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NASA NTRS1987

Development of a strain/temperature gauge and attachment system for use on carbon composites at elevated temperature

The difficulties encountered when instrumenting solid rocket motors for acquiring strain data are reviewed, emphasizing the strong temperature dependence due to apparent strain effects. The development of a strain/temperature gage to overcome some of these problems is discussed. This gage is designed to produce low apparent strain when attached to a carbon-carbon substrate. Characterization and performance data for gages attached with ceramic cement to carbon-carbon tensile coupons are presented, and the effect of a flame-sprayed installation process is discussed.

Lanius, S. J.↗

NASA NTRS1987

Tensile behavior of glass/ceramic composite materials at elevated temperatures

This paper describes the tensile behavior of high-temperature composite materials containing continuous Nicalon ceramic fiber reinforcement and glass and glass/ceramic matrices. The longitudinal properties of these materials can approach theoretical expectations for brittle matrix composites, failing at a strength and ultimate strain level consistent with those of the fibers. The brittle, high-modulus matrices result in a nonlinear stress-strain curve due to the onset of stable matrix cracking at 10 to 30 percent of the fiber strain to failure, and at strains below this range in off-axis plies. Current fibers and matrices can provide attractive properties well above 1000 C, but composites experience embrittlement in oxidizing atmospheres at 800 to 1000 C due to oxidation of a carbon interface reaction layer.The oxidation effect greatly increases the interface bond strength, causing composite embrittlement.

Mandell, J. F.↗

NASA NTRS1987

Results of an interlaboratory fatigue test program conducted on alloy 800H at room and elevated temperatures

The experimental approach adopted for low cycle fatigue tests of alloy 800H involved the use of electrohydraulic test systems, hour glass geometry specimens, diametral extensometers, and axial strain computers. Attempts to identify possible problem areas were complicated by the lack of reliable data for the heat of Alloy 800H under investigation. The method adopted was to generate definitive test data in an Interlaboratory Fatigue Test Program. The laboratories participating in the program were Argonne National Laboratory, Battelle Columbus, Mar-Test, and NASA Lewis. Fatigue tests were conducted on both solid and turbular specimens at temperatures of 20, 593, and 760 C and strain ranges of 2.0, 1.0, and 0.5 percent. The subject test method can, under certain circumstances, produce fatigue data which are serious in error. This approach subsequently was abandoned at General Atomic Company in favor of parallel gage length specimens and axial extensometers.

Ellis, J. R.↗

NASA NTRS1985

Elevated temperature strain gages

Materials were evaluated that could be used in manufacturing electrical resistance strain gages for static strain measurements at temperatures at or above 1273 K. Strain gage materials must have a characteristic response to strain, temperature and time that is reproducible or that varies in a predictable manner within specified limits. Several metallic alloys were evaluated, as well as a series of transition metal carbides, nitrides and silicides.

Brittain, J. O.↗

NASA NTRS1985

Elevated temperature crack growth

The purpose is to determine the ability of currently available P-I integrals to correlate fatigue crack propagation under conditions that simulate the turbojet engine combustor liner environment. The utility of advanced fracture mechanics measurements will also be evaluated during the course of the program. To date, an appropriate specimen design, a crack displacement measurement method, and boundary condition simulation in the computational model of the specimen were achieved. Alloy 718 was selected as an analog material based on its ability to simulate high temperature behavior at lower temperatures. Tensile and cyclic tests were run at several strain rates so that an appropriate constitutive model could be developed. Suitable P-I integrals were programmed into a finite element post-processor for eventual comparison with experimental data.

Malik, S. N.↗

NASA NTRS1988

Effects of moisture, elevated temperature, and fatigue loading on the behavior of graphite/epoxy buffer strip panels with center cracks

The effects of fatigue loading combined with moisture and heat on the behavior of graphite epoxy panels with either Kevlar-49 or S-glass buffer strips were studied. Buffer strip panels, that had a slit in the center to represent damage, were moisture conditioned or heated, fatigue loaded, and then tested in tension to measure their residual strength. The buffer strips were parallel to the loading direction and were made by replacing narrow strips of the 0 deg graphite plies with Kevlar-49 epoxy or S-glass epoxy on a 1-for-1 basis. The panels were subjected to a fatigue loading spectrum. One group of panels was preconditioned by soaking in 60 C water to produce a 1 percent weight gain then tested at room temperature. One group was heated to 82 C during the fatigue loading. Another group was moisture conditioned and then tested at 82 C. The residual strengths of the buffer panels were not highly affected by the fatigue loading, the number of repetitions of the loading spectrum, or the maximum strain level. The moisture conditioning reduced the residual strengths of the S-glass buffer strip panel by 10 to 15 percent below the ambient results. The moisture conditioning did not have a large effect on the Kevlar-49 panels.

