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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,729 records · Page 96
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Charge-carrier transport mechanisms in composites containing carbon-nanotube inclusions

From the microwave-radiation transmittance and reflectance spectra, the temperature dependence of the complex permittivity of carbon nanotubes, subjected to high-temperature annealing, and composite materials produced on their basis is determined. The electron transport mechanisms in composites with inclusions of unannealed carbon nanotubes and nanotubes subjected to high-temperature annealing are determined. The influence of the annealing temperature on the parameters that are characteristic of these mechanisms and control the temperature dependence of the conductivity of multiwall carbon nanotubes is established.

36 MATERIALS SCIENCE↗
NASA NTRS1977

Monopropellant thruster exhaust plume contamination measurements

The potential spacecraft contaminants in the exhaust plume of a 0.89N monopropellant hydrazine thruster were measured in an ultrahigh quartz crystal microbalances located at angles of approximately 0 deg, + 15 deg and + or - 30 deg with respect to the nozzle centerline. The crystal temperatures were controlled such that the mass adhering to the crystal surface at temperatures of from 106 K to 256 K could be measured. Thruster duty cycles of 25 ms on/5 seconds off, 100 ms on/10 seconds off, and 200 ms on/20 seconds off were investigated. The change in contaminant production with thruster life was assessed by subjecting the thruster to a 100,000 pulse aging sequence and comparing the before and after contaminant deposition rates. The results of these tests are summarized, conclusions drawn, and recommendations given.

Baerwald, R. K.↗
NASA NTRS1990

The effect of coatings and liners on heat transfer in a dry shaft-bush tribosystem

The temperatures due to frictional heating within a solid lubricated or coated journal bearing were analyzed by using a finite element method. A solid model of the shaft-bush tribocontact was generated with an eight-node, three-dimensional, first-order isoparametric heat-transfer element and the Patran solid modeler software. The Patmar (Patran-Marc) translator was used to help develop the Marc-based finite element program for the system; this software was used on the Cray X-MP supercomputer to perform a finite element analysis of the contact. The analysis was performed for various liner materials, for thin, hard, wear-resistant coated bearings, and for different geometries and thermal cooling boundary conditions. The analyses indicated that thermal conductivity of the liner or coating material is the most vital thermal parameter that controls the interface temperature. In addition to design variations, the proximity of the cooling source to the heat-flux-generating interface is critically important to the temperature control in the system.

Ghosh, Mihir K.↗
DOE OSTI2016

Multi-probe microstructure tracking during heat treatment without an in-situ setup: Case studies on martensitic steel, dual phase steel and β-Ti alloy

In-situ scanning electron microscopy observations of the microstructure evolution during heat treatments are increasingly demanded due to the growing number of alloys with complex microstructures. Post-mortem characterization of the as-processed microstructures rarely provides sufficient insight on the exact route of the microstructure formation. On the other hand, in-situ SEM approaches are often limited due to the arising challenges upon using an in-situ heating setup, e.g. in (i) employing different detectors, (ii) preventing specimen surface degradation, or (iii) controlling and measuring the temperature precisely. Here, we explore and expand the capabilities of the “mid-way” solution by step-wise microstructure tracking, ex-situ, at selected steps of heat treatment. This approach circumvents the limitations above, as it involves an atmosphere and temperature well-controlled dilatometer, and high resolution microstructure characterization (using electron channeling contrast imaging, electron backscatter diffraction, atom probe tomography, etc.). We demonstrate the capabilities of this approach by focusing on three cases: (i) nano-scale carbide precipitation during low-temperature tempering of martensitic steels, (ii) formation of transformation-induced geometrically necessary dislocations in a dual-phase steel during intercritical annealing, and (iii) the partial recrystallization of a metastable β-Ti alloy. - Highlights: • A multi-probe method to track microstructures during heat treatment is developed. • It enables the analysis of various complex phenomena, even those at atomistic scale. • It circumvents some of the free surface effects of classical in-situ experiments.

