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DOE OSTI2023

The Mu2e Crystal and SiPM Calorimeter: Construction Status

The Mu2e experiment at Fermilab searches for the neutrino-less conversion of a negative muon into an electron, with a distinctive signature of a mono-energetic electron with an energy of 104.967 MeV. The calorimeter is made of two disks of pure CsI crystals, each read out by two custom large-area UV-extended silicon photomultipliers (SiPMs). It plays a fundamental role in providing excellent particle identification capabilities and an online trigger filter while improving the track reconstruction, requiring better than 10% energy and 500 ps timing resolutions for 100 MeV electrons. In this article, we present the status of construction and the quality control (QC) performed on the produced crystals and photosensors, the development of the rad-hard electronics, and the most important results of the irradiation tests. Construction of the mechanics is also reported. Status and plans for the calorimeter assembly and its first commissioning are described.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Plutonium-238 Loadout Calorimeter Return To Service

The calorimeter in the transfer area in Building 7920 at the US Department of Energy’s Oak Ridge National Laboratory is used to measure the amount of 238 Pu in the Plutonium Heat Source Oxide. The calorimetry measurement is taken after the oxide is packaged in an ORISC (Oak Ridge Inner Shipping Capsule)/FSO (Fuel Storage Outer) assembly before loading into the Containment Vessel and shipping container. The equipment is used in three specific configurations: zero measurement (nothing in the sample cup), FSO measurement (actual measurement of 238 Pu), and reference calibration measurement (using the reference FSO as a known heat source). System checks were performed in July 2023 in preparation for scheduled material loadout. During these checks, personnel discovered that the reference FSO had experienced an electrical short in the heater cable and was no longer functional. The calorimeter was in the reference calibration measurement configuration at this time. Facility management was notified when the damage was discovered. The data from the Yokogawa recorder were pulled and analyzed for a span of time between September 2022 and July 2023. An unusual spike was found in the sample cup temperature data that started on October 19, 2022, and ended on October 20, 2022. The sample cup reached a temperature of 191.1°C. The maximum allowable temperature for the calorimeter thermopile to reach is 220°C based on the manufacturer statement provided in Appendix B of this report [1]. The calorimeter thermopile and the sample cup thermocouple are physically close to each other; therefore, the data suggest that the calorimeter itself never saw a temperature in excess of 191.1°C. Physical damage present on the cable, tape, and insulation suggests that the temperature reached a higher value in some locations within the sample cup than the data shows. Because of this discrepancy, testing of the calorimeter was required to confirm that the calorimeter is functioning the same as it was before the electrical short. The intent of this report is to assess the functionality of the calorimeter and determine if it is acceptable to use for 238 Pu loadout material measurement. Testing showed that the calorimeter is functionally equivalent to the initial calibration that was performed in the summer of 2021, and thus, the calorimeter was cleared to be used for its intended purposes.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS2021

Challenges with Heat Flux Calorimeters used in Arc Jets

Occasionally large errors have occurred in some of the calorimeters used in the arc jet facilities. Some slug calorimeters would measure twice the expected heat flux and some Coaxial TC calorimeters would measure half the expected heat flux. While these errors in heat flux measurements are easy to identify and discard / dismiss, the concern is that less spectacular errors are difficult to detect. This inspired a critical look at the calorimetry used to measure stagnation heat flux in the NASA Ames Arc Jet facilities. Numerous sources of error were investigated, and the culprit in the case of slug calorimeters was determined to be leaks in the stagnation calorimeter assembly resulting in flow along the side of the slug. In the case of the coaxial TC calorimeter, it is hypothesized that in some calorimeters there is a partial electrical short circuit in the Coaxial TC sensor element somewhere in the middle of the calorimeter.

