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NASA NTRS2006

Heliosheath Space Environment Interactions with Icy Bodies in the Outermost Solar System

The Voyager 1 and 2 spacecraft are exploring the space environment of the outermost solar system at the same time that earth-based astronomy continues to discover new icy bodies, one larger than Pluto, in the transitional region outward from the Classical Kuiper Belt to the Inner Oort Cloud. Some of the Scattered Disk Objects in this region periodically pass through the heliosheath, entered by Voyager 1 in Dec. 2004 and later expected to be reached by Voyager 2, and out even beyond the heliopause into the Very Local Interstellar Medium. The less energetic heliosheath ions, important for implantation and sputtering processes, are abundant near and beyond the termination shock inner boundary, but the source region of the more penetrating anomalous cosmic ray component has not yet been found. Advantageous for modeling of icy body interactions, the measured heliosheath flux spectra are relatively more stable within this new regime of isotropic compressional magnetic turbulence than in the upstream heliospheric environment. The deepest interactions and resultant radiation-induced chemistry arise from the inwardly diffusing component of the galactic cosmic ray ions with significant intensity modulation also arising in the heliosheath beyond Voyager 1. Surface gardening by high-velocity impacts of smaller bodies (e.g., fragments of previous KBO collisions) and dust is a further space weathering process setting the time scales for long term exposure of different regolith layers to the ion irradiation. Sputtering and ionization of impact ejecta grains may provide a substantial feedback of pickup ions for multiple cycles of heliosheath acceleration and icy body interaction. Thus the space weathering interactions are potentially of interest not only for effects on sensible surface composition of the icy bodies but also for evolution of the heliosheath plasma energetic ion, and neutral emission environment.

Cooper, John F.↗

NASA NTRS2008

M-BAND Analysis of Chromosome Aberration Induced by Fe-Ions in Human Epithelial Cells Cultured in 3-Dimensional Matrices

Energetic heavy ions pose a great health risk to astronauts in extended ISS and future lunar and Mars missions. High-LET heavy ions are particularly effective in causing various biological effects, including cell inactivation, genetic mutations, cataracts and cancer induction. Most of these biological endpoints are closely related to chromosomal damage, which can be utilized as a biomarker for radiation insults. Previously, we had studied low- and high-LET radiation-induced chromosome aberrations in human epithelial cells cultured in 2-dimension (2D) using the multicolor banding fluorescence in situ hybridization (mBAND) technique. However, it has been realized that the biological response to radiation insult in a 2D cellular environment in vitro can differ significantly from the response in 3-dimension (3D) or at the actual tissue level. In this study, we cultured human epithelial cells in 3D to provide a more suitable model for human tissue. Human mammary epithelia cells (CH184B5F5/M10) were grown in Matrigel to form 3D structures, and exposed to Fe-ions at NASA Space Radiation Laboratory (NSRL) at the Brookhaven National Laboratory or 137Cs-gamma radiation source at the University of Texas MD Anderson Cancer Center. After exposure, cells were allowed to repair for 16hr before dissociation and subcultued at low density in 2D. G2 and metaphase chromosomes in the first cell cycle were collected using a chemical-induced premature chromosome condensation (PCC) technique, and chromosome aberrations were analyzed using mBAND technique. With this technique, individually painted chromosomal bands on one chromosome allowed the identification of interchromosomal aberrations (translocation to unpainted chromosomes) and intrachromosomal aberrations (inversions and deletions within a single painted chromosome). Our data indicate a significant difference of the chromosome aberration yield between 2D and 3D cell cultures for gamma exposures, but not for Fe ion exposures. Therefore, the RBE for chromosome aberrations obtained in a 2D model may not represent accurately the RBE for tissues.

