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At least 19 records

Space environmental effects on graphite-epoxy compressive properties and epoxy tensile properties

This study characterizes the effects of electron radiation and temperature on a graphite-epoxy composite material. Compressive properties of the T300/934 material system were obtained at -250 F (-157 C), room temperature, and 250 F (121 C). Tensile specimens of the Fiberite 934 epoxy resin were fabricated and tested at room temperature and 250 F (121 C). Testing was conducted in the baseline (nonirradiated) and irradiated conditions. The radiation exposure was designed to simulate 30 year, worst-case exposure in geosynchronous Earth orbit. Mechanical properties tended to degrade at elevated temperature and improve at cryogenic temperature. Irradiation generally degraded properties at all temperatures.

Fox, Derek J.↗

Mechanical properties of neat polymer matrix materials and their unidirectional carbon fiber-reinforced composites

The mechanical properties of two neat resin systems for use in carbon fiber epoxy composites were characterized. This included tensile and shear stiffness and strengths, coefficients of thermal and moisture expansion, and fracture toughness. Tests were conducted on specimens in the dry and moisture-saturated states, at temperatures of 23, 82 and 121 C. The neat resins tested were American Cyanamid 1806 and Union Carbide ERX-4901B(MPDA). Results were compared to previously tested neat resins. Four unidirectional carbon fiber reinforced composites were mechanically characterized. Axial and transverse tension and in-plane shear strengths and stiffness were measured, as well as transverse coefficients of thermal and moisture expansion. Tests were conducted on dry specimens only at 23 and 100 C. The materials tested were AS4/3502, AS6/5245-C, T300/BP907, and C6000/1806 unidirectional composites. Scanning electron microscopic examination of fracture surfaces was performed to permit the correlation of observed failure modes with the environmental test conditions.

Zimmerman, Richard S.↗

Comparison of predicted and measured elastohydrodynamic film thickness in a 20-millimeter-bore ball bearing

Elastohydrodynamic film thicknesses were measured for a 20-mm bore ball bearing using the capacitance technique. The bearing was thrust loaded to 90, 445, and 778 N (20, 100, and 175 lb). The corresponding maximum contact stress on the inner race was 1.28, 2.09, and 2.45 GPa (185 000, 303,000, and 356, 000 psi). Test speeds ranged from 400 to 15,000 rpm. Measurements were taken with four different lubricants: (1) synthetic paraffinic; (2) synthetic paraffinic with additives; (3) synthetic type II aircraft oil; and (4) synthetic cycloaliphatic hydrocarbon traction fluid. The test bearing was mist lubricated. Test temperatures were 27, 65, and 121 C (80, 150, and 250 F). The measured results for the various test parameters were compared to theoretical predictions from computer programs. Also the data were plotted on dimensionless coordinates and compared to several classical isothermal theories.

Coy, J. J.↗

Behavior of composite bolted joints at elevated temperature

Experimental results from an investigation which examines the combined effects of temperature, joint geometry and out-of-plane constraint upon the response of mechanically fastened composite joints are presented. Data are presented for simulated mechanically fastened joint conditions in two laminate configurations fabricated from Hercules AS/3501-6 graphite-epoxy. Strength and failure mode results are presented for the test temperatures of 21 C, 121 C and 177 C and for a range of the geometric parameters W/D and e/D from 3.71 to 7.43 and 1.85 to 3.69, respectively. A hole diameter, D of 5.16 mm was utilized for all tests. Pin bearing tests with out-of-plane constraint were conducted at room temperature only. All elevated temperature data were generated for pin bearing conditions. Ultrasonic C scan inspection of the failed specimens was employed to assess the damage region and to determine failure mode. Comparative data are presented for pin bearing and out-of-plane constraint conditions for the above mentioned joint configurations. The joint under pin loading was modeled by two dimensional finite element methods. Predicted net section strain concentrations were compared with experimental results.

