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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Core Characterization: Computer Tomography, Geochemical, and Core Petrophysical Workflows for Emerging Critical Mineral Plays

The National Energy Technology Laboratory’s geoimaging lab in Morgantown, WV has been performing core characterization using multi-resolution Computed Tomography (CT) imaging and multisensor corelogger which allows for cm-resolution elemental and petrophysical measurements along whole core. This workflow has historically been used in unconventional gas plays and potential carbon storage locations. This rapid core characterization leads itself well as a first phase process in CM/REE evaluation efforts allowing for high-resolution, non-destructive investigation of elemental concentration using X-Ray Fluorescence and examination of core features through CT imaging.

Paronish, Thomas J.↗
DOE OSTI2024

Prospecting for Critical Minerals and Rare Earth Elements from Marcellus Shale in the Western Portion of the Appalachian Basin with Non-Destructive Core Characterization

Identification of sources for domestic critical minerals and rare earth elements (CM/REE) has been deemed essential for the energy transition by the United States Department of Energy (DOE). The U.S. DOE’s National Energy Technology Laboratory’s (NETL) Geomaterials Characterization Laboratory has performed non-destructive core characterizations on energy-relevant rock cores for the past decade. During this time, NETL has published over 36 technical reports and made the associated data publicly available. Much of this work focuses on unconventional shale gas, subsurface carbon storage systems, and carbon-ore. These efforts provide cm-scale petrophysical and elemental data, photographic documentation, detailed core descriptions, and computed tomography (CT) data for each well. This provides a first phase prospecting resource for CM/REE resources and can provide a map for pin-pointing intervals and lithologies for further development. Using historical core characterization data from 12 Marcellus wells from the western portion of the Appalachian Basin, this study builds an improved understanding of the chemostratigraphy of the basin. X-ray fluorescence (XRF) and CT images were used to determine lithologic intervals and potential ore bodies for further analysis, including benchtop digestion and inductively coupled plasma mass spectrometry (ICP-MS) to better understand the CM/REE enrichments.

Paronish, Thomas J.↗
DOE OSTI2021

Core Characterization of Bakken Shale from the Bedwell 33-52-1-1H Well, Sheridan County, Montana

The computed tomography (CT) facilities and the Multi-Sensor Core Logger (MSCL) at the National Energy Technology Laboratory (NETL) in Morgantown, West Virginia were used to characterize core of the Bedwell 33-52-1-1H well (API 25-091-21920), a wildcat field in Sheridan County, Montana. The primary impetus of this work is to provide a unique dataset to researchers at universities, national laboratories, geological surveys, and other locations for additional analyses. The resultant datasets are presented in this report and can be accessed from NETL's Energy Data eXchange (EDX) online system using the following link: https://edx.netl.doe.gov/dataset/bedwell-33-52-1-1h-well. The equipment and techniques used to characterize the full core were non-destructive, enabling future examinations and analyses to be performed on these cores. However, none of the equipment used was suitable for direct visualization of the pore space in fine-grained structures such as those found in shales; fractures, discontinuities, and millimeter scale features were readily detectable with the methods tested. Imaging with the NETL medical CT scanner was performed on the entire core. Qualitative analysis of the medical CT images, coupled with X-ray fluorescence (XRF), P-wave, and magnetic susceptibility measurements from the MSCL were useful in identifying zones of interest for more detailed analysis. A selection of samples (Table 1) were cored, sliced, and powdered for additional characterization analyses. These analyses did involve destructive subsampling of the full core at discrete sections, and the results are presented here in the context of the larger core description. Selected sections of the core were removed from the full core for detailed analyses using the following destructive techniques: bulk inductively coupled plasma-optical emission spectroscopy (ICP-OES), isolation of carbon and sulfur, Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), and higher resolution CT scan with NETL’s micro-CT scanning systems. The ability to quickly identify key areas for more detailed study with higher resolution will save time and resources in future studies. The combination of methods used provides a multi-scale analysis of the core; the resulting macro and micro descriptions are relevant to many subsurface energy related examinations traditionally performed at NETL.