Hada, M.↗

DOE OSTI2025

Biomass-Derived Carbon and Their Composites for Supercapacitor Applications: Sources, Functions, and Mechanisms

Biomass-derived carbons are eco-friendly and sustainable materials, making them ideal for supercapacitors due to their high surface area, excellent conductivity, cost-effectiveness, and environmental benefits. This review provides valuable insights into biomass-derived carbon and modified carbon for supercapacitors, integrating both experimental results and theoretical calculations. This review begins by discussing the origins of biomass-derived carbon in supercapacitors, including plant-based, food waste-derived, animal-origin, and microorganism-generated sources. Then, this review presents strategies to improve the performance of biomass-derived carbon in supercapacitors, including heteroatom doping, surface functionalization, and hybrid composite construction. Furthermore, this review analyzes the functions of biomass-derived carbon in supercapacitors both in its pure form and as modified materials. The review also explores composites derived from biomass-based carbon, including carbon/MXenes, carbon/MOFs, carbon/graphene, carbon/conductive polymers, carbon/transition metal oxides, and carbon/hydroxides, providing a thorough investigation. Most importantly, this review offers an innovative summary and analysis of the role of biomass-derived carbon in supercapacitors through theoretical calculations, concentrating on four key aspects: energy band structure, density of states, electron cloud density, and adsorption energy. Finally, the review concludes the future research directions for biomass carbon-based supercapacitors, including the discovery of novel biomass materials, tailoring surface functional groups, fabricating high-performance composite materials, exploring ion transfer mechanisms, and enhancing practical applications. In summary, this review offers a thorough exploration of the sources, functions, and mechanisms of biomass-derived carbon in supercapacitors, providing valuable insights for future research.

biomass-derived carbon↗

DOE OSTI2024

Centrality dependence of Lévy-stable two-pion Bose-Einstein correlations in $\sqrt{𝑠{𝑁⁢𝑁}}$ = 200 GeV Au + Au collisions

The PHENIX experiment measured the centrality dependence of two-pion Bose-Einstein correlation functions in $\sqrt{𝑠{𝑁⁢𝑁}}$ = 200 GeV Au + Au collisions at the Relativistic Heavy Ion Collider at Brookhaven National Laboratory. The data are well represented by Lévy-stable source distributions. The extracted source parameters are the correlation-strength parameter 𝜆, the Lévy index of stability 𝛼, and the Lévy-scale parameter 𝑅 as a function of transverse mass 𝑚 𝑇 and centrality. The 𝜆⁡(𝑚 𝑇 ) parameter is constant at larger values of 𝑚 𝑇 , but decreases as 𝑚 𝑇 decreases. The Lévy-scale parameter 𝑅⁡(𝑚 𝑇 ) decreases with 𝑚 𝑇 and exhibits proportionality to the length scale of the nuclear overlap region. The Lévy exponent 𝛼⁡(𝑚 𝑇 ) is independent of 𝑚 𝑇 within uncertainties in each investigated centrality bin, but shows a clear centrality dependence. At all centralities, the Lévy exponent 𝛼 is significantly different from that of Gaussian (𝛼 = 2) or Cauchy (𝛼 = 1) source distributions. Comparisons to the predictions of Monte-Carlo simulations of resonance-decay chains show that, in all but the most peripheral centrality class (50%–60%), the obtained results are inconsistent with the measurements, unless a significant reduction of the in-medium mass of the 𝜂′ meson is included. Finally, in each centrality class, the best value of the in-medium 𝜂′ mass is compared to the mass of the 𝜂 meson, as well as to several theoretical predictions that consider restoration of U 𝐴⁢ (1) symmetry in hot hadronic matter.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NASA NTRS1987

Effects of thermospheric motions on the polar wind - A time-dependent numerical study

This paper presents the results of a numerical study investigating the effects of low-altitude short-duration plasma heating episodes (such as horizontal frictional heating) on transient heavy ion outflows from the polar ionosphere using a time-dependent model. In a previous set of calculations, where the effects of high-altitude transient heat sources were investigated, the low-altitude neutral atmosphere (z less than 800 km) acted as a very efficient heat sink, absorbing most of the energy conducted to this region and thus preventing large differences between the ion and neutral temperatures. One purpose of the present study was to investigate whether realistic, specified low-altitude frictional heating rates, based on published experimental data, can result in elevated ion temperatures and lift a part of the heavy ion population over the gravitational barrier before the extra energy is lost to the neutral atmosphere. In these model calculations the specified heating generated an upflowing O(+) disturbance (with a normalized peak flux of about 100 million/sq cm per sec) moving upward along the open magnetic field line with a velocity of about 2 km/s. The spatial extent of the disturbance was approximately equal to the disturbance velocity times the duration of the heat source. The model results provide a possible mechanism to explain recent European Incoherent Scatter observations of high-latitude O(+) upwellings.

