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Birefringent coating for strain measurements on large surfaces contains constituents that can be premixed and sprayed as a single component with conventional paint spray equipment. Elevated temperatures are not required for spraying or curing of the coating material which has long pot life.
Epoxy birefringent coatings for nondestructive testing of honeycomb sandwich structures
A structural specimen coated with or constructed of photoelastic material, when illuminated with circularly polarized light will, when stressed: reflect or transmit elliptically polarized light, the direction of the axes of the ellipse and variation of the elliptically light from illuminating circular light will correspond to and indicate the direction and magnitude of the shear stresses for each illuminated point on the specimen. The principles of this invention allow for several embodiments of stress analyzing apparatus, ranging from those involving multiple rotating optical elements, to those which require no moving parts at all. A simple polariscope may be constructed having two polarizing filters with a single one-quarter waveplate placed between the polarizing filters. Light is projected through the first polarizing filter and the one-quarter waveplate and is reflected from a sub-fringe birefringent coating on a structure under load. Reflected light from the structure is analyzed with a polarizing filter. The two polarizing filters and the one-quarter waveplate may be rotated together or the analyzer alone may be rotated. Computer analysis of the variation in light intensity yields shear stress magnitude and direction.
Uniaxial tensile tests conducted on a variety of graphite/epoxy laminates, containing narrow rectangular slits, square or circular holes with various aspect ratios are discussed. The techniques used to study stable crack or damage zone growth--namely, birefringence coatings, COD gages, and microscopic observations are discussed. Initial and final fracture modes are discussed as well as the effect of notch size and shape, and laminate type on the fracture process. Characteristic lengths are calculated and compared to each other using the point, average and inherent flaw theories. Fracture toughnesses are calculated by the same theories and compared to a boundary integral equation technique. Finite width K-calibration factors are also discussed.
The results of uniaxial tensile tests conducted on a variety of graphite/epoxy laminates containing narrow rectangular slits and square or circular holes with various aspect ratios are discussed. The techniques used to study stable-crack or damage-zone growth - namely, birefringence coatings, COD gages, and microscopic observations are discussed. Initial and final-fracture modes are discussed as well as the effect of notch size and shape and laminate type on the fracture process. Characteristic lengths are calculated using the point, average and inherent flaw theories and comparisons with observations are discussed. Further, the effect of flaw geometry on stress states and deformations is assessed.
Visual observation inspection device for bonded honeycomb sandwich structures using birefringent plastic coatings
Stress distribution about a slowly growing crack determined by photoelastic-coating method
Birefringent technique to observe plastic strain concentration during tensile tests of copper strip specimens containing arrays of discontinuities
Formulations and properties of low modulus, birefringent polyurethane resins
Environment, mixing, casting, cure and calibration effects on clear bubble-free low modulus polyurethane birefringent resins
Liquid crystals for nondestructive thermographic analysis of flaws in bonded structures
This innovation consists of a new composition of matter where single-walled carbon nanotubes (SWNTs) are grown in aligned arrays from nanostructured flakes that are coated in Fe catalyst. This method of growth of aligned SWNTs, which can yield well over 400 percent SWNT mass per unit substrate mass, exceeds current yields for entangled SWNT growth. In addition, processing can be performed with minimal wet etching treatments, leaving aligned SWNTs with superior properties over those that exist in entangled mats. The alignment of the nanotubes is similar to that achieved in vertically aligned nanotubes, which are called "carpets. " Because these flakes are grown in a state where they are airborne in a reactor, these flakes, after growing SWNTs, are termed "flying carpets. " These flakes are created in a roll-to-roll evaporator system, where three subsequent evaporations are performed on a 100-ft (approx. =30-m) roll of Mylar. The first layer is composed of a water-soluble "release layer, " which can be a material such as NaCl. After depositing NaCl, the second layer involves 40 nm of supporting layer material . either Al2O3 or MgO. The thickness of the layer can be tuned to synthesize flakes that are larger or smaller than those obtained with a 40-nm deposition. Finally, the third layer consists of a thin Fe catalyst layer with a thickness of 0.5 nm. The thickness of this layer ultimately determines the diameter of SWNT growth, and a layer that is too thick will result in the growth of multiwalled carbon nanotubes instead of single-wall nanotubes. However, between a thickness of 0.5 nm to 1 nm, single-walled carbon nanotubes are known to be the primary constituent. After this three-layer deposition process, the Mylar is rolled through a bath of water, which allows catalyst-coated flakes to detach from the Mylar. The flakes are then collected and dried. The method described here for making such flakes is analogous to that which is used to make birefringent ink that is coated on U.S. currency. After deposition, the growth is carried out in a hot-filament chemical vapor deposition apparatus. A tungsten hot filament placed in the flow of H2 at a temperature greater than 1,600 C creates atomic hydrogen, which serves to reduce the Fe catalyst into a metallic state. The catalyst can now precipitate SWNTs in the presence of growth gases. The gases used for the experiments reported are C2H2, H2O, and H2, at rates of 2, 2, and 400 standard cubic centimeters per minute (sccm), respectively. In order to retain the flakes, a cage is constructed by spot welding stainless steel or copper mesh to form an enclosed area, in which the flakes are placed prior to growth. This allows growth gases and atomic hydrogen to reach the flakes, but does not allow the flakes, which rapidly nucleate SWNTs, to escape from the cage.
