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At least 1,729 records · Page 96

Response of thick, notched laminates subjected to tension-compression cyclic loads

The fatigue response of a (0/24/90/-45)s4 T300-5208 graphite-epoxy laminate with a drilled centerhole subjected to fully reversed tension-compression (R=-1, T-C) constant amplitude loading was investigated. Damage evaluation techniques such as stiffness monitoring, penetrant-enhanced X-ray radiography, C-scan, laminate deply and residual strength were used to establish the mechanisms of damage development as well as the relations between this damage and the stiffness, strength and life of the laminate. Damage initiated at the hole as matrix cracking parallel to the fibers in all plies. Matrix cracks had a significant effect on delamination initiation and growth. Delaminations initiated near the surface in the densely cracked region at the hole and grew along major matrix cracks. Compressive properties degraded more rapidly than tensile properties. At the stress levels used, residual tensile strength increased early in the fatigue life and remained approximately constant to near the end of life, when failure was precipitated by excessive laminate instability during the compressive portion of the loading.

Bakis, C. E.↗

Fatigue cracking of a bare steel first wall in an inertial confinement fusion chamber

Inertial confinement fusion power plants will deposit high energy X-rays onto the outer surfaces of the first wall many times a second for the lifetime of the plant. These X-rays create brief temperature spikes in the first few microns of the wall, which cause an associated highly compressive stress response on the surface of the material. The periodicity of this stress pulse is a concern due to the possibility of fatigue cracking of the wall. We have used finite element analyses to simulate the conditions present on the first wall in order to evaluate the driving force of crack propagation on fusion-facing surface cracks. Analysis results indicate that the X-ray induced plastic compressive stress creates a region of residual tension on the surface between pulses. This tension film will likely result in surface cracking upon repeated cycling. Additionally, the compressive pulse may induce plasticity ahead of the crack tip, leaving residual tension in its wake. However, the stress amplitude decreases dramatically for depths greater than 80–100 μm into the fusion-facing surface. Crack propagation models as well as stress-life estimates agree that even though small cracks may form on the surface of the wall, they are unlikely to propagate further than 100 μm without assistance from creep or grain erosion phenomena.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Hypervelocity Impact of Unstressed and Stressed Titanium in a Whipple Configuration in Support of the Orion Crew Exploration Vehicle Service Module Propellant Tanks

Hypervelocity impacts were performed on six unstressed and six stressed titanium coupons with aluminium shielding in order to assess the effects of the partial penetration damage on the post impact micromechanical properties of titanium and on the residual strength after impact. This work is performed in support of the definition of the penetration criteria of the propellant tanks surfaces for the service module of the crew exploration vehicle where such a criterion is based on testing and analyses rather than on historical precedence. The objective of this work is to assess the effects of applied biaxial stress on the damage dynamics and morphology. The crater statistics revealed minute differences between stressed and unstressed coupon damage. The post impact residual stress analyses showed that the titanium strength properties were generally unchanged for the unstressed coupons when compared with undamaged titanium. However, high localized strains were shown near the craters during the tensile tests.

Nahra, Henry K.↗

White Paper Summary of 2nd ASTM International Workshop on Hydrides in Zirconium Alloy Cladding

This white paper recommends that ASTM International develop standards to address the potential impact of hydrides on the long term performance of irradiated zirconium alloys. The need for such standards was apparent during the 2nd ASTM International Workshop on Hydrides in Zirconium Alloy Cladding and Assembly Components, sponsored by ASTM International Committee C26.13 and held on June 10-12, 2014, in Jackson, Wyoming. The potentially adverse impacts of hydrogen and hydrides on the long term performance of irradiated zirconium-alloy cladding on used fuel were shown to depend on multiple factors such as alloy chemistry and processing, irradiation and post irradiation history, residual and applied stresses and stress states, and the service environment. These factors determine the hydrogen content and hydride morphology in the alloy, which, in turn, influence the response of the alloy to the thermo-mechanical conditions imposed (and anticipated) during storage, transport and disposal of used nuclear fuel. Workshop presentations and discussions showed that although hydrogen/hydride induced degradation of zirconium alloys may be of concern, the potential for occurrence and the extent of anticipated degradation vary throughout the nuclear industry because of the variations in hydrogen content, hydride morphology, alloy chemistry and irradiation conditions. The tools and techniques used to characterize hydrides and hydride morphologies and their impacts on material performance also vary. Such variations make site-to-site comparisons of test results and observations difficult. There is no consensus that a single material or system characteristic (e.g., reactor type, burnup, hydrogen content, end-of life stress, alloy type, drying temperature, etc.) is an effective predictor of material response during long term storage or of performance after long term storage. Multi-variable correlations made for one alloy may not represent the behavior of another alloy exposed to identical conditions and the material responses to thermo-mechanical exposures will be different depending on the materials and systems used. The discussions at the workshop showed several gaps in the standardization of processes and techniques necessary to assess the long term performance of irradiated zirconium alloy cladding during dry storage and transport. The development of, and adherence to, standards to help bridge these gaps will strengthen the technical basis for long term storage and post-storage operations, provide consistency across the nuclear industry, maximize the value of most observations, and enhance the understanding of behavioral differences among alloys. The need for, and potential benefits of, developing the recommended standards are illustrated in the various sections of this report.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Concentric tubes cold-bonded by drawing and internal expansion

