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At least 19 records

Update on the Current R&D Activity in the U.S.

This presentation is to fulfil DOE commitment to GIF VHTR Materials PMB. Notched creep rupture testing: Weldment V-notch specimen test finished. 800C 60MPa, 15,716 hour rupture life. Two double V-notch specimen tests have finished. Crack growth tests: System modification was required for creep and creep-fatigue testing, Epsilon 3548COD Extensometer has been ordered, to allow load-line displacement measurements, to be paired with direct current potential drop already used to measure crack length, Sample redesigned in accordance to ASTM E2760 and E1457 to allow for both creep and creep-fatigue crack growth rate testing. Alloy 800H Weldments (1/2) and Alloy 800H Weldments (2/2), Variable Fatigue Testing, and Multi=axial Stress Relaxation. Continue work to finish 800H model, examine ?universal? constitutive model form.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Effect of Notches on Creep-Fatigue Behavior of a P/M Nickel-Based Superalloy

A study was performed to determine and model the effect of high temperature dwells on notched low cycle fatigue (NLCF) and notch stress rupture behavior of a fine grain LSHR powder metallurgy (PM) nickel-based superalloy. It was shown that a 90 second dwell applied at the minimum stress (min dwell) was considerably more detrimental to the NLCF lives than similar dwell applied at the maximum stress (max dwell). The short min dwell NLCF lives were shown to be caused by growth of small oxide blisters which caused preferential cracking when coupled with high concentrated notch root stresses. The cyclic max dwell notch tests failed mostly by a creep accumulation, not by fatigue, with the crack origin shifting internally to a substantial distance away from the notch root. The classical von Mises plastic flow model was unable to match the experimental results while the hydrostatic stress profile generated using the Drucker-Prager plasticity flow model was consistent with the experimental findings. The max dwell NLCF and notch stress rupture tests exhibited substantial creep notch strengthening. The triaxial Bridgman effective stress parameter was able to account for the notch strengthening by collapsing the notched and uniform gage geometry test data into a singular grouping.

Dwell Notch Fatigue↗

Hot isostatically pressed manufacture of high strength MERL 76 disk and seal shapes

The feasibility of using MERL 76, an advanced high strength direct hot isostatic pressed powder metallurgy superalloy, as a full scale component in a high technology, long life, commercial turbine engine were demonstrated. The component was a JT9D first stage turbine disk. The JT9D disk rim temperature capability was increased by at least 22 C and the weight of JT9D high pressure turbine rotating components was reduced by at least 35 pounds by replacement of forged Superwaspaloy components with hot isostatic pressed (HIP) MERL 76 components. The process control plan and acceptance criteria for manufacture of MERL 76 HIP consolidated components were generated. Disk components were manufactured for spin/burst rig test, experimental engine tests, and design data generation, which established lower design properties including tensile, stress-rupture, 0.2% creep and notched (Kt = 2.5) low cycle fatigue properties, Sonntag, fatigue crack propagation, and low cycle fatigue crack threshold data. Direct HIP MERL 76, when compared to conventionally forged Superwaspaloy, is demonstrated to be superior in mechanical properties, increased rim temperature capability, reduced component weight, and reduced material cost by at least 30% based on 1980 costs.

Eng, R. D.↗

Sensitivity of the creep-rupture properties of Waspaloy sheet to sharp-edged notches in the temperature range 1000-1400 deg F.

Time-dependent notch sensitivity of Waspaloy was observed at test temperatures from 1000 to 1300 deg F. Its occurrence in this range was dependent on the heat treatment. ?Overaging' eliminated the notch sensitivity. Optimum combination of smooth and notched specimen strengths for material solution treated at 1975 deg F were obtained by aging 24 hr at 1550 deg F. Necessary conditions for time-dependent notch sensitivity were (1) the notch specimen loads had to be below the approximate 0.2 percent offset yield strength; and (2 ) test data from smooth specimens had to indicate that small amounts of creep used up large fractions of creep-rupture life. No reasons were evident why these criteria will not prove applicable to other alloys.

Wilson, D. J.↗

Update on the Current R&D Activity in the U.S.

