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All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

The Single Event Error (SEE) test and analysis of the CMS Endcap Timing Layer readout chip

The ETROC2, the first full size and full functionality prototype chip for the CMS Endcap Timing Layer readout, is strategically designed to meet the SEE immunity requirements of detector operation with the low power constraint. The triplicated periphery and pixel I2C configuration registers are designed with self-correction feature. The pixel readout control is centralized in the global readout and fully triplicated. The pixel readout is not triplicated, instead protected with power-efficient one-bit correction Hamming code. The TMR protection of the on-pixel threshold calibration can be turned off allowing the detection of the beam spot during the beam test by checking the bit-flips of the internal memory cells. In the initial proton beam test in January 2024, the chip readout process did not hang throughout the tests. The Hamming code correction strategy works because the error corrected TDC data were observed in the data frames. The error-injection simulation is performed to analy ze the small number of bit-flips in the configuration registers. We also performed SEE testing with a heavy ion beam in April and the data analysis is ongoing. The detailed design on the SEE immunity and the testing as well as simulation results will be presented, including follow-up SEE testing results in May and June 2024.

Gong, Datao↗
NASA NTRS2023

Pulse Response of the Short-Wave Infrared Detection System of the Ocean Color Instrument for the NASA PACE Mission

The Ocean Color Instrument (OCI) on NASA’s Plankton, Aerosol, Cloud, ocean Ecosystem (PACE) mission is a hyperspectral Earth imager with a spatial resolution of 1 km x 1 km and a spectral resolution of 5 nm in 2.5 nm steps over 342-887 nm. In addition, OCI provides 7 discrete bands in the 940-2260 nm Short-Wave InfraRed (SWIR) range. The front-end optical imager is a rotating mirror-based system that images the ground scene onto a slit with an instantaneous field of view of 16 km x 1 km. For the SWIR bands, the slit-image is re-imaged onto a 16x1 micro-lens array that effectively acts as the focal plane since each lens element is fiber coupled to wavelength filtered InGaAs and HgCdTe Photo Diodes (PDs). The pulse response of the detection system is critical to OCI SWIR performance. We find that PDs introduce an inherent slow tail in the pulse response due to slow diffusion moving carriers in their n and p regions. We show that this introduces response errors ranging from 1 down to 0.01 % for up to tens of science pixels after the pulse depending on the PD design and materials. It is shown that the response is distinctly different for the InGaAs and HgCdTe PDs. We explain how the front-end design can further increase this error. Finally, we detail the cause of the slow pulse response tail, how to model it, its impact on OCI performance and how it is characterized and corrected to meet OCI requirements.

ocean color↗
NASA NTRS1986

Airborne spectroradiometry: The application of AIS data to detecting subtle mineral absorption features

Analysis of Airborne Imaging Spectrometer (AIS) data acquired in Australia has revealed a number of operational problems. Horizontal striping in AIS imagery and spectral distortions due to order overlap were investigated. Horizontal striping, caused by grating position errors can be removed with little or no effect on spectral details. Order overlap remains a problem that seriously compromises identification of subtle mineral absorption features within AIS spectra. A spectrometric model of the AIS was developed to assist in identifying spurious spectral features, and will be used in efforts to restore the spectral integrity of the data.

Cocks, T. D.↗
NASA NTRSDate not supplied

Considerations on Electrolytic Conductivity Measurement for Monitoring of Ionic Silver Biocide Dosing

NASA interest in ionic silver (Ag+) as a biocide for spacecraft potable water systems motivates the development of Ag+ concentration sensors to ensure nominal dosing. The electrolytic conductivity change of highly-purified potable water is linearly related to the concentration of chemically-dosed Ag+ and could serve as a useful proxy measurement, while the conductivity change during electrolytic dosing may be less so, depending on the influent water chemistry and electrolytic efficiency. Understanding and mitigating the potentially deleterious effects of Ag+ interaction with conductivity measurement systems requires investigation. Issues associated with traditional conductivity cells, which rely on wetted(typically metal or graphite) electrodes, and capacitively-coupled contactless conductivity detection (C4D) for this application are considered. Traditional conductivity cells may potentially be subject to significant excitation-induced or auto-galvanic reduction of Ag+. These may result in Ag+ depletion or electrode fouling and associated measurement error. Proper selection of electrode material, excitation parameters, and cell geometry may limit such effects. C4D uses electrodes placed outside an inert, insulating material, with dielectric polarization enabling the production of an electric field and resultant current across the analyte solution. This approach could potentially mitigate problems with Ag+ depletion and fouling by eliminating the possibility of auto-galvanic deposition and reducing the Faradaic current density. However, it is necessary to confirm C4D performance at very low conductivity levels and to determine if long-term operation produces conductive deposits, which could result in measurement error. A commercial C4D system with 1/16” (1.59 mm)outer diameter flow tubing and claimed performance in the conductivity range appropriate for this application was identified, and its sensitivity in the upper parts of this range was confirmed in a preliminary experiment. A concept for a C4D detector that could allow for full rate flow-through using planar electrodes and thin-film dielectric layers is discussed.