The birefringence of bare and coated substrates for magneto-optical recording is experimentally investigated using ellipsometry at the wavelengths of 632.8 nm and 780 nm. The rotation and ellipticity of the polarization state of the reflected or transmitted light is measured for different incident angles and different orientations of the incident linear polarization. The measured data is then fitted by a computer program which solves the Maxwell equations for the plane-wave propagation in a multilayer structure and minimizes the error between the measured and calculated data by adjusting the unknown parameters of the multilayer. This approach enables us to determine orientations of the three principal axes in the substrate and the corresponding refractive indices. A special feature of our ellipsometers is that a glass hemisphere is placed in contact with the substrate, which eliminates the refraction of the incident light and enables a maximum propagation angle of 70 degrees (with respect to the normal) in the substrate. This increases the sensitivity of the measurement. Certain anomalies were observed, which we believe are associated with the presence of grooves on these substrates.
Anisotropic phase retarders, used in high power laser facilities to perform polarization smoothing, can be obtained by the glancing angle deposition (GLAD) coating process. Due to its high laser resistance, the coatings are mainly made of silica. Therefore, limited attention has been given to other dielectric materials. Here we present a study on alumina GLAD anisotropic coatings; a material with high laser resistance, higher birefringence and lower environmental sensitivity than silica. Since the anisotropy is related to the coatings microstructure through the deposition angle, samples were coated at angles varying from ± 68° to ± 82° using the serial bideposition technique. They were characterized by ellipsometry, polarimetry, spectrophotometry and electron microscopy. We showed that the highest birefringence is obtained at a deposition angle of ± 76° with an in-plane value of 0.053. Based on these results, a quarter-wave plate at 351 nm was designed as a multilayer with seven pairs of anisotropic layers deposited at ± 76° and isotropic layers deposited at 0°. The fabricated coating exhibited a uniform retardance of 88.51 ± 0.45 nm. The alumina GLAD wave plates presented here, open the door to new possibilities in the laser field and especially in the field of fusion energy.
Highly stabilized lasers are an increasingly valuable tool for metrology. For many applications, however, existing Fabry Perot systems are too bulky and cumbersome. We are investigating the use of miniature monolithic whispering gallery mode resonators as reference cavities for laser stabilization. We seek to exploit the benefit of small size and vibration resistance by suppressing thermally induced frequency fluctuations. We have theoretically investigated the viability of using a thin-film coating to achieve temperature compensation. We have experimentally investigated an active temperature stabilization scheme based on birefringence in a crystalline resonator. We also report progress of laser locking to the resonators.
During a space mission, spacecraft surface materials are exposed to various damaging environmental factors including high-energy photons, electrons, atomic oxygen (AO) neutrals and ions, micrometeoroids and orbital debris, vacuum, and large temperature fluctuations. The resulting change in spacecraft material properties can significantly impact the performance and durability of spacecraft systems. Even though all aspects of the space environment can lead to the deterioration of spacecraft components, in low Earth orbit (LEO), the threat posed by AO is especially severe in terms of structural and optical damage, particularly to exterior spacecraft components that are susceptible to oxidation. A comprehensive understanding of material AO-induced weathering is essential for mission planning in the LEO environment. The presented work aims to evaluate the alterations in mechanical properties of selected innovative spacecraft materials and surface electronic system designs, such as Kapton® CR film coated front and back-side with polyimide coating containing AO-resistant filler, Kevlar EXO, and Bendable Electrodynamic Dust Shield (BEDS) architecture, under simulated AO exposure, utilizing the photoelasticity phenomenon in which birefringence is induced in a material when it is subjected to mechanical stress. Changes in stress patterns during the deformation of AO-exposed polymers were assessed using a large-field polariscope under varied deformation types. Patterns of colors were used for qualitative evaluations of residual stress. The stress patterns of the AO-exposed polymers were compared to those of the unexposed ones. Also, these patterns were correlated with data from Bidirectional Reflectance Distribution Function (BRDF) and surface morphology studies.