Bigelow, C. A.↗

NASA NTRS1988

An experimental comparison of several current viscoplastic constitutive models at elevated temperature

Four current viscoplastic models are compared experimentally for Inconel 718 at 593 C. This material system responds with apparent negative strain rate sensitivity, undergoes cyclic work softening, and is susceptible to low cycle fatigue. A series of tests were performed to create a data base from which to evaluate material constants. A method to evaluate the constants is developed which draws on common assumptions for this type of material, recent advances by other researchers, and iterative techniques. A complex history test, not used in calculating the constants, is then used to compare the predictive capabilities of the models. The combination of exponentially based inelastic strain rate equations and dynamic recovery is shown to model this material system with the greatest success. The method of constant calculation developed was successfully applied to the complex material response encountered. Backstress measuring tests were found to be invaluable and to warrant further development.

James, G. H.↗

NASA NTRS1988

Elevated temperature crack growth

The problem of crack growth in hot path components such as combustor liners is complicated by several practical and theoretical considerations. The loading environment of such components involves high temperature levels and gradients that lead to considerations such as thermal stresses, crack closure, hold time, inelastic strains (both time dependent and independent), and Thermal Mechanical Fatigue (TMF). In general, a good understanding of the influence of these factors on crack growth was not obtained. At the same time, several nonlinear fracture mechanics parameters were suggested for such applications; however, most of the proposed methods were not tested for broad applications such as required for hot section components. It was the purpose of this program to evaluate proposed nonlinear methods by performing a thorough experimental and analytical study. The results illustrated that much progress was made in developing nonlinear methods.

Kim, K. S.↗

NASA NTRS1988

Fracture resistance of a TiB2 particle/SiC matrix composite at elevated temperature

The fracture resistance of a commercial TiB 2 particle/SiC matrix composite was evaluated at temperatures ranging from 20 to 1400 °C. A laser interferometric strain gauge (LISG) was used to continuously monitor the crack mouth opening displacement (CMOD) of the chevron-notched and straight-notched, three-point bend specimens used. Crack growth resistance curves (R-curves) were determined from the load versus displacement curves and displacement calibrations. Fracture toughness, work-of-fracture, and R-curve levels were found to decrease with increasing temperature. Microstructure, fracture surface, and oxidation coat were examined to explain the fracture behavior.

Fracture↗

NASA NTRS1987

Electrical Properties of Materials for Elevated Temperature Resistance Strain Gage Application

The objective was to study the electrical resistances of materials that are potentially useful as resistance strain gages at 1000 C. Transition metal carbides and nitrides, boron carbide and silicon carbide were selected for the experimental phase of this research. Due to their low temperature coefficient of resistance and good stability, TiC, ZrC, B sub 4 C and beta-SiC are suggested as good candidates for high temperature resistance strain gage applications.

Lei, Jih-Fen↗

NASA NTRS1987

A model of ocean basin crustal magnetization appropriate for satellite elevation anomalies

A model of ocean basin crustal magnetization measured at satellite altitudes is developed which will serve both as background to which anomalous magnetizations can be contrasted and as a beginning point for studies of tectonic modification of normal ocean crust. The model is based on published data concerned with the petrology and magnetization of the ocean crust and consists of viscous magnetization and induced magnetization estimated for individual crustal layers. Thermal remanent magnetization and chemical remanent magnetization are excluded from the model because seafloor spreading anomalies are too short in wavelength to be resolved at satellite altitudes. The exception to this generalization is found at the oceanic magnetic quiet zones where thermal remanent magnetization and chemical remanent magnetization must be considered along with viscous magnetization and induced magnetization.

Thomas, Herman H.↗

NASA NTRS1987

Effect of initial gamma prime size on the elevated temperature creep properties of single crystal nickel base superalloys

The influence of initial gamma-prime size and shape on the high-temperature creep properties of two single-crystal Ni-base superalloys was investigated. The two alloys were chosen to represent different magnitudes of gamma/gamma-prime lattice mismatch. A range of initial microstructures was produced by various quenching and aging treatments. Creep-rupture testing at 1000 C was performed under stresses where gamma-prime directionally coarsens to form gamma/gamma-prime lamellae in the early portion of the creep life. Both alloys exhibited a peak in creep resistance as a function of initial gamma-prime size. The peak corresponded to an initial microstructure consisting of cuboidal precipitates aligned along 001 line directions. These aligned cuboidal gamma-prime particles directionally coarsened into a relatively perfect lamellar gamma/gamma-prime structure in the early stages of creep, whereas the more irregularly shaped and distributed gamma-prime particles in both under- and overaged material formed more irregular lamellae with more imperfections. The alloy with a lower magnitude of mismatch was less sensitive to initial gamma-prime size and shape.