silver↗
NASA NTRS1997

IAUC 6530: GRO J1744-28; C/1995 01

We have recorded a series of outbursts starting on 1996 Dec. 2 that are consistent with the position of GRO J1744-28, the bursting pulsar. The bursts are detected between 20 and 100 keV, and on Dec. 2 they came in variable rates ranging from every 300 to every 500 s, with a preliminary total number estimated between 80 and 1 00 events. After Dec. 3, the burst rate dropped to 15-20 bursts/day, where it has remained. The current average error radius of the burst locations is about 4 deg. The burst fluence is currently about 2 x 10E-7 erg cmE-2. This indicates that the source is in outburst again. Although the source location is currently very close to the sun, we encourage observations in other wavelengths whenever possible. Persistent, hard x-ray emission from GRO J1744-28 (IAUC 6272, 6284, 6285) is currently being detected through both pulsation and earth occultation. Pulsations with a period near 0.467 s became detectable on Dec. 17, rising to a 20- to 40-keV-rms-pulsed flux of 1.3(1) x 10E-9 erg cmE-1 sE-1 (170 mCrab) by 1997 Jan. 3. On Jan. 1.0, the intrinsic pulse frequency was 2.1408983(4) Hz, and the spin-up rate was 2.8(5) x l0E-12 HzsE-1. This assumes the following circular orbit parameters: P = 11.83665(14) days; epoch of longitude 90 deg = JD 2450126.9977(4) TDB; a sin i = 2.6371(5) light-s (determined using data from the 1995 Dec.-l996 Apr. outburst). Earth-occultation monitoring of flux from GRO J1744-28 shows its intensity increasing by a factor of about two during 1996 Dec. 25-1997 Jan. 6. Although source confusion prevents a precise flux estimate, subtracting a 25-percent background for unresolved galactic-center sources yields a persistent flux for Jan. 3-6 in the energy bands 20-30, 30-40, and 40-50 keV of 590, 470, and 290 mcrab, respectively."

Kouveliotou, Chryssa↗
NASA NTRS2015

Effect of a Synchrotron X-ray Microtomography Imaging Experiment on the Amino Acid Content of a CM Chondrite

X-ray microcomputed tomography and synchrotron X-ray microcomputed tomography (μCT) are becoming popular tools for the reconnaissance imaging of chondrites. However, there are occasional concerns that the use of μCT may be detrimental to organic components of a chondrite. Soluble organic compounds represent ~2–10% of the total solvent extractable carbon in CI and CM carbonaceous chondrites and amino acids are among the most abundant compounds in the soluble organic fraction. We irradiated two samples of the Murchison CM2 carbonaceous chondrite under conditions slightly harsher (increased beam exposure time) than those typically used for x-ray μCT imaging experiments to determine if detectable changes in the amino acid abundance and distribution relative to a nonexposed control sample occurred. After subjecting two meteorite portions to ionizing radiation dosages of 1.1 kiloGray (kGy) and 1.2 kGy with 48.6 and 46.6 keV monochromatic X-rays, respectively, we analyzed the amino acid content of each sample. Within analytical errors, we found no differences in the amino acid abundances or enantiomeric ratios when comparing the control samples (nonexposed Murchison) and the irradiated samples. We show with calculations that any sample heating due to x-ray exposure is negligible. We conclude that a monochromatic synchrotron X-ray μCT experiment at beamline 13-BM-D of the Advanced Photon Source, which imparts ~1 kGy doses, has no detectable effect on the amino acid content of a carbonaceous chondrite. These results are important for the initial reconnaissance of returned samples from the OSIRIS-REx and Hayabusa 2 asteroid sample return missions.