Metal tubes bonded together without heat application or brazing materials retain strength at elevated temperatures, and when subjected to constant or cyclic temperature gradients. Combination drawing and expansion process produces residual tangential tensile stress in the outer tube and tangential compressive stress in the inner tube.

Hymes, L. C.↗

The strength of laminated composite materials under repeated impact loading

When low velocity and energy impact is exerted on a laminated composite material, in a perpendicular direction to the plane of the laminate, invisible damage may develop. It is shown analytically and experimentally that the invisible damage occurs during the first stage of contact between the impactor and the laminate and is a result of the contact stresses. However, the residual flexural strength changes only slightly, because it depends mainly on the outer layers, and these remain undamaged. Repeated impact intensifies the damage inside the laminate and causes larger bending under equivalent impact load. Finally, when the damage is most severe, even though it is still invisible, the laminate fails because of bending on the tension side. If the repeated impact is halted before final fracture occurs the residual strength and modulus would decrease by a certain amount.

Rotem, Assa↗

Optical fiber sensors for damage analysis in aerospace materials

Under this grant, fiber optic sensors were investigated for use in the nondestructive evaluation of aging aircraft. Specifically, optical fiber sensors for detection and location of impacts on a surface, and for detection of corrosion in metals were developed. The use of neural networks was investigated for determining impact location by processing the output of a network of fiberoptic strain sensors distributed on a surface. This approach employs triangulation to determine location by comparing the arrival times at several sensors, of the acoustic signal generated by the impact. For this study, a neural network simulator running on a personal computer was used to train a network using a back-propagation algorithm. Fiber optic extrinsic Fabry-Perot interferometer (EFPI) strain sensors are attached to or embedded in the surface, so that stress waves emanating from an impact can be detected. The ability of the network to determine impact location by time-or-arrival of acoustic signals was assessed by comparing network outputs with actual experimental results using impacts on a panel instrumented with optical fiber sensors. Using the neural network to process the sensor outputs, the impact location can be inferred to centimeter range accuracy directly from the arrival time data. In addition, the network can be trained to determine impact location, regardless of material anisotropy. Results demonstrate that a back-propagation network identifies impact location for an anisotropic graphite/bismaleimide plate with the same accuracy as that for an isotropic aluminum plate. Two different approaches were investigated for the development of fiber optic sensors for corrosion detection in metals, both utilizing optical fiber sensors with metal coatings. In the first approach, an extrinsic Fabry-Perot interferometric fiber optic strain sensor was placed under tensile stress, and while in the resulting strained position, a thick coating of metal was applied. Due to an increase in the quantity of material, the sensor does not return to its original position upon removal of the applied stress, and some residual strain is maintained within the sensor element. As the metal thickness decreases due to corrosion, this strain is released, providing the sensing mechanism for corrosion detection. In the second approach, photosensitive optical fibers with long period Bragg gratings in the core were coated with metal. The Bragg gratings serve to couple core modes at discrete wavelengths to cladding modes. Since cladding modes interact with the metal coating surrounding the fiber cladding, the specific wavelengths coupled from core to cladding depend on the refractive index of the metal coating. Therefore, as the metal corrodes, the resulting change in index of the coating may be measured by measuring the change in wavelength of the coupled mode. Results demonstrate that both approaches can be successfully used to track the loss in metal coating on the optical fiber sensors due to corrosion.