Gombosi, T. I.↗

NASA NTRS2008

High- and low-LET Radiation-induced Chromosome Aberrations in Human Epithelial Cells Cultured in 3-dimensional Matrices

Energetic heavy ions pose a great health risk to astronauts who participate in extended ISS missions and will be an even greater concern for future manned lunar and Mars missions. High-LET heavy ions are particularly effective in causing various biological effects, including cell inactivation, genetic mutations, cataracts and cancer induction. Most of these biological endpoints are closely related to chromosomal damage, which can be utilized as a biomarker for radiation insults. Previously, we had studied low- and high-LET radiation-induced chromosome aberrations in human epithelial cells cultured in 2-dimension (2D) using the multicolor banding fluorescence in situ hybridization (mBAND) technique. However, it has been realized that the biological response to radiation insult in a 2D in vitro cellular environment can differ significantly from the response in 3-dimension (3D) or at the actual tissue level. In this study, we cultured human epithelial cells in 3D to provide a more suitable model for human tissue. Human mammary epithelial cells (CH184B5F5/M10) were grown in Matrigel to form 3D structures, and exposed to Fe-ions at NASA Space Radiation Laboratory (NSRL) at the Brookhaven National Laboratory or 137Cs-gamma radiation source at the University of Texas MD Anderson Cancer Center. After exposure, cells were allowed to repair for 16hr before dissociation and subcultured at low density in 2D. G2 and metaphase chromosomes in the first cell cycle were collected in the first cell cycle after irradiation using a chemical-induced premature chromosome condensation (PCC) technique, and chromosome aberrations were analyzed using mBAND technique. With this technique, individually painted chromosomal bands on one chromosome allowed the identification of interchromosomal aberrations (translocation to unpainted chromosomes) and intrachromosomal aberrations (inversions and deletions within a single painted chromosome). Our data indicate a significant difference in the chromosome aberration yield between 2D and 3D cell cultures after gamma exposures, but not after Fe ion exposures. Therefore, the Relative Biological Effect (RBE) for induction of chromosome aberrations obtained in a 2D model may not accurately represent RBE values obtained for tissue exposure.

Hada, M.↗

NASA NTRS2019

Highly Structured Slow Solar Wind Emerging From an Equatorial Coronal Hole

At solar minimum, the solar wind is observed at high solar latitudes as a predominantly fast (> 500 km/s), highly Alfvenic, rarefied stream of plasma originating deep within coronal holes, while near the ecliptic plane it is interspersed with a more variable slow (< 500 kms) wind. The precise origins of the slow wind streams are less certain, with theories and observations supporting sources from the tips of helmet streamers, interchange reconnection near coronal hole boundaries, and origins within coronal holes with highly diverging magnetic fields. The heating mechanism required to drive the solar wind is also an open question and candidate mechanisms include Alfven wave turbulence, heating by reconnection in nanoflares, ion cyclotron wave heating and acceleration by thermal gradients1. At 1 au, the wind is mixed and evolved and much of the diagnostic structure of these sources and processes has been lost. Here we present new measurements from Parker Solar Probe at 36 to 54 solar radii that show clear evidence of slow, Alfvenic solar wind emerging from a small equatorial coronal hole. The measured magnetic field exhibits patches of large, intermittent reversals associated with jets of plasma and enhanced Poynting flux and interspersed in a smoother and less turbulent flow with near-radial magnetic field. Furthermore, plasma wave measurements suggest electron and ion velocity-space micro-instabilities that have been identified with plasma heating and thermalization processes. Our measurements suggest an impulsive mechanism associated with solar wind energization and a heating role for micro-instabilities and provide strong evidence for low latitude coronal holes as a significant contribution to the source of the slow solar wind.