Calorimeter↗

NASA NTRS2018

Uncertainty Analysis of Coaxial Thermocouple Calorimeters Used in Arc Jets

Recent introduction of Coaxial Thermocouple type calorimeters into the NASA Ames arc jet facilities has inspired an analysis of 2D conduction effects internal to this type of calorimeter. Lateral conduction effects violate the 1D finite slab inverse analysis which is typically used to deduce the heat transfer to such calorimeters. The spherical shaped nose associated with most calorimeters (rather than flat) leads to a bias error that over-estimates the stagnation heating. Non-uniform heating on the face of spherically shaped calorimeters leads to conduction losses to the colder rim of the calorimeter which causes an underestimate of the stagnation heating. These two effects come into play at different times of the calorimeter's exposure to the arc jet, so they do not cancel. The spherical body effects come into play in the early stages of exposure, while the non-uniform heating effect becomes most severe at the later stages of exposure. The bias associated with spherical effects can be avoided by rewriting the 1D finite slab inverse analysis code to solve for 1D conduction in spherical coordinates. However, reducing the bias error associated non-uniform heating requires a somewhat ad hoc modification to the 1D finite element inverse analysis.

Isotherms↗

NASA NTRS2010

High Resolution, Non-Dispersive X-Ray Calorimeter Spectrometers on EBITs and Orbiting Observatories

X-ray spectroscopy is the primary tool for performing atomic physics with Electron beam ion trap (EBITs). X-ray instruments have generally fallen into two general categories, 1) dispersive instruments with very high spectral resolving powers but limited spectral range, limited count rates, and require an entrance slit, generally, for EBITs, defined by the electron beam itself, and 2) non-dispersive solid-state detectors with much lower spectral resolving powers but that have a broad dynamic range, high count rate ability and do not require a slit. Both of these approaches have compromises that limit the type and efficiency of measurements that can be performed. In 1984 NASA initiated a program to produce a non-dispersive instrument with high spectral resolving power for x-ray astrophysics based on the cryogenic x-ray calorimeter. This program produced the XRS non-dispersive spectrometers on the Astro-E, Astro-E2 (Suzaku) orbiting observatories, the SXS instrument on the Astro-H observatory, and the planned XMS instrument on the International X-ray Observatory. Complimenting these spaceflight programs, a permanent high-resolution x-ray calorimeter spectrometer, the XRS/EBIT, was installed on the LLNL EBIT in 2000. This unique instrument was upgraded to a spectral resolving power of 1000 at 6 keV in 2003 and replaced by a nearly autonomous production-class spectrometer, the EBIT Calorimeter Spectrometer (ECS), in 2007. The ECS spectrometer has a simultaneous bandpass from 0.07 to over 100 keV with a spectral resolving power of 1300 at 6 keV with unit quantum efficiency, and 1900 at 60 keV with a quantum efficiency of 30%. X-ray calorimeters are event based, single photon spectrometers with event time tagging to better than 10 us. We are currently developing a follow-on instrument based on a newer generation of x-ray calorimeters with a spectral resolving power of 3000 at 6 keV, and improved timing and measurement cadence. The unique capabilities of the x-ray calorimeter spectrometer, coupled with higher spectral resolution dispersive spectrometers to resolve line blends, has enabled many science investigations, to date mostly in our x-ray laboratory astrophysics program. These include measurements of absolute cross sections for Land K shell emission from Fe and Ni, charge exchange measurements in many astrophysically abundant elements, lifetime measurements, line ratios, and wavelength measurements. In addition, we have performed many additional measurements in nuclear physics, and in support of diagnostics for laser fusion, for example. In this presentation we will give a detailed overview of x-ray calorimeter instruments in general and in our EBIT laboratory astrophysics program in particular. We will also discuss the science yield of our measurements at EBIT over the last decade) prospects for future science enabled by the current generation of spectrometers and that will be expanded in the near future by the next generation of spectrometers starting in 2611.