Jon M. Friedrich↗
DOE OSTI2021

Determination of Seven Organic Impurities in FD&C Yellow No. 6 by Ultra-High-Performance Liquid Chromatography

The U.S. Food and Drug Administration (FDA) batch certifies FD&C Yellow No. 6 (Y6) to ensure that the color additive meets requirements published in the Code of Federal Regulations (CFR), including specifications for seven organic manufacturing impurities consisting of two intermediates, a reaction by-product, an impurity originating from an intermediate, and three subsidiary colors. An ultra-high-performance liquid chromatography (UHPLC) method was developed and validated for determining seven organic impurities in Y6. For comparison, the currently used high-performance liquid chromatography (HPLC) method was also validated. The new UHPLC method uses a 1.7 µm particle size biphenyl column with aqueous ammonium formate and methanol as eluants. Analytes are identified by comparing their retention times and UV-visible spectra to those of reference standards. Calibration is performed in the presence of the dye matrix and analyte levels are determined from their peak areas. UHPLC and HPLC validation studies obtained linear calibration curves and excellent values for limits of detection, limits of quantitation, recovery, repeatability, and intermediate precision for all analytes. Survey analyses of 30 samples using the UHPLC and HPLC methods yielded results that were consistent within experimental error; however, the UHPLC method provided more accurate results for two analytes that coelute using the HPLC method. The UHPLC method satisfies the accuracy and precision requisites for routine certification of Y6. The UHPLC method is faster and generates less waste than the HPLC method while delivering better sensitivity, separation, and accuracy.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

Collinear Three-Photon Excitation of a Strongly Forbidden Optical Clock Transition

The 1 𝑆 0 − 3 𝑃 0 clock transition in strontium serves as the foundation for the world’s best atomic clocks and for gravitational wave detector concepts in clock atom interferometry. This transition is weakly allowed in the fermionic isotope 87 Sr but strongly forbidden in bosonic isotopes. Here, we demonstrate coherent excitation of the clock transition in bosonic 88 Sr using a novel collinear three-photon process in a weak magnetic field. We observe Rabi oscillations with frequencies of up to 50 kHz using W/cm 2 laser intensities and Gauss-level magnetic field amplitudes. The absence of nuclear spin in bosonic isotopes offers decreased sensitivity to magnetic fields and optical lattice light shifts, enabling atomic clocks with reduced systematic errors. The collinear propagation of the laser fields permits the interrogation of spatially separated atomic ensembles with common laser pulses, a key requirement for dark matter searches and gravitational wave detection with next-generation quantum sensors.

74 ATOMIC AND MOLECULAR PHYSICS↗
DOE OSTI2025

Co-Firing Switchgrass and Waste Coal in A Power Plant: A Techno-Economic and Life Cycle Evaluation for The Ohio River Valley (SWITCH) (Final Technical Report for Ohio State/FE0032204)

Abandoned coal mine lands (AMLs) represent one of the most persistent environmental challenges in the United States. Prior to the enactment of the Surface Mining Control and Reclamation Act (SMCRA) in 1977, coal mining operations were not legally required to reclaim disturbed lands, leaving behind approximately 500,000 AML sites nationwide. These sites pose severe environmental and health risks, including acid mine drainage, soil and water contamination, and spontaneous combustion of waste coal piles. Millions of Americans live within one mile of these AMLs, underscoring the urgency of remediation. Traditional reclamation practices, such as planting cool-season grasses, often fail to fully restore ecological function or leverage the economic potential of these lands. This project addressed these challenges by developing integrated strategies for resource recovery, land reclamation, and sustainable energy production. This project evaluated an integrated strategy to convert this liability into an opportunity by recovering waste coal and co-firing it with switchgrass (Panicum virgatum L.) cultivated on reclaimed or marginal AML areas in existing coal-fired power plants. Switchgrass not only provides a renewable feedstock but also aids in land reclamation and carbon sequestration. 1) Remote Sensing and Machine Learning for Waste Coal Identification Using Sentinel-2 satellite imagery and supervised classification, we applied four machine learning models to detect historical waste coal piles. Random Forest achieved the highest accuracy (precision: 86%, recall: 77%). Time-series analysis revealed gradual vegetation recovery since 1986, indicating natural reclamation processes in historical sites, while active mining areas showed ongoing disturbance. This workflow enables scalable monitoring and prioritization of reclamation efforts. 2) UAS-Based Stockpile Volume Estimation To quantify recoverable waste coal, we evaluated Unmanned Aerial Systems (UAS) equipped with Light Detection and Ranging (LiDAR) and multispectral sensors. Structure-from-Motion (SfM) photogrammetry combined with interpolated Digital Terrain Models (DTMs) achieved strong agreement with LiDAR reference volumes (Root Mean Square Error (RMSE) ≈147 m 3 , Mean Absolute Percentage Error (MAPE) ≈2%). Sensitivity analysis confirmed that spatial resolution significantly influences accuracy, emphasizing the need for high-resolution data for precise volume estimation. This approach offers a scalable, cost-effective, and accurate alternative to conventional ground-based surveys. 3) Switchgrass Cultivation for Bioenergy and Water Quality Improvement We assessed the hydrological and water quality impacts of converting AMLs to switchgrass production areas using the Soil and Water Assessment Tool (SWAT). Results showed that converting 10% of the watershed area into the switchgrass production zone reduced streamflow by 3.1%, total suspended solids by 18.1%, total nitrogen by 7.6%, and total phosphorus by 6.2%, while achieving biomass yields of 8.6–9.2 metric tons per hectare. These findings highlight switchgrass as a dual-benefit strategy for land reclamation and bioenergy feedstock production. 4) Integrated Co-Firing and CCS for Carbon-Negative Power Generation We modeled co-firing scenarios using the Power Plant Flexible Model (PPFM) to evaluate plant efficiency, greenhouse gas (GHG) emissions, and levelized cost of electricity (LCOE). Without carbon capture and storage (CCS), increasing switchgrass co-firing ratios reduced LCOE from $\$$150/MWh at 0% biomass to $\$$110/MWh at full substitution. Under CCS, costs remained higher (~$\$$250/MWh at 0% biomass) but decreased to $\$$200/MWh at 100% biomass, while enabling net-zero or carbon-negative electricity due to switchgrass sequestration benefits. Although CCS introduced efficiency penalties, pairing it with biomass co-firing offset these impacts and maximized climate benefits. Overall, optimizing co-firing ratios between 60-100%, supported by reliable logistics and storage strategies, emerged as a practical pathway to balance affordability, sustainability, and net-zero or negative GHG emissions while promoting productive reuse of AMLs.