Solar physics↗

DOE OSTI2022

Molecular Characterization of Organophosphorus Compounds in Wildfire Smoke Using 21-T Fourier Transform-Ion Cyclotron Resonance Mass Spectrometry

Here, we present a detailed molecular characterization of organophosphorus compounds in ambient organic aerosol influenced by wildfire smoke. Biomass burning organic aerosol (BBOA) is an important source of phosphorus (P) to surface waters, where even a small imbalance in the P flux can lead to substantial effects on water quality, such as eutrophication, algal blooms, and oxygen depletion. We aimed to exploit the ultrahigh resolving power, mass accuracy, and sensitivity of Fourier transform-ion cyclotron resonance mass spectrometry (FT-ICR MS) to explore the molecular composition of an ambient BBOA sample collected downwind of Pacific Northwest wildfires. The 21-T FT-ICR MS yielded 10533 distinct formulae, which included molecular species comprising C, H, O, and P with or without N, i.e., organophosphorus compounds that have long been quantified in wildfire smoke but have not yet been characterized at the molecular level. The lack of detailed molecular characterization of organophosphorus compounds in BBOA is primarily due to their inherently low concentrations in aerosols and poor ionization efficiency in complex mixtures. We demonstrate that the exceptional sensitivity of the 21-T FT-ICR MS allows qualitative analysis of a previously uncharacterized fraction of BBOA without its selective concentration from the organic matrix, exemplifying the need for ultrahigh-resolution tools for a more detailed and accurate molecular depiction of such complex mixtures.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1987

Voyager 2 plasma ion observations in the magnetosphere of Uranus

Positive ion measurements in the magnetosphere of Uranus have been made by the Voyager 2 plasma science experiment. The paper presents an overview of the entire data set and a detailed analysis of the observations from the inner magnetosphere which complements and extends results reported elsewhere. Densities and temperatures are obtained from an analysis which incorporates details of the instrumental response. These results are then used to calculate flux tube particle and energy content to support the hypothesis that the plasma transport is controlled by a solar wind-driven magnetospheric convection system. Variations in the flux tube content suggest both a local source of plasma, produced from the neutral hydrogen corona of Uranus, and a nonlocal source, convected inwared and heated by adiabatic compression. In each case a proton composition is inferred. Sharp boundaries in the high-energy (approximately 1 keV) plasma population are interpreted in terms of the spatial extent of the magnetospheric convection, with significant shielding of the convection electric field. The convection theory is also used in a simulation of the low-energy (approximately 10 eV) ion component using the neutral hydrogen source, resulting in distribution functions which qualitatively agree with the observations.

Selesnick, Richard S.↗

DOE OSTI2023

Quantitative proton radiography and shadowgraphy for arbitrary intensities

Charged-particle radiography and shadowgraphy data can be directly inverted to obtain a line-integrated transverse Lorentz force or a line-integrated transverse refractive index gradient if intensity modulations due to scattering and absorption are negligible, and angular deflections are small. We develop a new direct-inversion algorithm based on plasma physics and compare it to a new Monge–Ampère code and an existing power diagram code. The measured or source intensity is represented by electrons subject to drag, and the other intensity by fixed ions. The decrease in kinetic plus electrostatic energy determines convergence. The displacement of the electrons from their initial to their equilibrium positions determines the line-integrated force or refractive index gradient. We have implemented two approaches: PIC (particle in cell) and Lagrangian fluid, in 1-D and 2-D. The PIC code works for arbitrary intensities, can work efficiently in parallel, and can make use of existing codes. The Lagrangian code requires less memory and is faster than the PIC code without massively parallel processing, but fails in 2-D for large intensity modulations. The Monge–Ampère code is by far the fastest in 2-D, without massively parallel processing, but fails for intensities with large voids, high contrast ratios and large deflections across the boundaries, and could not obtain the degree of convergence possible with the PIC code. As a result, the power diagram code was by far the slowest and most memory intensive, and failed for large peaks in the measured intensity.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2021

