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DOE OSTI2022

LLNL FY2022 Aging and Lifetimes Exit Criteria: Milestone 8118, GC#3

Adhesives and adhesive-bond joints play a critical role in many applications across the national security enterprise. They are ubiquitous and their aging performance can impact the physical and chemical behavior of complex systems. Previously, we have explored the chemical aging behavior of polyurethane adhesives (Halthane 73-18, Halthane 88-3, and Wilethane 44) exposed to varying levels of radiation and identified the primary chemical degradation products. In this work, we expand upon our analysis to understand how the mechanical properties of adhesives-bonded joints behave after radiation exposure.

36 MATERIALS SCIENCE↗

DOE OSTI2025

$Ξ$ 𝑐 → $Ξ$ form factors from lattice QCD with domain-wall quarks: A new piece in the puzzle of $Ξ^0_𝑐$ decay rates

We present a lattice quantum chromodynamics (QCD) determination of the vector and axial-vector form factors that describe the charm-baryon semileptonic decays Ξ 𝑐 → Ξ⁢ℓ + ⁢𝜈 ℓ . The calculation uses a domain-wall action for the up, down, and strange quarks, and an anisotropic clover action for the charm quark. We use four ensembles of gauge-field configurations generated by the RBC and UKQCD collaborations, with lattice spacings between 0.111 and 0.073 fm and pion masses ranging from 420 to 230 MeV. We present Standard Model predictions for the decay rates and branching fractions of Ξ$^0_𝑐$ → Ξ$^−_𝑐$⁢ℓ + ⁢𝜈 ℓ and Ξ$^+_𝑐$ → Ξ$^0_𝑐$⁢ℓ + ⁢𝜈 ℓ for ℓ =𝑒, 𝜇. In particular, we obtain Γ⁡(Ξ$^0_𝑐$ → Ξ − ⁢𝑒 + ⁢𝜈 𝑒 )/|𝑉 𝑐⁢𝑠 | 2 = 0.2515⁢(73) ps −1 and ℬ⁡(Ξ$^0_𝑐$ → Ξ − ⁢𝑒 +⁢ 𝜈 𝑒 ) = 3.58⁢(12)%. These values are higher than those predicted by a previous lattice calculation and substantially higher than the experimentally measured values, but consistent with expectations from approximate 𝑆⁢𝑈⁡(3) flavor symmetry.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2020

Directivity Modes of Earthquake Populations with Unsupervised Learning

We present a novel approach for resolving modes of rupture directivity in large populations of earthquakes. A seismic spectral decomposition technique is used to first produce relative measurements of radiated energy for earthquakes in a spatially compact cluster. The azimuthal distribution of energy for each earthquake is then assumed to result from one of several distinct modes of rupture propagation. Rather than fitting a kinematic rupture model to determine the most likely mode of rupture propagation, we instead treat the modes as latent variables and learn them with a Gaussian mixture model. The mixture model simultaneously determines the number of events that best identify with each mode. The technique is demonstrated on four datasets in California, each with compact clusters of several thousand earthquakes with comparable slip mechanisms. We show that the datasets naturally decompose into distinct rupture propagation modes that correspond to different rupture directions, and the fault plane is unambiguously identified for all cases. We find that these small earthquakes exhibit unilateral ruptures 63–73% of the time on average. Here, the results provide important observational constraints on the physics of earthquakes and faults.

58 GEOSCIENCES↗

DOE OSTI2024

An electrochemical generator for the continual supply of 213 Bi from 225 Ac for use in targeted alpha therapy applications

Bismuth-213 is a radionuclide of interest for targeted alpha therapy and is supplied via a radiochemical generator system through the decay of 225 Ac. Radionuclide generators employ longer lived “parent” radionuclides to routinely supply shorter-lived “daughter” radionuclides. The traditional 225 Ac/ 213 Bi radiochemical generator relies on an organic cation exchange resin where 225 Ac binds to the resin and 213 Bi is routinely eluted. These resins degrade when they absorb large doses of ionizing radiation (>1 × 10 6 Gy/mg), which has been observed when the loading activity of 225 Ac exceeds 2.59*10 9 Bq (70 mCi). Herein we report the development of an electrochemical generator for the supply of 213Bi that has the potential to overcome this limitation. Bismuth-213 spontaneously electrodeposits onto nickel foils in 0.1 M hydrochloric acid at 70 °C. Using this method, we were able to plate an average of 73 ± 4 % of the 213 Bi in solution and obtain a final 213 Bi recovery of 65 ± 8 % in 0.1 M citrate pH 4.5 via reverse electrolysis using titanium as the cathode. The recovered 213Bi had an average radiochemical purity of >99.8 % and was successfully used to radiolabel DOTATATE with an average radiochemical yield of 85.1 % (not optimized).

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