04 OIL SHALES AND TAR SANDS↗
DOE OSTI2022

On a Unified Core Characterization Methodology to Support the Systematic Assessment of Rare Earth Elements and Critical Minerals Bearing Unconventional Carbon Ores and Sedimentary Strata

A significant gap exists in our understanding and ability to predict the spatial occurrence and extent of rare earth elements (REE) and certain critical minerals (CM) in sedimentary strata. This is largely due to a lack of existing, systematic, and well-distributed REE and CM samples and analyses in United States sedimentary basins. In addition, the type of sampling and characterization performed to date has generally lacked the resolution and approach required to constrain geologic and geographic heterogeneities typical of subsurface, mineral resources. Here, we describe a robust and systematic method for collecting core scale characterization data that can be applied to studies on the contextual and spatial attributes, the geologic history, and lithostratigraphy of sedimentary basins. The methods were developed using drilled cores from coal bearing sedimentary strata in the Powder River Basin, Wyoming (PRB). The goal of this effort is to create a unified core characterization methodology to guide systematic collection of key data to achieve a foundation of spatially and geologically constrained REEs and CMs. This guidance covers a range of measurement types and methods that are each useful either individually or in combination to support characterization and delineation of REE and CM occurrences. The methods herein, whether used in part or in full, establish a framework to guide consistent acquisition of geological, geochemical, and geospatial datasets that are key to assessing and validating REE and CM occurrences from geologic sources to support future exploration, assessment, and techno-economic related models and analyses.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2024

NETL Non-Destructive Core Characterization

This product describes the Characterization efforts since 2017; the current methods used, publication, deep dives into method applications, and future direction of the Core Characterization work.

Paronish, Thomas J.↗
DOE OSTI2024

Carbon Storage Core Characterization Efforts at NETL

The multi-scale Computed Tomography (CT) and core flow facility in the Geocharacterization Laboratory at NETL, Morgantown yields porosity, permeability, and fracture properties of rock core samples obtained from the subsurface while maintaining the integrity of the sample. Additionally, geophysical bulk rock properties are analyzed with the laboratory’s GeoTEK multi-sensor core logger in a comparable fashion to downhole methods. NETL researchers collaborate with stakeholders within the carbon storage, oil and gas, and critical minerals sectors. Since 2017, over 1.88 miles of core have been analyzed within the laboratory and all data is publicly available through the Technical Report Series (TRS) on the Energy Data eXchange (EDX). Additionally, the website, RokBase, was curated to extrapolate and visualize the high-resolution data from field operations. The characterization of the Lively Grove #1 (LG#1) well provides a case study into the full capabilities of the Geocharacterization Laboratory. During the comprehensive study of LG#1 ~1-2 mm in diameter, vertical to bedding, cylindrical structures were identified throughout the St. Peter Formation. These structures are pervasive throughout the St. Peter Formation at depth and are characterized as the trace fossil, Skolithos.

Isom, Shelby L↗
DOE OSTI2025

Brady’s Geothermal Field Computed Tomography Core Characterization

We present a publicly accessible database centered around multi-scale Computed Tomographic (CT) imaging of samples from the BCH-03 well, supplemented by a wide range of supporting geological analyses (Brown, et al., 2022). The data include detailed petrologic descriptions of core samples, core-scale medical CT scans, high-resolution micro-CT scans, thin section photomicrographs, elemental abundance data from X-ray diffraction, velocity wave measurements, and helium porosimetry of the matrix.

computed tomography↗
DOE OSTI2026

Characterizing core and edge turbulence regimes with fluctuation imaging diagnostics in Wendelstein 7-X