Wilson, D. W.↗

Evaluation of an oil-debris monitoring device for use in helicopter transmissions

Experimental tests were performed on an OH-58A helicopter main-rotor transmission to evaluate an oil-debris monitoring device (ODMD). The tests were performed in the NASA 500-hp Helicopter Transmission Test Stand. Five endurance tests were run as part of a U.S. Navy/NASA/Army advanced lubricants program. The tests were run at 100 percent design speed, 117-percent design torque, and 121 C (250 F) oil inlet temperature. Each test lasted between 29 and 122 hr. The oils that were used conformed to MIL-L-23699 and DOD-L-85734 specifications. One test produced a massive sun-gear fatigue failure; another test produced a small spall on one sun-gear tooth; and a third test produced a catastrophic planet-bearing cage failure. The ODMD results were compared with oil spectroscopy results. The capability of the ODMD to detect transmission component failures was not demonstrated. Two of the five tests produced large amounts of debris. For these two tests, two separate ODMD sensors failed, possibly because of prolonged exposure to relatively high oil temperatures. One test produced a small amount of debris and was not detected by the ODMD or by oil spectroscopy. In general, the ODMD results matched the oil spectroscopy results. The ODMD results were extremely sensitive to oil temperature and flow rate.

Lewicki, David G.↗

Experimental evaluation of a translating nozzle sidewall radial turbine

Studies have shown that reduced specific fuel consumption of rotorcraft engines can be achieved with a variable capacity engine. A key component in such an engine in a high-work, high-temperature variable geometry gas generator turbine. An optimization study indicated that a radial turbine with a translating nozzle sidewall could produce high efficiency over a wide range of engine flows but substantiating data were not available. An experimental program with Teledyne CAE, Toledo, Ohio was undertaken to evaluate the moving sidewall concept. A variety of translating nozzle sidewall turbine configurations were evaluated. The effects of nozzle leakage and coolant flows were also investigated. Testing was done in warm air (121 C). The results of the contractual program were summarized.

Roelke, Richard J.↗

Flight test measurements and analysis of sonic boom phenomena near the shock wave extremity

The sonic boom flight test program conducted at Jackass Flats, Nevada, during the summer and fall of 1970 consisted of 121 sonic-boom-generating flights over the 1500 ft instrumented BREN tower. This test program was designed to provide information on several aspects of sonic boom, including caustics produced by longitudinal accelerations, caustics produced by steady flight near the threshold Mach number, sonic boom characteristics near lateral cutoff, and the vertical extent of shock waves attached to near-sonic airplanes. The measured test data, except for the near-sonic flight data, were analyzed in detail to determine sonic boom characteristics for these flight conditions and to determine the accuracy and the range of validity of linear sonic boom theory. The caustic phenomena observed during the threshold Mach number flights and during the transonic acceleration flights are documented and analyzed in detail. The theory of geometric acoustics is shown to be capable of predicting shock wave-ground intersections, and current methods for calculating sonic boom pressure signature away from caustics are shown to be reasonably accurate.

Haglund, G. T.↗

Preventing Damaging Pressure Gradients at the Walls of an Inflatable Space System

An inflatable structural system to deploy a space system such as a solar shield, an antenna or another similar instrument requires a stiffening element after it is extended by the inflated gas pressure. The stiffening element has to be packaged in folded configuration before the deployment. It must be relatively small, lightweight, non-damaging to the inflated system and be able to become stiff in a short time. One stiffening method is to use a flexible material inserted in the deployable system, which, upon a temperature curing, can become stiff and is capable of supporting the entire structure. There are two conditions during the space operations when the inflated volume could be damaged: during the transonic region of the launch phase and when the curing of the rigidizing element occurs. In both cases, an excess of pressure within the volume containing the rigid element could burst the walls of the low-pressure gas inflated portion of the system. This paper investigates those two conditions and indicates the vents, which will prevent those damaging overpressures. Vent openings at the non-inflated volumes have been calculated for the conditions existing during the launch. Those vents allow the initially folded volume to exhaust the trapped atmospheric gas at approximately the same rate as the ambient pressure drops. That will prevent pressure gradients across the container walls which otherwise could be as high as 14.7 psi. The other condition occurring during the curing of the stiffening element has been investigated. This has required the testing of the element to obtain the gas generation during the curing and the transformation from a pliable material to a rigid on The tested material is a composite graphite/epoxy weave. The outgassing of the uncured sample at 121 deg Celcius was carried with the Cahn Microbalance and with other outgassing facilities including the micro-CVCM ASTM E-595 facility. The test provided the mass of gas evolved during the test. That data, including the chemical nature of the evolved gas, provided the data for the calculation of the pressure produced within the volume. The evaluation of the areas of the vents that would prevent excessive pressures and provide a rapid release of the gas away from contamination sensitive surfaces has be carried out. The pressure decay with time has been indicated.