Schindler, Paul↗

Three-Axis Distributed Fiber Optic Strain Measurement in 3D Woven Composite Structures

Recent advancements in composite materials technologies have broken further from traditional designs and require advanced instrumentation and analysis capabilities. Success or failure is highly dependent on design analysis and manufacturing processes. By monitoring smart structures throughout manufacturing and service life, residual and operational stresses can be assessed and structural integrity maintained. Composite smart structures can be manufactured by integrating fiber optic sensors into existing composite materials processes such as ply layup, filament winding and three-dimensional weaving. In this work optical fiber was integrated into 3D woven composite parts at a commercial woven products manufacturing facility. The fiber was then used to monitor the structures during a VARTM manufacturing process, and subsequent static and dynamic testing. Low cost telecommunications-grade optical fiber acts as the sensor using a high resolution commercial Optical Frequency Domain Reflectometer (OFDR) system providing distributed strain measurement at spatial resolutions as low as 2mm. Strain measurements using the optical fiber sensors are correlated to resistive strain gage measurements during static structural loading. Keywords: fiber optic, distributed strain sensing, Rayleigh scatter, optical frequency domain reflectometry

Castellucci, Matt↗

Hypervelocity Impact of Unstressed and Stressed Titanium in a Whipple Configuration in Support of the Orion Crew Exploration Vehicle Service Module Propellant Tanks

Hypervelocity impacts were performed on six unstressed and six stressed titanium coupons with aluminium: shielding in order to assess the effects of the partial penetration damage on the post impact micromechanical properties of titanium and on the residual strength after impact. This work is performed in support of the defInition of the penetration criteria of the propellant and oxidizer tanks dome surfaces for the service module of the crew exploration vehicle where such a criterion is based on testing and analyses rather than on historical precedence. The objective of this work is to assess the effects of applied biaxial stress on the damage dynamics and morphology. The crater statistics revealed minute differences between stressed and unstressed coupon damage. The post impact residual stress analyses showed that the titanium strength properties were generally unchanged for the unstressed coupons when compared with undamaged titanium. However, high localized strains were shown near the craters during the tensile tests.

Nahra, Henry K.↗

Residual thermal and moisture influences on the strain energy release rate analysis of local delaminations from matrix cracks

An analysis utilizing laminated plate theory is developed to calculate the strain energy release rate associated with local delaminations originating at off-axis, single ply, matrix cracks in laminates subjected to uniaxial loads. The analysis includes the contribution of residual thermal and moisture stresses to the strain energy released. Examples are calculated for the strain energy release rate associated with local delaminations originating at 90 degrees and angle-ply (non-90 degrees) matrix ply cracks in glass epoxy and graphite epoxy laminates. The solution developed may be used to assess the relative contribution of mechanical, residual thermal, and moisture stresses on the strain energy release rate for local delamination for a variety of layups and materials.

Obrien, T. K.↗

Residual thermal and moisture influences on the analysis of local delaminations

An analysis using laminated plate theory is developed to calculate the strain energy release rate associated with local delaminations originating at off-axis, angle-ply, matrix cracks in laminates subjected to uniaxial loads. The analysis includes the contribution of residual thermal and moisture stresses to the strain energy released. Examples are calculated for the strain energy release rate associated with local delaminations originating at 90 deg and angle-ply(non 90 deg) matrix-ply cracks in glass-epoxy and graphite-epoxy laminates. The solution developed may be used to assess the relative contribution of mechanical, residual thermal, and moisture stresses on the strain energy release rate for local delamination for a variety of lay-ups and materials.

O'Brien, T. K.↗

Comparison of woven and stitched out-of-autoclave E-glass/epoxy composites subjected to quasi-static and cyclic tensile loads

Tensile quasi-static and fatigue behaviors of out-of-autoclave, quasi-isotropic, E-glass/epoxy composites with woven and stitched fiber architectures are compared. Some specimens were cyclically loaded to failure, while others were tested for residual modulus and ultimate strength. Both laminates survived 10 7 cycles at a maximum stress of 94.8 MPa but failed prior to 10 7 cycles at a maximum stress greater than or equal to 124.1 MPa. For the stress-lifetime diagram and residual strength, the woven laminate had superior properties below 10 4 cycles and the stitched laminate had superior properties above 10 5 cycles. While intralaminar crack density was higher in the stitched laminate, the woven laminate demonstrated a higher percentage of delaminated area.