36 MATERIALS SCIENCE↗
NASA NTRS2014

Iodine Hall Thruster Propellant Feed System for a CubeSat

There has been significant work recently in the development of iodine-fed Hall thrusters for in-space propulsion applications.1 The use of iodine as a propellant provides many advantages over present xenon-gas-fed Hall thruster systems. Iodine is a solid at ambient temperature (no pressurization required) and has no special handling requirements, making it safe for secondary flight opportunities. It has exceptionally high ρI sp (density times specific impulse), making it an enabling technology for small satellite near-term applications and providing system level advantages over mid-term high power electric propulsion options. Iodine provides thrust and efficiency that are comparable to xenonfed Hall thrusters while operating in the same discharge current and voltage regime, making it possible to leverage the development of flight-qualified xenon Hall thruster power processing units for the iodine application. Work at MSFC is presently aimed at designing, integrating, and demonstrating a flight-like iodine feed system suitable for the Hall thruster application. This effort represents a significant advancement in state-of-the-art. Though Iodine thrusters have demonstrated high performance with mission enabling potential, a flight-like feed system has never been demonstrated and iodine compatible components do not yet exist. Presented in this paper is the end-to-end integrated feed system demonstration. The system includes a propellant tank with active feedback-control heating, fill and drain interfaces, latching and proportional flow control valves (PFCV), flow resistors, and flight-like CubeSat power and control electronics. Hardware is integrated into a CubeSat-sized structure, calibrated and tested under vacuum conditions, and operated under under hot-fire conditions using a Busek BHT-200 thruster designed for iodine. Performance of the system is evaluated thorugh accurate measurement of thrust and a calibrated of mass flow rate measurement, which is a function of reservoir temperature/pressure, the flow resistors, and the setting of the PFCV. The calibration is performed using independent flow control monitoring techniques, providing an in situ measure of the flowrate as a function of controllable parameters. The reservoir temperature controls the iodine sublimation rate, providing propellant to ths thruster by pressurizing the propellant feed system to approx.1-2 psi. Control of the temperature and the PFCV are used to maintain reservoir pressure and keep the thruster discharge current constant.

Polzin, Kurt A.↗
NASA NTRS1991

Water vapor recovery from plant growth chambers

NASA is investigating the use of plant growth chambers (PGCs) for space missions and for bases on the moon and Mars. Key to successful development of PGCs is a system to recover and reuse the water vapor that is transpired from the leaves of the plants. A design is presented for a simple, reliable, membrane-based system that allows the recovery, purification, and reuse of the transpired water vapor through control of temperature and humidity levels in PGCs. The system is based on two membrane technologies: (1) dehumidification membrane modules to remove water vapor from the air, and (2) membrane contactors to return water vapor to the PGC (and, in doing so, to control the humidity and temperature within the PGC). The membrane-based system promises to provide an ideal, stable growth environment for a variety of plants, through a design that minimizes energy usage, volume, and mass, while maximizing simplicity and reliability.

Ray, R. J.↗
DOE OSTI2015

A new apparatus design for high temperature (up to 950 °C) quasi-elastic neutron scattering in a controlled gaseous environment

A design for a sample cell system suitable for high temperature Quasi-Elastic Neutron Scattering (QENS) experiments is presented. The apparatus was developed at the Spallation Neutron Source in Oak Ridge National Lab where it is currently in use. The design provides a special sample cell environment under controlled humid or dry gas flow over a wide range of temperature up to 950 °C. Using such a cell, chemical, dynamical, and physical changes can be studied in situ under various operating conditions. While the cell combined with portable automated gas environment system is especially useful for in situ studies of microscopic dynamics under operational conditions that are similar to those of solid oxide fuel cells, it can additionally be used to study a wide variety of materials, such as high temperature proton conductors. The cell can also be used in many different neutron experiments when a suitable sample holder material is selected. The sample cell system has recently been used to reveal fast dynamic processes in quasi-elastic neutron scattering experiments, which standard probes (such as electrochemical impedance spectroscopy) could not detect. In this work, we outline the design of the sample cell system and present results demonstrating its abilities in high temperature QENS experiments.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