An NRC-sponsored assessment of a previous version of Section III, Division 5 of the ASME BPVC identified an inadequate understanding of the impact of a multiaxial stress, structural discontinuities, and notch effects.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Effects of Geometric Discontinuities on Creep Behavior of Alloy 617

Due to the excellent long-term high-temperature performance of Alloy 617, the Alloy has been identified as the primary structural material for the intermediate heat exchanger of the Very High Temperature Reactor (VHTR). Both the base and welded alloy has been qualified to be used up to 950 °C up to 100,000 hours by the American Society of Mechanical Engineer (ASME) Boiler and Pressure Vessel Code (BPVC). The qualification properties of the material were exclusively determined by uniaxial creep tests. The components may, however, experience multiaxial stress conditions in service due to the reactor geometry. This study used notched creep tests to investigate the effect of geometric discontinuities on creep behavior of both the base and welded Alloy 617. The V-notch tests reveal that the geometric discontinuities do not reduce the creep rupture live under high and intermediate stress conditions. The U-notch tests show that a larger radius notch behave in a similar way as a straight gauge section of a uniaxial test. The creep rupture live of the welded alloy was slightly longer than the base metal.

36 - MATERIALS SCIENCE↗

Time-dependent edge notch sensitivity of Inconel 718 sheet in the temperature range 900 to 1400 F (482 to 760 C)

Time-dependent notch sensitivity of Inconel 718 sheet occurred at 900 to 1200 F when notched specimens were loaded below the yield strength, and tests on smooth specimens showed that small amounts of creep consumed large fractions of creep-rupture life. The severity of the notch sensitivity decreased with decreasing solution treatment temperature and increasing time and/or temperature of the aging treatment. Elimination of the notch sensitivity was correlated with a change in the dislocation mechanism from shearing to by-passing precipitate particles.

Wilson, D. J.↗

Relationship of mechanical characteristics and microstructural features to the time-dependent edge notch sensitivity of inconel 718 sheet

Time-dependent notch sensitivity of Inconel 718 sheet was observed at 900 F to 1200 F (482 - 649 C). It occurred when edge-notched specimens were loaded below the yield strength and smooth specimen tests showed that small amounts of creep consumed large rupture life fractions. The severity of the notch sensitivity was reduced by decreasing the solution temperature, increasing the time and/or temperature of aging and increasing the test temperature to 1400 F (760 C). Elimination of time-dependent notch sensitivity correlated with a change in dislocation motion mechanism from shearing to by-passing precipitate particles.

Wilson, D. J.↗

Characterization of the mechanical and physical properties of TD-NiCr (Ni-20Cr-2ThO2) alloy sheet

Sheets of TD-NiCr processed using techniques developed to produce uniform material were tested to supply mechanical and physical property data. Two heats each of 0.025 and 0.051 cm thick sheet were tested. Mechanical properties evaluated included tensile, modulus of elasticity, Poisson's Ratio, compression, creep-rupture, creep strength, bearing strength, shear strength, sharp notch and fatigue strength. Test temperatures covered the range from ambient to 1589K. Physical properties were also studied as a function of temperature. The physical properties measured were thermal conductivity, linear thermal expansion, specific heat, total hemispherical emittance, thermal diffusivity, and electrical conductivity.

Fritz, L. J.↗

Determination of structural engineering properties of incoloy 903 and CTX-1 alloys

Tension, notched tension, compression, density, thermal conductivity, and thermal expansion tests were conducted on Incoloy 903 over the temperature range 20 K (-423 F) through 1033 K (1400 F). Fracture toughness tests were performed at room temperature (RT). Creep and rupture tests were conducted at 811 K (1000 F), 922 K (1200 F), and 1033 K (1400 F) for this alloy. Transverse unnotched and notched fatigue tests at R = 0.1 were performed at RT and 922 K (1200 F). For CTX-1 alloy, tension, Charpy V-notch impact, density, thermal conductivity, and thermal expansion tests were conducted over the temperature range 20 K (-423 F) through 1033 K (1400 F). Poisson's ratio was determined at RT, 811 K (1000 F), 922 K (1200 F), and 1033 K (1400 F). Notched tension and compression tests were performed at 20 K (-423 F), RT, and 922 K (1200 F); plane strain fracture toughness tests were conducted at RT, 77 K (-320 F), and 20 K (-423 F). Creep and rupture tests were performed at 811 K (1000 F), 922 K (1200 F), and 1033 K (1400 F); longitudinal unnotched and notched fatigue tests at R = 0.1 were conducted at RT and 922 K (1200 F). Results are presented and discussed.

Ruff, P. E.↗

Time-dependent edge-notch sensitivity of oxide and gamma prime dispersion strengthened sheet materials at 1000 to 1800 F (538 - 982 C)

Research was carried out to determine whether an oxide dispersion hardened alloy, TD-Ni, Cr, and low volume fraction gamma prime strengthened nickel-base alloy, Modified Waspaloy, were susceptible to time-dependent edge-notch sensitivity. The results were evaluated in terms of the mechanical characteristics of the alloys and the dislocation motion mechanisms operative. As far as could be determined, the results of the investigation were consistent with the following important concepts developed for Waspaloy and Inconel 718: (1) Time-dependent edge-notch sensitivity occurs when notched specimens are loaded below the approximate 0.2 percent smooth specimen offset yield strength and when data from smooth specimens indicate that small amounts of creep consume large rupture life fractions. (2) When precipitate particles are sheared by dislocations, the deformation is localized and time-dependent notch sensitivity occurs. When dislocations by-pass precipitate particles the deformation is homogeneous. Under these conditions, no time-dependent notch sensitivity has been observed.