Porter, Frederick S.↗

DOE OSTI2023

Neutron calorimeter development at fission and fusion pulsed neutron sources

A neutron calorimeter fielded in pulsed neutron irradiation experiments at the National Ignition Facility (NIF) and White Sands Missile Range Fast Burst Reactor (WSMR FBR) is described, and results are provided and discussed. The calorimeter is modular in design to allow fielding of various neutron absorber materials and thicknesses, as well as use at both fission and fusion sources, all of which has been done. Neutron calorimeters designed for fission sources have been fielded at fusion sources as well, but these instances are not documented in available literature—making this work novel. The functional calorimeter consists of a neutron absorber and two sheathed, grounded thermocouples secured within a subassembly made of thermally insulating materials. This subassembly is placed into a sealed vessel for material and facility safety considerations. The device was fielded at NIF in four polar-direct-drive exploding pusher shots and eleven WSMR FBR pulses. Calorimeter data from NIF experiments show a discernable thermal response accredited to neutron heating within the first 10 s, but the data are dominated by noise from ambient X-ray heating after time = 10 s post-pulse. This response is highly consistent between shots and linearly related to incident neutron fluence and neutron absorber thickness. A temperature rise of 1.1E-2 K/(10 13 neutrons/cm 2 ) per millimeter of absorber thickness was determined for both 0.4 mm and 1 mm thick depleted uranium absorbers with linear best fit R 2 of 0.97 and 0.98 for each thickness and y-axis offsets of 8.8E-3 and 1.3E-2, respectively. WSMR FBR experiment data show a temperature rise of 6.2E-2 K/(10 13 neutrons/cm 2 ) with linear best fit R 2 of 0.14 and y-axis offset of 7.6E-3 for a calorimeter with a 1 mm thick enriched boron carbide ( 10 B 4 C) absorber, though it must be noted that device-to-device variability is significant at both facilities. So these data are also affected by noise on a similar timescale as at NIF, though the noise is significantly lesser in magnitude but oscillatory.

42 ENGINEERING↗

DOE OSTI2025

Gas-Gap Calorimeter Sizing and Rating Tools for Heat Pipe Experimentation

Effective gas-gap calorimeter sizing and rating tools are required to design calorimeters that enable well-defined operating conditions, high cooling powers, and accurate calorimetry. The present report describes two tools utilizing Microsoft Excel and MathWorks MATLAB that enable the sizing and rating of gas-gap calorimeters with a He-Ar binary gas mixture in the gap. The Excel tools are two easy-to-use spreadsheets for calculating heat pipe operating temperature or He-Ar mole fractions given the required inputs. The MATLAB tool includes similar models with more robust solution algorithms along with sub-options for full-vacuum, static gas-gap, and forced circulation in the gas-gap. The accuracy of the developed tools were demonstrated by comparing with existing work in literature. The MATLAB tool was used for a parametric study to determine the gas-gap thickness, coolant gap thickness, coolant flow rate, and coolant inlet temperatures for the testing of a 3/4 in outer diameter heat pipe up to powers of 10 kW and temperatures of 1,000°C. The effects of heat pipe and calorimeter inner shell surface emissivities were investigated, considering the inability to control or accurately measure surface emissivities in most applications. It was found that controlling the He-Ar mole fractions provides a wide operating range for gas-gap thicknesses around ~ 0.042--0.090 in (~ 1.07--2.29 mm) for a surface emissivity range of 0.4--0.8, since conduction heat transfer is a significant fraction of the heat transfer across the gas-gap. In addition, it was found that turbulent flow in the coolant gap is needed at high input powers to prevent shell temperatures from approaching the boiling temperature of the water coolant. The parametric study resulted in choosing stainless steel tubes with an outer diameter and thickness of 1 x 0.065 in as the inner shell, and a 1-1/2 x 0.156 in as the outer shell of the calorimeter. Overall, this report presents the necessary information for the sizing and rating of gas-gap calorimeters with He-Ar mixtures for the testing of high-temperature heat pipes (~ 500--1,000°C).