01 COAL, LIGNITE, AND PEAT↗
DOE OSTI2023

Fast-, Light-Cured Scintillating Plastic for 3D-Printing Applications

Additive manufacturing techniques enable a wide range of possibilities for novel radiation detectors spanning simple to highly complex geometries, multi-material composites, and metamaterials that are either impossible or cost prohibitive to produce using conventional methods. The present work identifies a set of promising formulations of photocurable scintillator resins capable of neutron-gamma pulse shape discrimination (PSD) to support the additive manufacturing of fast neutron detectors. The development of these resins utilizes a step-by-step, trial-and-error approach to identify different monomer and cross-linker combinations that meet the requirements for 3D printing followed by a 2-level factorial parameter study to optimize the radiation detection performance, including light yield, PSD, optical clarity, and hardness. The formulations resulted in hard, clear, PSD-capable plastic scintillators that were cured solid within 10 s using 405 nm light. The best-performing scintillator produced a light yield 83% of EJ-276 and a PSD figure of merit equaling 1.28 at 450–550 keVee.

Frandsen, Brian G. (ORCID:0000000319964320)↗
NASA NTRS1972

Conceptual design and analysis of an infared horizon sensor with compensation for atmospheric variability

A horizon detection logic, based on a ratio-of-integrated-radiance concept, which detects the earth's horizon at a relatively stable height under all geographic and meteorological conditions was evaluated by computer simulation on a body of synthesized radiance profiles. An error-sensitivity analysis of the concept was performed, and optimum design parameter values for a sensor were determined. A conceptual design for an improved 15 micron sensor based on this analysis is discussed.

Jalink, A., Jr.↗
NASA NTRS1973

Orbiting astronomical observatory-Copernicus

Of the three observatories planned in NASA's OAO program, one, OAO-3, is still in orbit and producing scientifically useful data. The prime experiment is the Princeton telescope spectrometer. Following a brief history of the OAO program, a description is given of the Princeton telescope with its 80-cm primary mirror, and of the spectrometer, which yields a resolution of up to 0.05 A. The spacecraft guidance system is also described. This system initially points the observatory to within a few arc minutes of the target, places the 0.3-arc sec slit on the star in less than 3 minutes, and holds on the star for up to 50 minutes with errors less than 0.05 arc sec. The main scientific results are described under the following categories: (1) the widespread presence of molecular hydrogen; (2) the search for other molecules, including detection of CO; (3) the nature of the interstellar medium as inferred from the detection of various atomic lines; (4) the study of chromospheres in late type stars; and (5) the study of mass loss in binaries and single stars.

York, D. G.↗
NASA NTRS1975

Automatic interface measurement and analysis

A technique for detecting and measuring the interface between two categories in classified scanner data is described together with two application demonstrations. Measurements were found to be accurate to 1.5% root mean square error on features of known length while comparison of measurements made using the technique on LANDSAT data to opisometer measurements on 1:24,000 scale maps shows excellent agreement. Application of the technique to two frames of LANDSAT data classified using a two channel, two class classifier resulted in a computation of 64 km annual decrease in shoreline length. The tidal shoreline of a portion of Alabama was measured using LANDSAT data. Based on the measurement of this portion, the total tidal shoreline length of Alabama is estimated to be 1313 kilometers.