Scialdone, John J.↗

Influence of electron radiation and temperature on the cyclic, matrix dominated response of graphite-epoxy

The effects of electron radiation and elevated temperature on the matrix-dominated cyclic response of standard T300/934 and a chemically modified T300/934 graphite-epoxy are characterized. Both materials were subjected to 1.0 x 10 to the 10th rads of 1.0 MeV electron irradiation, under vacuum, to simulate 30 years in geosynchronous orbit. Cyclic tests were performed at room temperature and elevated temperature (121 C) on 4-ply unidirectional laminates to characterize the effects associated with irradiation and elevated temperature. Both materials exhibited energy dissipation in their response at elevated temperature. The irradiated modified material also exhibited energy dissipation at room temperature. The combination of elevated temperature and irradiation resulted in the most severe effects in the form of lower proportional limits, and greater energy dissipation. Dynamic-mechanical analysis demonstrated that the glass transition temperature, T(g), of the standard material was lowered 39 C by irradiation, wereas the T(g) of the modified material was lowered 28 C by irradiation. Thermomechanical analysis showed the occurrence of volatile products generated upon heating of the irradiated materials.

Reed, Susan M.↗

Establishment of quality, reliability and design standards for low, medium, and high power microwave hybrid microcircuits

Quality, reliability, and design standards for microwave hybrid microcircuits were established. The MSFC Standard 85M03926 for hybrid microcircuits was reviewed and modifications were generated for use with microwave hybrid microcircuits. The results for reliability tests of microwave thin film capacitors, transistors, and microwave circuits are presented. Twenty-two microwave receivers were tested for 13,500 unit hours. The result of 111,121 module burn-in and operating hours for an integrated solid state transceiver module is reported.

Robinson, E. A.↗

Mechanical properties characterization of composite sandwich materials intended for space antenna applications

The composite materials proposed for use in the Advanced Communications Technology Satellite (ACTS) Program contains a new, high modulus graphite fiber as the reinforcement. A study was conducted to measure certain mechanical properties of the new fiber-reinforced material as well as of a composite-faced aluminum honeycomb sandwich structure. Properties were measured at -157, 22, and 121 C. Complete characterization of this material was not intended. Longitudinal tensile, picture-frame shear, short-beam shear, and flexural tests were performed on specimens of the composite face-sheet materials. Unidirectional, cross-plied, and quasi-isotropic fiber composite ply layup designs were fabricated and tested. These designs had been studied by using NASA's Integrated Composite Analyzer (ICAN) computer program. Flexural tests were conducted on (+/- 60/0 deg) sub s composite-faced sandwich structure material. Resistance strain gages were used to measure strains in the tensile, picture-frame, and sandwich flexural tests. The sandwich flexural strength was limited by the core strength at -157 and 22 C. The adhesive bond strength was the limiting factor at 121 C. Adhesive mechanical properties are reflected in sandwich structure flexural properties when the span-to-depth ratio is great enough to allow a significant shear effect on the load-deflection behavior of the sandwich beam. Most measured properties agreed satisfactorily with the properties predicted by ICAN.