Towards green synthesis of Mn 4+ -doped fluoride phosphors: a review

Mn 4+ -doped fluoride phosphors are attractive for application in white solid-state lighting devices because their distinct red emission can improve the color rendering index, while the earth-abundance of Mn 4+ ions can reduce the production cost. However, highly hazardous HF is used as the fluoride source in the synthesis processes, which requires extreme caution. In this review, we introduce various methods for synthesizing Mn 4+ -doped fluoride phosphors, categorized according to the presence or absence of HF in the synthesis. The underlying optical properties of the phosphors fabricated using the various methods are discussed. In addition, in the discussion of each method, we emphasize on the key factors and strategies for developing phosphors. Finally, this review highlights perspectives on and future directions for the safe synthesis of Mn 4+ -doped fluoride phosphors to achieve solid-state lighting devices with superior optical properties.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Space charge effects in the SπRIT time projection chamber

Time projection chambers (TPCs) are widely used in nuclear and particle physics. They are particularly useful when measuring reaction products from heavy ion collisions. Most nuclear experiments at low energy are performed in a fixed target configuration, in which the unreacted beam will pass through the detection volume. As the beam intensity increases, the buildup of positive ions created from the ionization of the detector gas by the beam creates the main source of space charge, distorting the nominal electric field of the TPC. This has a profound effect on the accuracy of the measured momenta of the emitted particles. In this paper we will discuss the magnitude of the effects and construct an observable appropriate for fixed target experiments to study the effects. Finally, we will present an algorithm for correcting the space charge and discuss some of the implications it has on the momentum determination.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

Investigation of a digitizer for the plastic scintillation detectors of time-of-flight mass measurements

A CAEN DT5742 digitizer has been investigated to process the fast signals from the photomultiplier tubes of the time-of-flight detectors for fast ion beams. A test setup consisting of two plastic scintillation detectors and a pulsed laser source provided signals which were recorded by the digitizer and systematically analyzed with different algorithms to derive the amplitude, rise time and arrival time of the detection signal. To obtain the best amplitude and time resolutions, various optimization techniques including peak fitting and signal smoothing, interpolation improvement, and time-walk correction by amplitude and rise time have been performed and compared in detail. Here we compared the time resolutions obtained by three digital algorithms of leading-edge, zero-crossing constant-fraction (ZC-CFD) and direct constant-fraction discriminations. Finally, we found that the best time-of-flight resolution between two PMTs can be achieved as 12 ps by the method using sample minimum for peak location and using the time-walk-resistant ZC-CFD with 4-point interpolation for timing.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Bulk flow and correlation measurements at LHCb

Particle correlations are a powerful tool to study the properties of the bulk nuclear matter produced in relativistic heavy ion collisions. The momentum correlations between identical particles originating from the same particle-emitting source, referred to as the Bose-Einstein correlations, measure scales that are related to the geometrical size of the source. The two-particle azimuthal angular correlations measure the spatial anisotropy of produced particles, providing information on collective phenomena arising in the dense nuclear medium. This contribution will discuss new LHCb measurements of Bose- Einstein correlations and, for the first time, the collective flow coefficients in the far forward rapidity region.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2020

Improved core-edge compatibility using impurity seeding in the small angle slot (SAS) divertor at DIII-D