Faller, K. H.↗
NASA NTRS1980

Aviation accidents and the theory of the situation

Social-psychological factors effecting the performance of flight crews are examined. In particular, a crew member's perceptual-psychological constructs of the flight situation (theories of the situation) are discussed. The skills and willingness of a flight crew to be alert to possible errors in the theory become critical to their effectiveness and their ability to ensure a safe flight. Several major factors that determine the likelihood that a faulty theory will be detected and revised are identified.

Bolman, L.↗
NASA NTRS1983

A new AM Her-like X-ray source

The discovery of a new X ray source associated with a binary and classifiable as a member of the AM Her class of objects is reported. The object was located with a detector on the HEAO A-2 spacecraft and by the imaging proportional counter on the Einstein Observatory. Detection occurred in the 0.15-0.4 keV band, and intensity variations of a factor of 2 were observed to happen on a time scale of around 2 hr. A location error box 0.9 deg on a side was constructed from the 2.95 deg overlapping FWHM field of view of the HEAO detector. The object, designated HO139-68, was reexamined using photometric and spectroscopic scans of it and the companion, which has been observed to be an ordinary late type star. Evidence for the presence of a magnetic white dwarf in the binary is discussed, noting indications of cyclotron emission. The X ray source flux is estimated to be 2.3/10 billion erg per sq cm per sec.

Agrawal, P. C.↗
NASA NTRS1986

Evaluation of 2 cognitive abilities tests in a dual-task environment

Most real world operators are required to perform multiple tasks simultaneously. In some cases, such as flying a high performance aircraft or trouble shooting a failing nuclear power plant, the operator's ability to time share or process in parallel" can be driven to extremes. This has created interest in selection tests of cognitive abilities. Two tests that have been suggested are the Dichotic Listening Task and the Cognitive Failures Questionnaire. Correlations between these test results and time sharing performance were obtained and the validity of these tests were examined. The primary task was a tracking task with dynamically varying bandwidth. This was performed either alone or concurrently with either another tracking task or a spatial transformation task. The results were: (1) An unexpected negative correlation was detected between the two tests; (2) The lack of correlation between either test and task performance made the predictive utility of the tests scores appear questionable; (3) Pilots made more errors on the Dichotic Listening Task than college students.

Vidulich, M. A.↗
NASA NTRS1986

Fast transients - A search in X-rays for short flares, bursts, and related phenomena

The HEAO 1 A-2 database on fast high energy X-ray transients was examined for any discernible regularities. The data were taken over the interval 1977-79 with six collimated multiwire, multilayer, proportional counters that had a sensitivity sufficient for detecting events lasting 1-5 sec at energies as low as 8-120 keV. The entire sky was surveyed completely three times in the observational period. Best-fit position, error box corners, mean transient flux and quiescent flux data are provided for all six of the type 3 events that were found. All the sources were within the Galaxy. The duration of the events ranged from 60-2000 sec. The limited number of events observed leads to estimates of 10,000-200,000 events per year. It is suggested that all the events originate from hard flares occurring at a rate of 20,000/yr on dMe/dKe stars.

Connors, A.↗
NASA NTRS1987

The imaging of extra-galactic low-energy gamma-ray sources prospects, techniques, and instrumentation

Improved understanding of the nature of active galaxies will require detailed observations of 10 to 20 sources, while understanding of their gamma ray luminosity function and its evolution will require the detection of approximately 100 sources. Instruments capable of detecting 100 active galaxies at low-energy, gamma ray energies are achievable. The angular resolution of an instrument, as well as its sensitivity, can limit the number of sources it can observe. An investigation of the angular resolution requirements for future low-energy gamma ray instruments is presented. It was found that the strictest requirements arise not from the need to resolve detectable sources, but from the need to control the level of direction-to-direction fluctuations in the diffuse background level. It was concluded that gamma-ray instruments capable of detecting 100 active galaxies must have sub-degree angular resolution. The use of the coded aperture imaging technique is proposed as a method of achieving accurate control of systematic errors and fine angular resolution without unduly increasing the time needed to conduct full sky surveys. An analysis of coded aperture imaging is presented for instruments that employ masks based on hexagonal uniformly redundant arrays. An instrument, the gamma-ray imaging payload, was built that employs these imaging techniques. The design and testing of the instrument is described in detail. Preliminary results from a balloon flight of the instruments are shown, demonstrating its imaging performance.

Finger, Mark Harold↗