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At least 1,711 records · Page 95
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Kinetic Isotope Effect in the Radical Step-Growth Termination of On-Surface Synthesized Graphene Nanoribbons

Bottom-up on-surface synthesis has emerged as a versatile tool to access and finely tune the electronic structure of nanographenes. The controlled generation of reactive intermediates catalyzed and stabilized by a supporting substrate has enabled the design, assembly, and characterization of a wide range of exotic tailor-made quantum materials. Even under these tightly controlled conditions, the growth of extended structures remains limited by termination processes and undesired side reactions. Here, we identify an H atom transfer as one principal contributor to the radical step growth termination that limits the on-surface growth of N = 7 armchair graphene nanoribbons (7-AGNRs) on Au(111) surfaces. Analysis of 7-AGNR lengths grown from protiated and deuterated molecular precursors reveals a primary kinetic isotope effect of KIE ∼ 1.4. First-principles density functional theory calculations suggest that a concerted H atom transfer mechanism that involves the breaking of a C–H/D bond in the transition state is associated with radical chain termination.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2025

Gating Single Molecules with Counterions

We report atomic-scale gating and visualization of local charge distribution within individual rare-earth-based molecular complexes on a metallic surface. The complexes are formed by a positively charged lanthanum ion coordinated to a (pcam)3 molecule and a negatively charged counterion trapped underneath via electrostatic interactions on a Au(111) surface. Local gating is performed by adding an additional negatively charged counterion to one side of the complex, which results in the redistribution of charges within the complex and a positive shift of the frontier orbitals. This is caused by the internal Stark effect induced by the added counterion. This effect is directly captured using tunneling spectroscopy and spectroscopic mapping at 5 K substrate temperature. The polarizability of the complex is corroborated by density functional theory and analytical calculations based on experimental findings. Furthermore, the influence of charge polarization on nearby complexes is investigated in a cluster purposely assembled using three complexes, which reveals maintaining the charge states as in single complexes. These findings will enable the design of robust charged rare-earth complexes to be tailored for potential solid-state applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Auxiliary heating and current drive physics for the ST-E1 fusion power plant

This work describes the physics basis for the proposed auxiliary heating and current drive system on the ST-E1 fusion power plant. The ST-E1 flattop plasma considered here is fully non-inductive with a bootstrap fraction of 0.9 and the remaining current driven by EC waves. Using the recently published physics-based optimization method for EC launchers (Lopez et al 2025 Plasma Phys. Control. Fusion 67 055012), we show that the target flattop ECCD can be achieved with a net efficiency of 52 kA MW −1 using fundamental O-mode (O1) with frequency range 160–200 GHz launched from the low-field side top half of the vacuum vessel (LFS top-launch). From considering two candidate rampup scenarios, we conclude that LFS top-launch O1 ECCD can be equally effective during the early stages of plasma operation, although poloidal steering might be needed. X-mode waves injected from the LFS midplane are also shown to be effective for rampup even when T e < 1 keV. We also present modeling results for the pre-conceptual design of an ICRH system proposed for ST-E1. Using TORIC, we find that an ICRH system aiming for 42–48 MHz and toroidal mode number n φ ~ 10 robustly achieves dominant ion damping via Helium-3 minority heating transitioning to second-harmonic Tritium heating. We then show that such waves can be efficiently generated by a 5-strap traveling-wave antenna (TWA) using the Petra-M code. The TWA has a 40–45 MHz passband within which ~60% of the power entering the TWA is coupled to the plasma with the remaining ~40% of the power being transmitted through the TWA and possibly recirculated; the power reflected back into the transmission lines is negligible. This passband structure persists even when the evanescent distance is increased by a factor of two, or when the magnetic-field angle is increased by 30°, demonstrating inherent load resilience that will be crucial for effective ICRH on ST-E1.

electron cyclotron↗
DOE OSTI2022

Anti-Icing Coatings using Ionomer Film Layer Structuring

This research effort examined the application of Nafion polymers in alcohol solvents as an anti-ice surface coating, as a mixture with hydrophilic polymers and freezing point depressant salt systems. Co-soluble systems of Nafion, polymer and salt were applied using dip coating methods to create smooth films for frost observation over a Peltier plate thermal system in ambient laboratory conditions. Cryo-DSC was applied to examine freezing events of the Nafion-surfactant mixtures, but the sensitivity of the measurement was insufficient to determine frost behavior. Collaborations with the Fog Chamber at Sandia-Albuquerque, and in environmental SAXS measurements with CINT-LANL were requested but were not able to be performed under the research duration. Since experimental characterization of these factors is difficult to achieve directly, computational modeling was used to guide the scientific basis for property improvement. Computational modeling was performed to improve understanding of the dynamic association between ionomer side groups and added molecules and deicing salts. The polyacrylic acid in water system was identified at the start of the project as a relevant system for exploring the effect of varying counterions on the properties of fully deprotonated polyacrylic acid (PAA) in the presence of water. Simulations were modeled with four different counterions, two monovalent counterions (K+ and Na+) and two divalent counterions (Ca2+ and Mg2+). The wt% of PAA in these systems was varied from ~10 to 80 wt% PAA for temperatures from 250K to 400K. In the second set of simulations, the interpenetration of water into a dry PAA film was studied for Na+ or Ca2+ counterions for temperatures between 300K and 400K. The result of this project is a sprayable Nafion film composite which resists ice nucleation at -20 °C for periods of greater than three hours. It is composed of Nafion polymer, hydrophilic polyethylene oxide polymer and CaCl2 anti-ice crosslinker. Durability and field performance properties remain to be determined.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1972