Particle Mass Flow Control and Measurement for High-Temperature Particle Receivers

This work is developing particle flow control and measurement methods for next-generation concentrating solar power systems employing particle-based technologies. Particle receivers are being pursued to provide substantial performance improvements through higher temperatures (>700 °C) for more efficient and cost-effective CSP systems with direct storage for electricity generation, process heating, thermochemistry, and solar fuels production. This specific work will develop technologies that enable more efficient particle receivers and scalable methods to accommodate variable irradiances during commercial on-sun operation. The development of next-generation particle-receiver systems and methods with potentially high consequences for improved performance and cost savings for CSP applications is an appropriate role for the government.

14 SOLAR ENERGY↗
NASA NTRS2001

Apparatus and Method for Measuring Air Temperature Ahead of an Aircraft for Controlling a Variable Inlet/Engine Assembly

The apparatus and method employ remote sensing to measure the air temperature a sufficient distance ahead of the aircraft to allow time for a variable inlet/engine assembly to be reconfigured in response to the measured temperature, to avoid inlet unstart and/or engine compressor stall. In one embodiment, the apparatus of the invention has a remote sensor for measuring at least one air temperature ahead of the vehicle and an inlet control system for varying the inlet. The remote sensor determines a change in temperature value using at least one temperature measurement and prior temperature measurements corresponding to the location of the aircraft. The control system uses the change in air temperature value to vary the inlet configuration to maintain the position of the shock wave during the arrival of the measured air in the inlet. In one embodiment, the method of the invention includes measuring at least one air temperature ahead of the vehicle, determining an air temperature at the vehicle from prior air temperature measurements, determining a change in temperature value using the air temperature at the vehicle and the at least one air temperature measurement ahead of the vehicle, and using the change in temperature value to-reposition the airflow inlet, to cause the shock wave to maintain substantially the same position within the inlet as the airflow temperature changes within the inlet.

Gary, Bruce L.↗
DOE OSTI2024

Review of Solid State Consolidation Processing Techniques of ODS Steels (Hot Extrusion, Hot Isostatic Pressing, Spark Plasma Sintering, and Stir Friction Consolidation): Resulting Microstructures and Mechanical Properties

This paper reviews the solid-state consolidation processing techniques for Oxide Dispersion Strengthened steels and compares them in terms of the resulting microstructure and reported mechanical properties. Synthesis techniques include hot extrusion, hot isostatic pressing, spark plasma sintering and friction consolidation. The effects of process parameters on the resulting microstructures and performance are discussed for each technique. Average oxide size, average grain size, and porosity are compared across techniques, as well as mechanical strength and ductility. Across consolidation techniques where temperature can be controlled, a low sintering temperature with a high sintering pressure is favorable for keeping oxide sizes, grain sizes, and porosity low. The use of yttrium and titanium for oxide formation has been evidenced to reduce oxide sizes, and tungsten additions have been shown to improve strength. Current literature suggests that the more mature hot extrusion technique produces stronger steel with consistently fine oxides, while other alternative solid-state consolidation, while promising, offer margin for improvement.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Quantitative Cu Counting Methodologies for Cu/SSZ-13 Selective Catalytic Reduction Catalysts by Electron Paramagnetic Resonance Spectroscopy