Materials Science↗

A study on the thermal and moisture influences on the free-edge delamination of laminated composites

A simple delamination analysis method is presented here. It is based on a shear-type deformation theory and includes hygrothermal effects. These environmental conditions are applied to the strain energy release rate and interlaminar shear stresses. The method is applied to mixed mode edge delamination specimens made of T300/5208 graphite/epoxy material. Residual thermal and moisture stresses significantly influenced the strain energy release rate and interlaminar stresses. Both experienced large increases when thermal conditions were added to the mechanical strains. These effects were alleviated when moisture stresses were included. Thermal effects on the interlaminar shear stress and total energy release rate were totally alleviated for the same specific moisture content. Moreover, the value of the moisture content was not significantly affected by the stacking sequence for the laminates considered.

Mahler, Mary A.↗

Strong correlation between stress drop and peak ground acceleration for recent M1–4 earthquakes in the San Francisco Bay Area

Theoretical and observational studies suggest that between-event variability in the median ground motions of larger ( M≥5 ) earthquakes is controlled primarily by the dynamic properties of the earthquake source, such as Brune-type stress drop. Analogous results remain equivocal for smaller events due to the lack of comprehensive and overlapping ground-motion and source-parameter datasets in this regime. Here in this paper, we investigate the relationship between peak ground acceleration (PGA) and dynamic stress drop for a new dataset of 5297 earthquakes that occurred in the San Francisco Bay area from 2002 through 2016. For each event, we measure PGA on horizontal-component channels of stations within 100 km and estimate stress drop from P-wave spectra recorded on vertical-component channels of the same stations. We then develop a nonparametric ground-motion prediction equation (GMPE) applicable for the moderate (M 1–4) earthquakes in our study region, using a mixed-effects generalization of the Random Forest algorithm. We use the Random Forest GMPE to model the joint influence of magnitude, distance, and near-site effects on observed PGA. We observe a strong correlation between dynamic stress drop and the residual PGA of each event, with the events with higher-than-expected PGA associated with higher values of stress drop. The strength of this correlation increases as a function of magnitude but remains significant even for smaller magnitude events with corner frequencies that approach the observable bandwidth of the acceleration records. Mainshock events are characterized by systematically higher stress drop and PGA than aftershocks of equivalent magnitude. Coherent local variations in the distribution of dynamic stress drop provide observational constraints to support the future development of nonergodic GMPEs that account for variations in median stress drop at different source locations.

58 GEOSCIENCES↗

Uncovering hidden bias in neutron diffraction residual strain measurements

When calculating residual strain via neutron or X-ray diffraction, uncertainties propagated from the peak fit are often inadequate to describe the true scatter of measurements about a singular strain state, such as one that should describe a macroscopic continuum. Because diffraction is inherently a selective process, orientation-dependent scatter arises from the sub-sampling of strong microstructure and strain gradients. This paper investigates the appropriateness of propagated uncertainties with reference to their original intention, i.e. noise about a mean value. Thirty-six unique orientations of strain measurements are taken at multiple locations within an additive friction-stir deposition component with fine-scale gradients (∼200 µm) of plastic strain, texture and residual elastic strain. Multiple strain and stress calculation pathways are compared: direct substitution of three measurements into Hooke's law, direct inversion of any six unique orientations into the strain state tensor and thirty-six measurement least-squares estimation. For the last two cases, the appropriateness of the uncertainty interval is statistically evaluated on the basis of a physical constraint: common agreement under the strain transformation law. For this sample, the direct inversion of six measurements retains a conservative estimate of the uncertainty. However, propagated uncertainties in the least-squares solution greatly underestimate the true experimental scatter. A simple pathway to estimate appropriate uncertainty intervals is suggested. These results demonstrate that the interpretation of uncertainty in residual strain is strongly dependent on intrinsic sample-dependent effects, and that oversampling orientations and statistical analysis can give more accurate results with realistic uncertainties.