22 - GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2024

Lead tungstate calorimeters at Jefferson Lab and perspectives for the Electron–Ion Collider

Electromagnetic calorimeters based on PbWO4 scintillating crystals have a widespread applica- tion in experiments at different accelerator facilities such as CERN, FNAL, GSI, and Jefferson Lab. The unique properties of PbWO4 crystals, including a small radiation length and Molire radius, make them ideal for building high-granularity, radiation-hard detectors. This enables excellent spa- tial separation and energy resolution of reconstructed electromagnetic showers, making PbWO4 crystals the material of choice for numerous experiments. Lead tungstate calorimeters have been successfully used in several experiments at Jefferson Lab. Two large-scale detectors have been re- cently fabricated for future experiments : the Neutral Particle Spectrometer and the lead tungstate calorimeter of the GlueX detector. The future application of PbWO4 crystals in the ElectronIon Collider further highlights their ongoing importance in advancing experimental capabilities. In planning new experiments, the development of calorimeter instrumentation technologies becomes paramount. The integration of modern photodetectors, such as Silicon photomultipliers that are capable of operating in strong magnetic fields, and the implementation of streaming readout data acquisition systems, sophisticated shower reconstruction algorithms, and real-time data analysis are some examples of the continuously growing requirements of experimental setups. I will give an overview of the lead tungstate scintillating calorimeters and discuss some recent advancement in the calorimeter instrumentation.

Somov, Alexander↗

NASA NTRS1997

Energy Calibration of the Scintillating Optical Fiber Calorimeter Chamber (SOFCAL)

The Scintillating Optical Fiber Calorimeter (SOFCAL) detector is designed to make direct measures of the primary cosmic ray spectrum from -200 GeV/amu - 20 TeV/amu. The primary particles are resolved into groups according to their charge (p, He, CNO, Medium Z, Heavy Z) using both active and passive components integrated into the detector. The principal part of SOFCAL is a thin ionization calorimeter that measures the electromagnetic cascades that result from these energetic particles interacting in the detector. The calorimeter is divided into two sections: a thin passive emulsion/x-ray film calorimeter, and a fiber calorimeter that uses crossing layers of small scintillating optical fibers to sample the energy deposition of the cascades. The energy determination is made by fitting the fiber data to transition curves generated by Monte Carlo simulations. The fiber data must first be calibrated using the electron counts from the emulsion plates in the calorimeter for a small number of events. The technique and results of this calibration will be presented together with samples of the data from a balloon flight.

Christl, M. C.↗

NASA NTRS2001

An Imaging Calorimeter for Access-Concept Study

A mission concept study to define the "Advanced Cosmic-ray Composition Experiment for Space Station (ACCESS)" was sponsored by the National Aeronautics and Space Administration (NASA). The ACCESS instrument complement contains a transition radiation detector and an ionization calorimeter to measure tile spectrum of protons, helium, and heavier nuclei up to approximately 10(exp 15) eV to search for the limit of S/N shock wave acceleration, or evidence for other explanations of the spectra. Several calorimeter configurations have been studied, including the "baseline" totally active bismuth germanate instrument and sampling calorimeters utilizing various detectors. The Imaging Calorimeter for ACCESS (ICA) concept comprises a carbon target and a calorimeter using a high atomic number absorber sampled approximately each radiation length (rl) by thin scintillating fiber (SCIFI) detectors. The main features and options of the ICA instrument configuration are described in this paper. Since direct calibration is not possible over most of the energy range, the best approach must be decided from simulations of calorimeter performance extrapolated from CERN calibrations at 0.375 TeV. This paper presents results from the ICA simulations study.

Parnell, T. A.↗

NASA NTRS2009

X-Ray Calorimeter Arrays for Astrophysics

High-resolution x-ray spectroscopy is a powerful tool for studying the evolving universe. The grating spectrometers on the XMM and Chandra satellites started a new era in x-ray astronomy, but there remains a need for instrumentation that can provide higher spectral resolution with high throughput in the Fe-K band (around 6 keV) and can enable imaging spectroscopy of extended sources, such as supernova remnants and galaxy clusters. The instrumentation needed is a broad-band imaging spectrometer - basically an x-ray camera that can distinguish tens of thousands of x-ray colors. The potential benefits to astrophysics of using a low-temperature calorimeter to determine the energy of an incident x-ray photon via measurement of a small change in temperature was first articulated by S. H. Moseley over two decades ago. In the time since, technological progress has been steady, though full realization in an orbiting x-ray telescope is still awaited. A low-temperature calorimeter can be characterized by the type of thermometer it uses, and three types presently dominate the field. The first two types are temperature-sensitive resistors - semiconductors in the metal-insulator transition and superconductors operated in the superconducting-normal transition. The third type uses a paramagnetic thermometer. These types can be considered the three generations of x-ray calorimeters; by now each has demonstrated a resolving power of 2000 at 6 keV, but only a semiconductor calorimeter system has been developed to spaceflight readiness. The Soft X-ray Spectrometer on Astro-H, expected to launch in 2013, will use an array of silicon thermistors with I-IgTe x-ray absorbers that will operate at 50 mK. Both the semiconductor and superconductor calorimeters have been implemented in small arrays, kilo-pixel arrays of the superconducting calorimeters are just now being produced, and it is anticipated that much larger arrays will require the non-dissipative advantage of magnetic thermometers.