This NASA Technical Memorandum summarizes windowpane optical analyses for the OSIRIS-REx (Origins, Spectral Interpretation, Resource Identification and Security Regolith Explorer) mission [1] supported by the SCIFLI (Scientifically Calibrated In-Flight Imagery) team [2] at NASA Langley Research Center (NASA LaRC). The SCIFLI team led a NASA multi-center team in characterization of fused silica (FS) and anti-reflective coated (AR-coated) sapphire materials for use as aircraft windowpanes. These materials were needed for the Hypervelocity OSIRIS-REx Reentry Imaging & Spectroscopy (HORIS) mission and were tested to generate performance parameters relevant to the flight environment. Some of the assessed parameters included optical quality, transmittance, reflectance, color balance, birefringence, transmitted wavefront error, wedge, and haziness of the windows. In order to evaluate the material characteristics in a uniform manner, several criteria were held constant. For example, the physical dimensions of the test articles were held constant (i.e., 17-inch diameter aircraft windowpane and 2-inch diameter witness samples). In this way, the comparison of test results from one material specimen to another was invariant with regard to the manner in which the tests were conducted. This also reduced the variability in how the data were reported. As a result, the results shown in this report, including test data generated by NASA can be used for windowpane material evaluation and future material design trades. Window designers can use the data and the testing method along with the testing matrices to efficiently match material performance to their design and mission objectives and requirements. Standardized testing methodologies and data reduction procedures are described in this report. Unless otherwise noted in the data itself, all the windowpane materials were tested in order to characterize their performance for the HORIS mission. One appendix has been included in this report. These include detailed wavefront interferograms of transmitted wavefront error and optical wedge used in the generation of aggregated material performance.
Far and extreme ultraviolet optical thin film filters find many uses in space astronomy, space astrophysics, and space aeronomy. Spacebased spectrographs are used for studying emission and absorption features of the earth, planets, sun, stars, and the interstellar medium. Most of these spectrographs use transmission or reflection filters. This requirement has prompted a search for selective filtering coatings with high throughput in the FUV and EUV spectral region. Important progress toward the development of thin film filters with improved efficiency and stability has been made in recent years. The goal for this field is the minimization of absorption to get high throughput and enhancement of wavelength selection. The Optical Aeronomy Laboratory (OAL) at the University of Alabama in Huntsville has recently developed the technology to determine optical constants of bulk and film materials for wavelengths extending from x-rays (0.1 nm) to the FUV (200 nm), and several materials have been identified that were used for designs of various optical devices which previously have been restricted to space application in the visible and near infrared. A new design concept called the Pi-multilayer was introduced and applied to the design of optical coatings for wavelengths extending from x-rays to the FUV. Section 3 of this report explains the Pi-multilayer approach and demonstrates its application for the design and fabrication of the FUV coatings. Two layer Pi-stacks have been utilized for the design of reflection filters in the EUV wavelength range from 70 - 100 nm. In order to eliminate losses due to the low reflection of the imaging optics and increase throughput and out-of-band rejection of the EUV instrumentation we introduced a self-filtering camera concept. In the FUV region, MgF2 and LiF crystals are known to be birefringent. Transmission polarizers and quarterwave retarders made of MgF2 or LiF crystals are commercially available but the performances are poor. New techniques for the design of the EUV and FUV polarizers and quarterwave retarders are described in Section 5. X- and gamma-ray detectors rely on a measurement of the electron which is effected when a ray interacts with matter. The design of an x- and gamma-ray telescope to operate in a particular region of the spectrum is, therefore, largely dictated by the mechanism through which the rays interact. Energy selection and the focusing of the incident high energy rays can be achieved with spectrally selective high reflective multilayers. The design and spectral performance of narrowband reflective x-ray Pi-multilayers are presented in section 6.