Impurity seeding studies in the slot divertor (SAS) at DIII-D have revealed a strong relationship between the detachment onset and pedestal characteristics with both target geometry and impurity species. N 2 seeding in the slot has led to the first simultaneous observation of detachment on the entire suite of boundary diagnostics viewing the SAS without degradation of core confinement. SOLPS-ITER simulations with D+C+N, full cross-field drifts and n-n collisions activated are performed for the first time in DIII-D to interpret the behavior. This illustrates a strong effect of divertor configuration and plasma drifts on the recycling source distribution with significant consequences on plasma flows. Flow reversal is found for both main ions and impurities affecting strongly the impurity transport and providing an explanation for the observed dependence on strike point location of the detachment onset and impurity leakage found in the experiments. Matched discharges with either nitrogen or neon injection show that while nitrogen does not significantly affect the pedestal, neon leads to increased pedestal pressure gradient and improved pedestal stability. Little nitrogen penetrates in the core, but a great amount of neon is found in the pedestal consistent with the different ionization potentials of the two impurities. This research demonstrates that neutral and impurity distributions in the divertor can be controlled through variations in strike point locations in a fixed baffle structure. Divertor geometry combined with impurity seeding enables mitigated divertor heat flux balancing core contamination and thus leading to enhanced divertor dissipation and improved core-edge compatibility which are essential for ITER and for future fusion reactors.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Laser and optical transport line for laser-based ion beam diagnostics and control in the SNS linear accelerator

We report our recent upgrade of the laser and optical transport line for the laser-based ion beam diagnostics (laser wire) system at the linear accelerator (linac) of the Spallation Neutron Source (SNS). A new light source based on diodepumped solid-state laser amplifiers has been developed to provide near diffraction-limited laser beam with a variety of pulse structures. The free-space optical transport line has been modified to include image relay optics with remote control, which greatly improved the laser beam quality and position stability at individual measurement stations. The upgraded system enables novel beam diagnostics/control capabilities including longitudinal profile measurement and high-energy proton beam extraction from the SNS linac.

Liu, Yun↗

DOE OSTI2022

Challenges to Reliable Production Nitrogen Doping of Nb for SRF Accelerating Cavities

Over the last several years, alloying of the surface layer of niobium SRF cavities has been demonstrated to beneficially lower the superconducting RF surface resistance. Nitrogen, titanium, and oxygen have all been demonstrated as effective alloying agents, occupying interstitial sites in the niobium lattice within the RF penetration depth and even deeper, when allowed to thermally diffuse into the surface at appropriate temperatures. The use of nitrogen for this function has been often termed ’nitrogen doping’ and is being applied in the LCLS-II and LCLS-II HE projects. We report characterization studies of the distribution of nitrogen into the exposed niobium surface and how such distribution is affected by the quality of the vacuum furnace environment in which the doping takes place, and the complexity of nitride crystal growth on different grain orientations of surface niobium. Using state-of-the-art quantification methods by dynamic secondary ion mass spectrometry (SIMS) depth profiling in niobium, we identify several phenomena involving furnace-sourced contamination. We also highlight a potential issue with N₂ flow constraints from the flange ’caps’ used during heat treatments.

Reece, Charles↗

DOE OSTI2020

Electrodes with Electrodeposited Water-excluding Polymer Coating Enable High-Voltage Aqueous Supercapacitors

Aqueous supercapacitors are powerful energy sources, but they are limited by energy density that is much lower than lithium-ion batteries. Since raising the voltage beyond the thermodynamic potential for water splitting (1.23 V) can boost the energy density, there has been much effort on water-stabilizing salvation additives such as Li 2 SO 4 that can provide an aqueous electrolyte capable of withstanding ~1.8 V. Guided by the first-principles calculations that reveal water can promote hydrogen and oxygen evolution reactions, here, we pursue a new strategy of covering the electrode with a dense electroplated polymerized polyacrylic acid, which is an electron insulator but a proton conductor and proton reservoir. The combined effect of salvation and coating expands the electrochemical window throughout pH 3 to pH 10 to 2.4 V for both fast and slow proton-mediated redox reactions. This allows activated carbon to quadruple the energy density, a kilogram of nitrogen-doped graphene to provide 127 Watt-hour, and both to have improved endurance because of suppression of water-mediated corrosion. Therefore, aqueous supercapacitors can now achieve energy densities quite comparable to that of a lithium-ion battery, but at 100 times the charging/discharging speed and cycle durability.

Dong, Wujie↗