Nathal, M. V.↗

NASA NTRS1988

Assessing forest damage in high-elevation coniferous forests in Vermont and New Hampshire using Thematic Mapper data

This study evaluates the potential of measuring/mapping forest damage in spruce-fir forests in the Green Mountains of Vermont and White Mountains of New Hampshire using Landsat Thematic Mapper (TM) data. The TM 1.65/0.83-micron (TM5/4) and 2.22/0.83-micron (TM7/4) band ratios were found to correlate well with ground-based measurements of forest damage (a measure of percentage foliar loss) at 11 spruce-fir stands located on Camels Hump, a mountain in northern Vermont. Images using 0.56 and 1.65-micron bands with 1.65/0.83-micron band ratios indicated locations of heavy conifer forest damage. Both 1.65/0.83 and 2.22/0.83-micron band ratios were used to quantify levels of conifer forest damage among individual mountains throughout many of the Green and White Mountains. Damage was found to be consistently higher for the Green than the White Mountains.

Vogelmann, James E.↗

NASA NTRS1988

Elevated temperature durability of ceramic materials

Fast fracture, stress rupture, and cyclic high temperature durability characterizations have been conducted for advanced silicon carbide and silicon nitride ceramics applicable to gas turbine hot section components. The fast fracture and stress rupture tests were conducted in four-point flexure at temperatures of up to 1540 C; the durability tests involved cycling specimens to temperatures of 1370 C and air quenching at 200 C for up to 3500 hrs. Materials with further reliability improvements are noted to be required for gas turbine hot section component applications.

Lindberg, Laura J.↗

NASA NTRS1988

Observations on the dynamics of electromagnetically levitated liquid metals and alloys at elevated temperatures

Electromagnetic levitation and heating of small (0.5 to 1.0 gm) samples of Cu, Ni, and Ni-base alloys were performed in inert atmospheres. These experiments were recorded by high-speed photography using both regular film and video methods. Initial studies revealed interesting dynamics of the droplets that included axisymmetric oscillation, rotation, and oscillation mode changes. An attempt is made to explain the behavior using available models.

Hansen, G. P.↗

NASA NTRS1986

Elevated temperature strain gages

One of the goals of the HOST Program is the development of electrical resistance strain gages for static strain measurements at temperatures equal to or greater than 1273 K. Strain gage materials must have a reproducible or predictable response to temperature, time and strain. It is the objective of this research to investigate criteria for the selection of materials for such applications through electrical properties studies. The results of the investigation of two groups of materials, refractory compounds and binary alloy solid solutions are presented.

Brittain, J. O.↗

NASA NTRS1986

Determination of surfaces of constant inelastic strain rate at elevated temperature

An experimental effort to perform special exploratory multiaxial deformation tests on tubular specimens of type 316 stainless steel at 650 C (1200 F) is described. One test specimen was subjected to a time-independent torsional shear strain test history, and surfaces of constant inelastic strain rate (SCISRs) in an axial/torsional stress space were measured at various predetermined points during the test. A second specimen was subjected to a 14-week time-dependent (creep-recovery-creep periods) torsional shear stress histogram SCISRs determinations made at 17 points during the test. The tests were conducted in a high temperature, computer controlled axial/torsional test facility using high-temperature multiaxial extensometer. The effort was successful, and for the first time the existence of surfaces of constant inelastic strain rate was experimentally demonstrated.

Battiste, R. L.↗

NASA NTRS1986

Elevated temperature crack growth

It is necessary to relate the processes that control crack growth in the immediate vicinity of the crack tip to parameters that can be calculated from remote quantities, such as forces, stresses, or displacements. The most likely parameters appear to be certain path-independent (PI) integrals, several of which have already been proposed for application to high temperature inelastic problems. The ability of currently available PI-integrals to correlate fatigue crack propagation under conditions that simulate the engine combustor liner environment was determined. The utility of advanced fracture mechanics measurements will also be evaluated and determined during the course of the program.

Malik, S. N.↗