -55°C and 22°C at across all compressive loads. It was observed from results from creep relaxation testing that there is thermal contraction and expansion occurring at 55°C and 100°C respectively, which can be observed by the resultant graphs. The recoverability of thermally cycled specimens are better than those that just experienced a high temperature hold. After the seven-day thermal cycle, the samples stabilized and maintained their structure.

Lazarin, Robert↗
DOE OSTI2023

Interface gasket for building envelope

A gasket assembly for attaching a window to a panel opening includes an inner frame, an outer frame, and an elastic material connecting the inner frame to the outer frame. The elastic material extends contiguously and circumferentially to couple the outer frame to the inner frame. The outer frame and inner frame can include gap flanges and the elastic material can include opposing lateral side portions. The gap flanges are embedded in the lateral side portions of the elastic material. The outer frame includes connecting structure for coupling of the outer frame to the panel opening. The inner frame includes a connecting structure for coupling of the gasket assembly to the window. The gasket assembly is configured to support the window in the panel opening and form a seal between the panel opening and the window. A method of making a gasket assembly is also disclosed.

Aaron, Adam M.↗
DOE OSTI2025

3D printed polymer gaskets for custom-form batteries

Additive manufacturing (AM) processes, like 3D printing, help to facilitate complex and customizable battery geometries which can provide design freedom and enhance volumetric energy density within electronic devices. AM materials must have the thermal and mechanical properties that enable printability, and when used in batteries, AM materials must also be chemically and electrochemically compatible with the battery chemistry. The compatibility between AM materials and the battery is of particular importance for the cell packaging materials which must be inert and are often overlooked. This study systematically studies AM-compatible polymeric materials for use as gaskets in lithium-ion cells. The materials investigated include three thermoplastics suitable for material extrusion printing: polylactic acid (PLA), polycarbonate, and polypropylene/polyethylene copolymer (PPPEC); and two photoresins suitable for vat photopolymerization (VPP) printing: an acrylate-based photoresin and a polyethylene glycol diacrylate photoresin. The AM gasket materials were tested in comparison to a conventional commercial polypropylene gasket. Mechanical testing (swell measurements and material stiffness) and electrochemical testing (linear sweep voltammetry and galvanostatic cycling of full cells) demonstrated that PLA and the VPP polymers were the least compatible with the lithium-ion battery chemistry, despite their prevalent use in studies of AM batteries, and that PPPEC was the most compatible.

3D printing↗
DOE OSTI2022

H-Canyon Jumper Gasket Sealing Evaluation

H-Canyon Documented Safety Analysis approved December 2019 credits the leak integrity of HCanyon (HCA) process tanks, piping, and jumpers in preventing the release of radioactive material in a post seismic environment. Demonstration of leak tightness capability for this equipment was achieved through substantial analytical effort. However, one potential weak point that affects leak integrity exists at the gasketed joint between Hanford Connectors (HC) and nozzles. Review of the HCA Crane Log over a three-year period indicates the HCs periodically leak. Savannah River National Laboratory (SRNL) was requested to perform gasket compression tests that evaluate gasket relaxation characteristics, i.e., creep, and provide improvements to the HC installation process that can reduce or eliminate the frequency of leaks at HCs. A HC torque value of 312 ft-lbf is the target value used because it is the minimum torque value, with 95% confidence, when an unlubricated HC is impacted for standard sealing period of 9 seconds.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS2003

Gasket Assembly for Sealing Mating Surfaces

A pair of substantially opposed mating surfaces are joined to each other and sealed in place by means of an electrically-conductive member which is placed in proximity to the mating surfaces. The electrically-conductive member has at least one element secured thereto which is positioned to contact the mating surfaces, and which softens when the electrically-conductive member is heated by passing an electric current therethrough. The softened element conforms to the mating surfaces, and upon cooling of the softened element the mating surfaces are joined together in an effective seal. Of particular significance is an embodiment of the electrically-conductive member which is a gasket having an electrically-conductive gasket base and a pair of the elements secured to opposite sides of the gasket base. This embodiment is positioned between the opposed mating surfaces to be joined to each other. Also significant is an embodiment of the electrically-conductive member which is an electrically-conductive sleeve having an element secured to its inner surface. This embodiment surrounds cylindrical members the bases of which are the substantially opposed mating surfaces to be joined, and the element on the inner surface of the sleeve contacts the outer surfaces of the cylindrical members.

