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Tl2InBi crystallizes in the orthorhombic Immm space group. The structure is one-dimensional and consists of two Tl2InBi ribbons oriented in the (1, 0, 0) direction. Tl is bonded in a linear geometry to one In and one Bi atom. The Tl–In bond length is 2.87 Å. The Tl–Bi bond length is 2.78 Å. In is bonded in a linear geometry to two equivalent Tl atoms. Bi is bonded in a linear geometry to two equivalent Tl atoms.
TlIn2Bi crystallizes in the orthorhombic Immm space group. The structure is one-dimensional and consists of two TlIn2Bi ribbons oriented in the (1, 0, 0) direction. Tl is bonded in a linear geometry to two equivalent In atoms. Both Tl–In bond lengths are 2.89 Å. In is bonded in a linear geometry to one Tl and one Bi atom. The In–Bi bond length is 2.73 Å. Bi is bonded in a linear geometry to two equivalent In atoms.