Bowles, Kenneth J.↗

Mechanical properties characterization of composite sandwich materials intended for space antenna applications

The composite materials proposed for use in the Advanced Communications Technology Satellite (ACTS) program contains a new, high modulus graphite fiber as the reinforcement. A study was conducted to measure certain mechanical properties of the new fiber-reinforced material as well as of a composite-faced aluminum honeycomb sandwich structure. Properties were measured at -157, 22, and 121 C. Complete characterization of this material was not intended. Longitudinal tensile, picture-frame shear, short-beam shear, and flexural tests were performed on specimens of the composite face-sheet materials. Unidirectional, cross-plied, and quasi-isotropic fiber composite ply layup designs were fabricated and tested. These designs had been studied by using NASA's Integrated Composite Analyzer (ICAN) computer program. Flexural tests were conducted on (+/- 60/0 deg) sub s composite-faced sandwich structure material. Resistance strain gages were used to measure strains in the tensile, picture-frame, and sandwich flexural tests. The sandwich flexural strength was limited by the core strength at 157 and 22 c. The adhesive bond strength was the limiting factor at 121 C. Adhesive mechanical properties are reflected in sandwich structure flexural properties when the span-to-depth ratio is great enough to allow a significant shear effect on the load-deflection behavior of the sandwich beam. Most measured properties agreed satisfactorily with the properties predicted by ICAN.

Bowles, Kenneth J.↗

A Scheme for finding the Front Boundary of an Interplanetary Magnetic Cloud

We developed a scheme for finding the front boundary of an interplanetary magnetic cloud (MC) based on criteria that depend on the possible existence of any one or all of six specific solar wind features. The features that the program looks for, within +/- 2 hours of a preliminarily determined time for the front boundary, estimated either by visual inspection or by an automatic MC identification scheme, are: (1) a sufficiently large directional discontinuity in the interplanetary magnetic field (IMF), (2) existence of a magnetic hole, (3) a significant proton plasma beta drop, (4) a significant proton temperature drop, (5) a marked increase in the IMF's intensity, and (6) a significant decrease in a normalized root-mean-square deviation (RMS)of the magnetic field - where the scheme was tested using 5, 10, 15, and 20 minute averages of the relevant physical quantities, in order to find the optimum average (and RMS) to use. Other criteria, besides these six, were examined and dismissed as not reliable, e.g., plasma speed. The scheme was developed specifically for aiding in forecasting the strength and timing of a geomagnetic storm due to the passage of an interplanetary MC in real-time, but can be used in post ground-data collection for imposition of consistency in choosing a MC's front boundary. The scheme has been extensively tested, first using 80 bona fide MCs over about 9 years of WIND data, and also for 121 MC-like structures as defined by a program that automatically identifies such structures over the same period. Optimum limits for various parameters in the scheme were found by statistical studies of the WIND MCs. The resulting limits can be user-adjusted for other data sets, if desired. Final testing of the 80 MCs showed that for 50 percent of the events the boundary estimates occurred within +/-10 minutes of visually determined times, 80 percent occurred within +/-30 minutes, and 91 percent occur within +/-60 minutes, and three or more individual boundary tests were passed for 88 percent of the total MCs. The scheme and its testing will be described.

Lepping, Ronald P.↗

Technical Evaluation Motor 3 (TEM-3)

A primary objective of the technical evaluation motor program is to recover the case, igniter and nozzle hardware for use on the redesigned solid rocket motor flight program. Two qualification objectives were addressed and met on TEM-3. The Nylok thread locking device of the 1U100269-03 leak check port plug and the 1U52295-04 safe and arm utilizing Krytox grease on the barrier-booster shaft O-rings were both certified. All inspection and instrumentation data indicate that the TEM-3 static test firing conducted 23 May 1989 was successful. The test was conducted at ambient conditions with the exception of the field joints (set point of 121 F, with a minimum of 87 F at the sensors), igniter joint (set point at 122 F with a minimum of 87 F at sensors) and case-to-nozzle joint (set point at 114 F with a minimum of 87 F at sensors). Ballistics performance values were within specification requirements. Nozzle performance was nominal with typical erosion. The nozzle and the case joint temperatures were maintained at the heaters controlling set points while electrical power was supplied. The water and the CO2 quench systems prevented damage to the metal hardware. All other test equipment performed as planned, contributing to a successful motor firing. All indications are that the test was a success, and all expected hardware will be refurbished for the RSRM program.