Two density fluctuation imaging systems, phase contrast imaging (PCI) and gas puff imaging (GPI) measure spatially resolved density fluctuations with high time resolution throughout the core plasma (PCI) and in the scrape-off layer (GPI) of the Wendelstein 7-X (W7-X) stellarator. Both systems combined give a comprehensive overview of overall fluctuation levels, spectral properties such as their distribution in frequency and wavenumber space as well as their spatial distribution. These tools are used to assess changes in density turbulence in three representative discharges that transition into stable divertor detachment by different strategies (impurity seeding, density ramping and power starvation). Several general trends are identified when the radiated power fraction is systematically increased: In the plasma edge, the line emission observed by GPI shifts radially inward with a drop in electron temperature, and normalized intensity fluctuation profiles follow this inward shift. Skewness and kurtosis of these edge fluctuations are reduced, indicating a reduction of large intermittent transport events, and poloidal phase velocities decrease in magnitude. These observations are consistent with a reduced power input into the plasma edge and a general reduction of turbulent activity. Core density fluctuation levels remain nearly constant in the impurity seeding scenario, indicating that detachment does not significantly impact turbulence there. However, a strong reduction in the dominant outboard fluctuation phase velocity is observed that deviates from the previous interpretation of neoclassical radial electric field changes, showing that the core plasma is not completely unaffected. In the density ramp and power starvation scenarios, undesirable and irregular large-scale events arise clearly in both diagnostic systems as the radiative fraction is increased. Impurity seeding therefore seems to be a promising strategy on W7-X to achieve detachment without significantly altering core turbulence, especially when targeting a specific operating point in core density and heating power.

Wendelstein 7-X↗
DOE OSTI2022

Core Characterization of the Whipkey ST1 Well - Marcellus Shale

CT and geophysical data of the Marcellus from the Whipkey ST 1 well in Greene Co PA API No: 37-059-24715 latitude 39.9000020N, longitude -80.0199970W Please see the following technical report for further details. Crandall, D.; Moore, J.; Brown, S.; Mackey, P.; Carr, T. Computed Tomography Scanning and Geophysical Measurements of the Marcellus Formation from the Whipkey ST 1 Well NETL-TRS-X-2018; NETL Technical Report Series; U.S. Department of Energy, National Energy Technology Laboratory: Morgantown, WV, 2018; p 54.

Computed Tomography↗
DOE OSTI2022

Computed Tomography Scanning and Geophysical Measurements of the Patterson #5-25 Well in Western Kansas

The computed tomography (CT) facilities and the Multi-Sensor Core Logger (MSCL) at the National Energy Technology Laboratory (NETL) site in Morgantown, West Virginia, were used to characterize core from the Patterson Field site. This core came from a vertical well (Patterson #5-25 well) that was obtained as part of the U.S. Department of Energy (DOE) sponsored Integrated Midcontinental Stacked Carbon Storage Hub. The primary impetus of this work is a collaboration between NETL and the Kansas Geological Survey to characterize core from the Patterson Field site. The 625 ft of whole core from the Atoka Formation to Precambrian Basement was characterized at NETL. As part of this effort, bulk scans of core were obtained. This report, and the associated scans, provide detailed datasets not typically made publicly available for carbon capture utilization and storage analysis. The resultant datasets are presented in this report and can be accessed from NETL's Energy Data eXchange (EDX) online system using the following link: https://edx.netl.doe.gov/dataset/patterson-5-25-well. All equipment and techniques used were non-destructive, enabling future examinations and analyses to be performed on these cores. None of the equipment used was suitable for direct visualization of the shale pore space, although fractures and discontinuities were detectable with the methods tested. Low resolution CT imagery with the NETL medical CT scanner was performed on the entire core. Qualitative analysis of the medical CT images, coupled with x-ray fluorescence (XRF), P-wave, and magnetic susceptibility measurements from the MSCL are useful in identifying zones of interest for more detailed analysis as well as fractured zones. The ability to quickly identify key areas for more detailed study with higher resolution will save time and resources in future studies. The combination of methods used provided a multi-scale analysis of this core and provided both a macro and micro description of the core that is relevant for many subsurface energy related examinations that have traditionally been performed at NETL.

58 GEOSCIENCES↗