Bryant, Melvin A., III↗
NASA NTRS1966

Rubber and alumina gaskets retain vacuum seal in high temperature EMF cell

Silicone rubber gasket and an alumina gasket retain a vacuum inside a high temperature EMF cell in which higher and lower density liquid metal electrodes are separated by an intermediate density fused salt electrolyte. This innovation is in use on a sodium bismuth regenerable EMF cell in which the fused salts and metals are at about 500 deg to 600 deg C.

Hesson, J. C.↗
NASA NTRS1974

Reinforced polyquinoxaline gasket and method of preparing the same

A gasket or seal resistant to ionizing radiation and liquid hydrogen temperatures is made up of a laminated polyquinoxaline resin-fiberglass cloth body portion and a molded polyquinoxaline encapsulating film. The laminated body is prepared by stacking thin sheets of the resin alternately with fiberglass cloth and heating the assembly under pressure with the temperature, pressure and resin film thickness being controlled so that only partial impregnation of the fiberglass cloth is produced. The encapsulating resin film is preheated at about 300 f and applied to the laminate body by molding at a temperature of about 625 F. The molded gasket is then deflashed and post-cured by heating at 675 to 700 F.

Vanauken, R.↗
NASA NTRS1981

Spiral-wound gasket forms low-temperature seal

Spiral-wound cryogenic gasket with one component requires no encapsulant and is easily produced with self-locking features. Seal either opens and closes or is fixed. It is made by skiving strip from circumference of disk of glass-filled material. Successive turns of strip are spirally wrapped in groove machined into one flange surface. Closing joint compresses gasket.

Irick, S. C.↗
NASA NTRS1996

Leakage Through a Channel Formed by a Gasket, a Sealing Surface, and a Filament Trapped Between Them

Plumbing for the transport of liquid Hydrogen or liquid Oxygen at the Kennedy Space Center (KSC) is very critical. Every piece of hardware for handling such a hazardous cryogen is subject to testing prior to installation and use. Safe, realistic testing of all such hardware is prohibitively expensive, which leads, perforce, to expidients such as: (1) lead testing with non-flammable tracer fluids (e.g, liquid nitrogen) and (2) leak testing with room temperature tracer fluids (e.g. liquid helium). Such expedients undermine the realism of the tests. If however, one could apply rational fluid dynamics methods to derive a general analytical expression with which one could relate the throughput of gaseous Helium through a given leak channel to the throughput of liquid Hydrogen through the same channel, then one could recover much of the information that one would otherwise forfeit through these expedients. These facts lead to the following questions: (1) What would be an example of a generic flaw in a gasket?; and (2) How can one calculate the flow of fluid in it? The report addresses these questions. It considers a particular leak geometry, namely one formed by a gasket, a sealing surface, and a filament trapped between them (so that the cross section of the leak channel is a flat bottomed curvilinear triangle, two sides of which are circular arcs and which has cusps on all three corners).

Russell, John↗
NASA NTRS2006

Partial-Vacuum-Gasketed Electrochemical Corrosion Cell

An electrochemical cell for making corrosion measurements has been designed to prevent or reduce crevice corrosion, which is a common source of error in prior such cells. The present cell (see figure) includes an electrolyte reservoir with O-ring-edged opening at the bottom. In preparation for a test, the reservoir, while empty, is pressed down against a horizontal specimen surface to form an O-ring seal. A purge of air or other suitable gas is begun in the reservoir, and the pressure in the reservoir is regulated to maintain a partial vacuum. While maintaining the purge and partial vacuum, and without opening the interior of the reservoir to the atmosphere, the electrolyte is pumped into the reservoir. The reservoir is then slowly lifted a short distance off the specimen. The level of the partial vacuum is chosen such that the differential pressure is just sufficient to keep the electrolyte from flowing out of the reservoir through the small O-ring/specimen gap. Electrochemical measurements are then made. Because there is no gasket (and, hence, no crevice between the specimen and the gasket), crevice corrosion is unlikely to occur.

Bonifas, Andrew P.↗