Garecht, Diane↗

Effects of potassium titanate fiber on the wear of automotive brake linings

Asbestos reinforcing fiber in an automotive friction material was replaced by an experimental ingredient having better thermal stability, and the effects on wear and friction were studied. A friction materials test machine (SAE J661a) was used to determine friction and wear, under constant energy output conditions, as a function of temperature between 121 and 343 C (250 and 650 F). When potassium titanate fiber replaced one half of the asbestos in a standard commercial lining, with a 40 percent upward adjustment of phenolic resin content, wear above 204 C (400 F) was improved by 40% and friction by 30%. Tests on a full-scale inertial dynamometer supported the findings of the sample dynamometer tests. It was demonstrated that the potassium titanate fiber contributes directly to the improvement in wear and friction.

Halberstadt, M. L.↗

Medical Ceramic Oxygen Generator (M-COG) Technology Description

Medical Ceramic Oxygen Generator Technology Description is presented to ISO technical committee 121, subcommittee SC6. Operating principles of ceramic oxygen generation are described, M-COG prototype system designs are described, testing and test results are summarized, and M-COG technology applications for medical oxygen are reviewed and evaluated.

oxygen↗

In-Situ Detection of Process-Induced Porosity During Cure of Out-of-Autoclave Composites

Composite materials offer unique benefits in aerospace applications, including high strength-to-weight ratio, and are becoming increasingly used by industry manufacturers. Current manufacturing and processing methods can lead to defects in the composites, which are identified after fabrication using inspection methods. This study utilized a high-temperature ultrasonic inspection system to detect process-induced porosity in an out-of-autoclave (OOA) composite panel during cure. In order to perform ultrasonic scans in-situ during cure, the system needed to be able to operate at oven temperatures up to 200 °C. There are no commercially available ultrasonic scanning systems that can operate continuously at these temperatures, so an enclosure was fabricated to insulate the ultrasonic system in the curing oven. The enclosure housed a MISTRAS® motorized X-Y raster scanner and contact transducer (Olympus® X2002). The Olympus® X2002 contact transducer is a continuous high-temperature delay line transducer with a center frequency of 2.25 MHz. In order to prevent the inside of the enclosure from reaching high temperatures, a sparge pipe inside the cooling enclosure was connected to a liquid nitrogen (LN2) tank outside of the oven via insulated hoses. The cooling system was automatically controlled by a temperature controller that was programmed to open a solenoid valve along the hose at 31 ℃ and close at 28 ℃ inside the cooling enclosure. When the solenoid valve was open, LN2 would flow from the LN2 tank and vaporize prior to reaching cooling enclosure. A U-shaped sparge pipe had holes drilled along its length to uniformly introduce cold nitrogen gas into the cooling enclosure. This prevented the motors from ever reaching the maximum desired operating temperature of 38 ℃. In the bottom of the enclosure, the tool plate was placed with the composite facing the outside of the enclosure, exposing it to the temperatures of the oven. The tool plate was 63.5 mm thick borosilicate glass, which was chosen for its low ultrasonic attenuation and moderate thermal conductivity. A thin layer of ultrasonic couplant was placed on the tool plate. The transducer sent and received ultrasonic waves through the tool plate into the composite. A MISTRAS® Remote UT System performed all wave generation, analog to digital conversion, and data acquisition and processing. The transducer was connected directly to the Remote UT System via a high-temperature BNC cable (CD International, RG-316). Polyimide insulated copper wire was used to connect the scanner to a 2-axis motor drive, which was connected to the Remote UT System. The motor drive and Remote UT System were located outside the industrial oven. A diagram of the ultrasonic system is shown in Figure 1. Figure 1: Diagram of ultrasonic in-situ defect detection system. In this study, a porosity gradient was introduced into the carbon fiber reinforced polymer (CFRP) composite through a misfit of the part and caul plate. A 24-ply quasi-isotropic ([0/90, ±45]12S) composite panel was laid up using Newport® AS4C-M/NB321 out-of-autoclave (OOA) plain weave (PW) prepreg (42% resin content, 195 g/m2). The first 16 plies were 203 mm × 203 mm. Ply drops were incorporated into the panel by decreasing the length of plies 17-24. The sizes of each ply are included in Table 1. All plies were centered along their length (x-axis) creating a trapezoidal type cross-section. Table 1: Ply sizes Plies Length (mm) Width (mm) 1-16 203 203 17-18 102 203 19-20 85 203 21-22 68 203 23-24 51 203 A 15-5 stainless steel caul plate (Size: 203 × 203 × 1.2 mm) was placed on the laminate. The composite and caul plate were vacuum bagged to the tool plate. Per the product datasheet, Newport 321 can be cured between 121 °C and 149 °C, depending on service temperature, with a hold for 90-120 minutes. Based on prior thermal testing of the cooling enclosure, the desired composite temperature cycle could be attained when the air temperature of the oven was ramped to 160 °C at a rate of 1.7 °C/min with a 3 hour hold. The extended hold was not necessary to cure the composite, but did allow for additional scans at the cure temperature during preliminary testing. The composite panel was under vacuum pressure for the entire cure cycle. Under vacuum, the caul plate deformed causing high and low pressure regions. The low-pressure regions formed high porosity in the composite part. The ultrasonic data collected showed that the inspection system was able to monitor the evolution of porosity within the composite throughout the cure cycle. Fifty scans of a 203 mm × 51 mm (8 in. × 2 in.) area of the composite were completed throughout the cure cycle. The scan speed was set to 43 mm/s in the x-direction and 36 mm/s in the y-direction, with a 1.0 mm/pixel resolution in both directions. Each scan took approximately five minutes to complete. Figure 2 shows C-scan amplitude data (top view) from one scan during the cure cycle. The color map indicates the maximum amplitude (%) measured with a time gate that contains reflections from the back surface (furthest from the transducer in contact with the caul plate) of the composite. Because porosity in the composite increases the ultrasonic attenuation in the composite part, a higher amplitude (red) indicates low porosity and a lower amplitude (blue) indicates high porosity. The regions where the caul plate was applying increased pressure (center and ends of the panel) resulted in reduced porosity, whereas the ply drop regions had reduced pressure and thus had higher porosity. Figure 2: Amplitude C-scan (top view) of OOA composite from one scan during the 160 °C temperature hold. Higher amplitude (red) indicates low porosity. Lower amplitude (blue) indicates high porosity. A B-scan is a two-dimensional image plotting the ultrasonic signals from a single y-position at every x-location of the composite panel. The travel time (μs) of the ultrasonic wave (representing the through-thickness location) is plotted along the y-axis, and the ultrasonic wave signal is represented as a contour map. Based on the B-scan data, the location of the defects with respect to the composite thickness was able to be determined. The ply drop regions had high porosity near the front (tool plate) surface of the composite (Figure 3). Figure 3: B-scan (cross-section view) of OOA composite from one scan during the 160 °C temperature hold. Using the data obtained from amplitude C-scans and B-scans throughout the cure cycle, the high and low porosity regions within the composite laminate were detected and localized with high spatial resolution. This paper will discuss the evolution of porosity content in the OOA composite during cure. OOA tests aided the transition of this system to an autoclave, which is the primary method of curing aerospace-grade thermoset composites.

Tyler B. Hudson↗

Radiation and thermal effects on the time-dependent response of T300/934 graphite/epoxy

Experimental studies have suggested that radiation, in conjunction with elevated temperatures, may lead to an exacerbation of the time-dependent response of such materials as T300/934 graphite/epoxy. Attention is given to the results of an investigation into such radiation/temperature effects with this composite system; creep tests were conducted on specimens of both irradiated and nonirradiated T300/934 composite and neat 934 resin specimens, at room temperature and 121 C. The radiation was of 1 MeV electrons, for a total dose of 10,000 Mrads; this simulates a 30-year exposure to radiation in geosynchronous orbit. Irradiation at elevated temperature led to a significant creep-response increase in the initial stages of loading.

Yancey, Robert N.↗