Kilbourne, Caroline A.↗

NASA NTRS2018

Uncertainty Analysis of Coaxial Thermocouple Calorimeters Used in Arc Jets

Recent introduction of Coaxial Thermocouple type calorimeters into the NASA Ames arc jet facilities has inspired an analysis of 2D conduction effects internal to this type of calorimeter. The 1D finite slab inverse analysis (which is typically used to deduce the heat transfer to the calorimeter) relies on the assumption that lateral conduction (i.e., 2D effects) is negligible. Most calorimeter bodies have a spherical nose, which in itself is a violation of the 1D finite slab analysis assumption. Secondly most calorimeters experience a variation in heating across the face of the body which is also a violation of the 1D finite slab analysis assumption. It turns out that these two effects tend to cancel each other to some extent. This paper shows the extent to which error exists in the analysis of the Coaxial Thermocouple type calorimeters, and also offers analysis strategies for reducing the errors.

Lateral Conduction↗

DOE OSTI2024

Comparison of point cloud and image-based models for calorimeter fast simulation

Score based generative models are a new class of generative models that have been shown to accurately generate high dimensional calorimeter datasets. Recent advances in generative models have used images with 3D voxels to represent and model complex calorimeter showers. Point clouds, however, are likely a more natural representation of calorimeter showers, particularly in calorimeters with high granularity. Furthermore, point clouds preserve all of the information of the original simulation, more naturally deal with sparse datasets, and can be implemented with more compact models and data files. In this work, two state-of-the-art score based models are trained on the same set of calorimeter simulation and directly compared.

47 OTHER INSTRUMENTATION↗

DOE OSTI2026

Commissioning of the large-scale lead tungstate scintillating calorimeter

Here, we report on the installation and initial commissioning of a large-scale lead tungstate (PbWO4) scintillating crystal calorimeter developed for high-rate photon detection and precise energy measurement. The calorimeter comprises 1596 high-granularity, high-resolution scintillating crystals optimized for electromagnetic-shower detection over a wide energy range. Scintillation light from each crystal is read out by Hamamatsu R4125 photomultiplier tubes equipped with a custom voltage divider and front-end amplifier to ensure stable gain at high rates. All calorimeter modules were fabricated and characterized using a light-emitting diode–based optical test system prior to installation to verify uniformity and photodetector performance. After installation, the electromagnetic calorimeter was fully integrated into the experiment data acquisition and energy-based trigger systems. The optical response of the modules was equalized using the light-monitoring system, cosmic-ray muons, and photons from Compton-scattering events. Commissioning results demonstrate a reliably calibrated optical response and stable detector performance during the first run. These results validate the calorimeter design and commissioning methodology for large-scale scintillator-based photonic instrumentation.

Analog to digital converters↗

DOE OSTI2024

The optimal use of segmentation for sampling calorimeters

One of the key design choices of any sampling calorimeter is how fine to make the longitudinal and transverse segmentation. Here, to inform this choice, we study the impact of calorimeter segmentation on energy reconstruction. To ensure that the trends are due entirely to hardware and not to a sub-optimal use of segmentation, we deploy deep neural networks to perform the reconstruction. These networks make use of all available information by representing the calorimeter as a point cloud. To demonstrate our approach, we simulate a detector similar to the forward calorimeter system intended for use in the ePIC detector, which will operate at the upcoming Electron Ion Collider. We find that for the energy estimation of isolated charged pion showers, relatively fine longitudinal segmentation is key to achieving an energy resolution that is better than 10% across the full phase space. These results provide a valuable benchmark for ongoing EIC detector optimizations and may also inform future studies involving high-granularity calorimeters in other experiments at various facilities.