36 MATERIALS SCIENCE↗

Shear Behavior of Artificial Clay Seams within Bedded Salt Structures

Bedded salt contains thin layers of clay, also known as clay seams, in-between far thicker layers of salt. These inhomogeneities are thought to have first-order effects on the closure of nearby drifts and potential roof collapses. Despite their importance, characterizations of the peak shear strength and residual shear strength of clay seams in salt are extremely rare in the published literature. A previous paper reported results from laboratory direct shear experiments on clay seam samples from the Permian Basin in New Mexico. These clay seams behaved similar to intact salt, which was attributed to the abundance of salt crystals intersecting the clay seams. None of those specimens contained a distinct ¼" - ½" (6 -12 mm) thick clay seam, as has been observed in drifts at the Waste Isolation Pilot Plant (WIPP). Due to the difficulty in obtaining WIPP samples with these types of clay seams, artificial seams of bentonite and brine sandwiched between sections of salt were created and shear tested. Eight 4" diameter samples were created with either a ¼" or ½" a thick seam and then consolidated at 3000 psi prior to shear testing. The direct shear tests on these samples were performed at nominal normal stresses representative of expected WIPP in-situ conditions (500 to 1500 psi). The resulting shear stress vs. shear displacement curves exhibited a peak followed by a gradual decay of shear strength. The shear stress never transitioned to a true residual shear stress plateau, so the final shear strength at the end of each test (0.75" of shear displacement) was analyzed instead. Both the peak shear strength and the final shear strength conformed to Mohr- Coulomb behavior with friction angles and cohesion strengths consistent with a saturated, highly consolidated, clay. These new artificial clay seam results and the previous clay-interspersed-with-salt results likely bound the expected shear behavior of WIPP clay seams.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Effects of internal swelling on residual elasticity of a quasi-brittle material through a composite sphere model

This work describes the development of a micromechanical-based constitutive model accounting for the effect of internal expansion on the residual elasticity of a Hashin composite material. This material is made of spherical inclusions that are subjected to gradual swelling within a quasi-brittle matrix. The main focus of this work is to describe and analyze the material mechanical response, with an additional focus on the internal swelling’s effect on the stress–strain response and residual elasticity. Microstructural features and parameters of major importance for the mechanical responses were identified. The innovative characteristics of the proposed approach are summarized as follows: (1) a full determination of the physics of a complete-damage problem throughout the whole process of inclusion swelling with upscaling techniques, which transfers the microcrack-related properties from the lower scale to upper scale; and (2) an evolution of the mechanical fields and the corresponding residual elasticity for various inclusion swelling levels. Concerning the matrix–inclusion composite, it was hypothesized that only the matrix was susceptible to cracking, with varied degrees of damage, whereas the inclusions behave elastically and the elastic modulus of the expanding inclusions remains constant. It is to emphasize that the gradual swelling of inclusions is modeled by an increasing strain in the current micromechanical-based constitutive model, and the microcracks are represented by a set of randomly oriented penny-shaped microcracks with identical radii (namely, closed cracks). The main contribution of the current research is to establish the exact mathematical solutions for the mechanical fields (stress, strain) caused by the swelling of the inclusions (mechanical loading) and derive the effective residual elasticity of a composite (structural response) subject to internal expansion and quasi-brittle damage. Based on the assumption of closed cracks that could be extended to open cracks in the upcoming work, the results proposed by the present paper help to understand the non-linear mechanical behavior of quasi-brittle materials subject to microcracking and provide a theoretical framework to be used as academical benchmark for numerical simulations.

36 MATERIALS SCIENCE↗

Quantitative Profiling of Protein S-Glutathionylation Reveals Redox-Dependent Regulation of Macrophage Function During Nanoparticle-Induced Oxidative Stress

Engineered nanoparticles (ENPs) are emerging functional materials increasingly utilized for commercial and medical applications. Due to the potential hazard effects of ENPs to human health, it is significant to assess and understand the underlying mechanisms of nanotoxicity. Here, we investigate protein S-glutathionylation (SSG) as an underlying regulatory mechanism for ENP-induced oxidative stress in macrophages by applying a recently developed quantitative redox proteomics approach for site-specific measurements of SSG. Three high-volume production ENPs (SiO 2 , Fe 3 O 4 and CoO) were selected as representative ENPs with low, moderate, and high reactive oxygen species (ROS) activity, respectively. Among these nanoparticles, we observe that CoO led to the most significant dose-dependent oxidative stress and increase of protein SSG modifications in macrophages. Our site-specific SSG changes highlighted a broad set of redox sensitive proteins and their specific Cys residues potentially implicated in stress response. Functional analysis revealed that the most significantly enriched functional categories for SSG-modified proteins were stress response, cellular structure change, and cell death or survival. Moreover, ENPs-induce oxidative stress levels (CoO > Fe 3 O 4 > SiO 2 ) were found to correlate well with the levels of impairment of macrophage phagocytic activity and the overall degrees of increases in SSG. RNA silencing knockdown experiment of glutaredoxin 1 (Grx1) also led to a decreased phagocytic activity in macrophages, which suggested a regulatory role of SSG in phagocytosis. Together, the results provided valuable insights of protein SSG as a potential regulatory mechanism in response to nanomaterial-induced oxidative stress and immunity dysfunction.

60 APPLIED LIFE SCIENCES↗