Wilson, D. J.↗

Influence of gaseous hydrogen on the mechanical properties of high temperature alloys

Tensile tests of six nickel-base and one cobalt-base alloy were conducted in 34.5 MN/sq m helium and hydrogen environments at temperatures from 297 K to 1,088 K. Mechanical properties tests of the nickel-base alloy MAR M-246 (Hf modified), in two cast conditions, were conducted in gaseous environments at temperatures from 297 K to 1,144 K and pressures from one atmosphere to 34.5 MN/sq m. The objective of this program was to obtain the mechanical properties of the various alloys proposed for use in space propulsion systems in a pure hydrogen environment at different temperatures and to compare with the mechanical properties in helium at the same conditions. All testing was conducted on solid specimens exposed to external gaseous pressure. Smooth and notched tensile properties were determined using ASTM tensile testing techniques, and creep-rupture life was determined using ASTM creep-rupture techniques. Low-cycle fatigue life was established by constant total strain and constant stress testing using smooth specimens and a closed-loop test machine.

Source record↗

Characterization of an oxide dispersion strengthened superalloy, MA-6000E, for turbine blade applications

Alloy MA 6000E was developed by the mechanical alloying process for turbine blade applications. The nominal composition of the experimental alloy is Ni-15CR-2Mo-4W-4.5Al- 2.5Ti-2Ta- .15Zr-.05C-.01B-1.1Y2O3. The 1000 hour rupture strength in the longitudinal direction is about 145 MPa at 1093 C and about 483 MPa at 760 C. The alloy displays normal three-stage creep behavior. Typically the creep elongation is 3.5% at 760 C and 2% at 1093 C. The alloy is notch ductile (K sub 1 = 3.5). The rupture properties of the alloy are not significantly degraded by thermal cycling or prior stress isothermal exposure. The alloy also has excellent longitudinal high and low cycle fatigue resistance. Limited testing indicates that MA 6000E posesses good off-axis mechanical properties. The transverse tensile elongation at 760 C is about 3%. The 100 hour transverse rupture strength is 331 MPa at 760 C and about 55 MPa at 1093 C.

Kim, Y. G.↗

Factors Influencing Dwell Fatigue Cracking in Notches of Powder Metallurgy Superalloys

The influences of heat treatment and cyclic dwells on the notch fatigue resistance of powder metallurgy disk superalloys were investigated for low solvus high refractory (LSHR) and ME3 disk alloys. Disks were processed to produce material conditions with varied microstructures and associated mechanical properties. Notched specimens were first subjected to baseline dwell fatigue cycles having a dwell at maximum load, as well as tensile, stress relaxation, creep rupture, and dwell fatigue crack growth tests at 704 C. Several material heat treatments displayed a bimodal distribution of fatigue life with the lives varying by two orders-of-magnitude, while others had more consistent fatigue lives. This response was compared to other mechanical properties, in search of correlations. The wide scatter in baseline dwell fatigue life was observed only for material conditions resistant to stress relaxation. For selected materials and conditions, additional tests were then performed with the dwells shifted in part or in total to minimum tensile load. The tests performed with dwells at minimum load exhibited lower fatigue lives than max dwell tests, and also exhibited early crack initiation and a substantial increase in the number of initiation sites. These results could be explained in part by modeling evolution of peak stresses in the notch with continued dwell fatigue cycling. Fatigue-environment interactions were determined to limit life for the fatigue cycles with dwells.

Gabb, T. P.↗

Hydrogen environment embrittlement of astroloy and Udimet 700 (nickel-base) and V-57 (iron-base) superalloys

The sensitivity to hydrogen environment embrittlement of three superalloys was determined. Astroloy forgings were resistant to embrittlement during smooth tensile, notched tensile, and creep testing in 3.5-MN/sq m hydrogen over the range 23 to 760 C. The notched tensile strength of Udimet 700 bar stock in hydrogen at 23 C was only 50 percent of the baseline value in helium. Forgings of V-57 were not significantly embrittled by hydrogen during smooth tensile testing over the range 23 to 675 C; creep and rupture lives of V-57 were degraded by hydrogen. Postcreep tensile ductility of V-57 was reduced by 40 percent after creep exposure in hydrogen.

Gray, H. R.↗