Here, two Cu/SSZ-13 selective catalytic reduction (SCR) catalysts with distinct Si/Al ratios and isolated Z2Cu and ZCuOH distributions are prepared for in situ electron paramagnetic resonance (EPR) spectroscopic studies. These in situ studies include dehydration, titration of dehydrated samples with NO+O 2 and NH 3 , titration of NH 3 saturated samples with NO+O 2 , and finally steady-state standard NH 3 -SCR reaction. During dehydration, EPR active hydrated ZCuOH loses H 2 O ligands and becomes EPR silent due to a pseudo Jahn-Teller effect; a portion of ZCuOH also undergoes autoreduction to ZCu(I) species, a process that also induces EPR invisibility. During NO+O 2 treatment of dehydrated samples, ZCu(I) species are oxidized to Cu(II)-NO 3 - species, regaining EPR visibility. During NH3 titration, EPR silent dehydrated ZCuOH can also regain EPR visibility by coordinating with NH 3 ligands. During NO+O 2 titration of NH 3 -saturated samples, EPR active Cu contents first decrease due to Cu(II) reduction to Cu(I), and then increase due to Cu(II)-NO 3 - species formation. However, the Cu(II)-NO 3 - formation chemistry is substantially slower for the Si/Al = 36 catalyst. In steady-state SCR studies, the EPR active content decreases with increasing temperature in the kinetically controlled low-temperature regime and becomes largely invariant in mass-transfer limited regime. Importantly, Cu sites in the SCR more active Si/Al = 6 catalyst display substantially higher EPR visibility than the SCR less active Si/Al = 36 catalyst at any reaction temperatures tested. The higher Cu loading for the former catalyst is believed to be key for this difference.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

One-Step High-Throughput Blade Coating of Perovskite Solar Cells

A metal halide perovskite (MHP) solution was developed that is compatible with high speed (1 m min -1 ) one-step blade coating. MHP solar cells from the developed solution can produce power conversion efficiency over 18% in ambient environment without any addition of antisolvent, gas drying, vacuum treatment or high-temperature annealing. Careful control of the annealing temperature allows fabricating of a more stable MHP due to the increased crystallinity of the MHP film. This development on one-step, antisolvent (or similar processing) treatment free, blade coating technique paves the way for the rollto- roll production of high-efficiency MHP solar cells.

14 SOLAR ENERGY↗
DOE OSTI2022

Diffusion-assisted molecular beam epitaxy of CuCrO 2 thin films

Using molecular beam epitaxy (MBE) to grow multielemental oxides (MEOs) is generally challenging, partly due to difficulty in stoichiometry control. Occasionally, if one of the elements is volatile at the growth temperature, stoichiometry control can be greatly simplified using adsorption-controlled growth mode. Otherwise, stoichiometry control remains one of the main hurdles to achieving high-quality MEO film growths. Here, in this paper, we report another kind of self-limited growth mode, dubbed diffusion-assisted epitaxy, in which excess species diffuses into the substrate and leads to the desired stoichiometry, in a manner similar to the conventional adsorption-controlled epitaxy. Specifically, we demonstrate that using diffusion-assisted epitaxy, high-quality epitaxial CuCrO 2 films can be grown over a wide growth window without precise flux control using MBE.

36 MATERIALS SCIENCE↗
NASA NTRS1978

Thermal response to ozone fluctuations of the stratosphere

Correlations between stratospheric meteorological parameters and ozone amount are examined in terms of radiation absorption by ozone. Fluctuations of ozone concentration at subtropic latitudes in summer are analyzed on the assumption that local temperature is governed entirely by radiative equilibrium. The analysis suggests that the fluctuations of mean monthly temperature and ozone are not only correlated, but also follow the order-of-magnitude values expected if ozone heating dominates the temperatures. Most direct control of ozone on temperature exists in the lowest parts of the stratosphere.

Stanulonis, S. F.↗
NASA NTRS1984

Thermal considerations in the use of solid state power amplifiers on the GOES spacecraft

The use of solid state power amplifiers (SSPA) in satellites has been quite prevalent in several frequency bands. This trend is evidenced by the use of SSPAs at Hughes in the UHF band (Leasat/Syncom IV), S band (GOES), C band (Telstar), and SHF band. The junction temperature of the transistor is the driving requirement which determines the lifetime of the transistor, SSPA, and the payload. This temperature is determined by the transistor characteristics, use of the device, and mounting temperature of the SSPA. The temperature of the spacecraft in the area of the SSPA can be controlled by active or passive means. The various factors and interrelationships used to calculate and control the temperatures of SSPAs are described. The thermal design and calculation of junction temperatures are exemplified with the Geostationary Operational Environmental Satellite spacecraft.

Mallette, L.↗