47 OTHER INSTRUMENTATION↗

DOE OSTI2025

A gravity-based mounting approach for large-scale cryogenic calorimeter arrays

Cryogenic calorimeters are among the leading technologies for searching for rare events. The CUPID experiment is exploiting this technology to deploy a tonne-scale detector to search for neutrinoless double-beta decay of 100 Mo. The CUPID collaboration proposed an innovative approach to assembling cryogenic calorimeters in a stacked configuration, held in position solely by gravity. This gravity-based assembly method is unprecedented in the field of cryogenic calorimeters and offers several advantages, including relaxed mechanical tolerances and simplified construction. To assess and optimize its performance, we constructed a medium-scale prototype hosting 28 Li 2 MoO 4 crystals and 30 Ge light detectors, both operated as cryogenic calorimeters at the Laboratori Nazionali del Gran Sasso (Italy). Despite an unexpected excess of noise in the light detectors, the results of this test proved (i) a thermal stability better than ±0.5 mK at 10 mK, (ii) a good energy resolution of Li 2 MoO 4 cryogenic calorimeters, (6.6 ± 2.2) keV FWHM at 2615 keV, and (iii) a Li 2 MoO 4 light yield measured by the closest light detector of 0.36 keV/MeV, sufficient to guarantee the particle identification requested by CUPID.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

NASA NTRS1990

Development of a scintillating optical fiber ionization calorimeter

A design study of a scintillation fiber (SF) calorimeter for a cosmic ray observation is made. An evaluation of various fibers and design configuration was made. The proposed design has a dimension of 1 m (W) x 1 m (L) x 16 cm (H) contains 1000 fibers at each of 40 x- or 40 y-layers interleaved with 1mm thick leadplates. Two or four CCD Particle Track Imaging Systems are connected to a bundle of SF edges at x- and y-ends. The overall weight of a calorimeter is 1,200 kg including read-out systems and supporting boards. The designed calorimeter can measure cosmic ray nuclei and gamma-rays with position, angles and energy information suitable for detailed spectrum analysis. The system is particularly beneficial at very high energies where the flux is extremely low and it requires a very long exposure over many years in space. Emulsion chambers have an advantage for cosmic ray measurements if the exposure is limited to several months in space. In fact, the most important energy region for the current cosmic ray studies is at around 1,000 TeV where a drastic change of elemental composition is indicated by various indirect observations. A detector whose size is in the order of 1 m(sup 2) requires several years of exposure in space accumulate sufficient statistics near 1,000 TeV. Emulsions will be strongly contaminated by background radiation for such a long duration flight, while SF calorimeter is totally immune from this concern. This is particularly important for long-duration experiments. The SF calorimeter also allows time-tagging of individual events, extending the experimental capability in various ways.

Takahashi, Y.↗

NASA NTRS1993

Calibration of a calorimeter for measuring the performance of thermal control surfaces

The calibration to evaluate the heat leak in terms of the deviation from a perfect calorimeter is described. A thermal vacuum test was carried out to characterize the performance of the calorimeter. The calorimeter was equipped with a heater to control the sample disc temperature and with specific instrumentation to measure the heat leak. The radiation sink temperature of the black cavity target was varied from -192 to +31C, while the heater power was varied from 0 to 311 milliwatts. A steady state thermal model was developed to correlate the results. The calorimeter performance was characterized in terms of the heat leak as a percentage of the ideal heat flow of the calorimeter disc. Large deviations from ideal performance occur at low sink temperatures. The effect of the use of the heater is discussed. The effects of transient conditions during low Earth orbit are discussed. It is concluded that heat leak calibrations are necessary for a wide range of conditions.

Houseman, John↗