Effect of transient winds on the flow quality of an open-circuit wind-tunnel model

The effect of a transient wind on the test-section flow quality of an open-circuit wind tunnel was investigated experimentally. The investigation was restricted to transient wind effects associated with the inlet. A small open-circuit wind tunnel was placed outside in the real wind environment. Test-section speed and angularity as well as wind speed and direction was measured by high-response instrumentation. The inlet configuration was varied with a set of screens, a removable honeycomb, and a removable inlet lip. Acceptable flow was obtained at all wind angles and for wind- to test-section-velocity ratios up to 0.4 with an inlet configuration having five screens, a honeycomb, and a lip. With inlet configurations sensitive to winds, a transient wind parallel to the tunnel axis produced local fluctuations in test-section speed and angularity; however, oscillation of the average test-section speed was not evident. The effect of wind direction was negligible up to wind angles of 45 deg relative to the tunnel axis. At larger wind angles, flow distortions occurred primarily on the windward side of the test section.

Breunlin, D. C.↗
NASA NTRS1973

Loading and heating of a large flat plate at Mach 7 in the Langley 8-foot high-temperature structures tunnel

Surface pressure and cold-wall heating rate distributions (wall-temperature to total-temperature ratio approximately 0.2) were obtained on a large, flat calibration panel at a nominal Mach number of 7 in an 8-foot high-temperature structures tunnel. Panel dimensions were 42.5 by 60.0 in. Test objectives were: (1) to map available flat-plate loading and heating provided by the facility and (2) to determine effectiveness of leading-edge bluntness, boundary-layer trips, and aerodynamic fences in generating a uniform, streamwise turbulent flow field over the test surface of a flat-sided panel holder.

Deveikis, W. D.↗
NASA NTRS1973

Simulated meteoroid penetration of reusable surface insulation

Meteoroid impact simulation test results on insulation tiles were used to determine penetration resistance of reusable surface insulation attached to simulated shuttle structures. The probability of no meteoroid damage to a typical shuttle orbiter was determined. Specimens were plasma jet tested to determine effects of various size meteoroid cavities on their thermal performance. None of the tiles failed catastrophically, but large, egg-shaped craters did result from meteoroid penetration. The metallic side of a specimen that was completely penetrated showed a petalled hole typical for thin gage shielded structures.

Lehman, J. K.↗
NASA NTRS1977

A study of density fronts and their effects on coastal pollutants

Density fronts represent regions of extremely high gradient or discontinuity in various parameters of physical interest, the most important being the water velocity and density fields. Such fronts strongly influence pollutant dispersion, by capturing oil slicks and other pollutants concentrated in surface films and drawing them down into the water column. Satellites, aircraft and boats were used to study the behavior of different types of fronts in Delaware Bay and their effect on pollutants in order to provide a basis for improving an oil drift and spreading model. Landsat satellites provided the most effective means of determining the location and extent of frontal systems over all portions of the tidal cycle. Satellite observations of flood-associated fronts on the New Jersey side of the Bay and ebb-associated fronts on the Delaware side agreed with boat measurements and model predictions.

Klemas, V.↗
NASA NTRS1979

Vortex-lift roll-control device

A wing is described for aircraft of cropped, arrow-type planform with thin leading and side edges. The wing has a pivotable tip to alter the crop angle of the wing during flight. Increasing the crop angle causes the wing side edge to become a trailing edge which reduces the strength of the side edge vortex flow. Decreasing the crop angle causes opposite results, in particular the side edge is now a leading edge and can generate a leading edge vortex flow. The wing constitutes a roll control device for aircraft of the stated design particularly effective at higher angles of attack.

Lamar, J. E.↗
NASA NTRS1992

Optimum design of a gearbox for low vibration

A computer program was developed for designing a low vibration gearbox. The code is based on a finite element shell analysis, a modal analysis, and a structural optimization method. In the finite element analysis, a triangular shell element with 18 degrees-of-freedom is used. In the optimization method, the overall vibration energy of the gearbox is used as the objective function and is minimized at the exciting frequency by varying the finite element thickness. Modal analysis is used to derive the sensitivity of the vibration energy with respect to the design variable. The sensitivity is representative of both eigenvalues and eigenvectors. The optimum value is computed by the gradient projection method and a unidimensional search procedure under the constraint condition of constant weight. The computer code is applied to a design problem derived from an experimental gearbox in use at the NASA Lewis Research Center. The top plate and two side plates of the gearbox are redesigned and the contribution of each surface to the total vibration is determined. Results show that optimization of the top plate alone is effective in reducing total gearbox vibration.

Inoue, Katsumi↗
NASA NTRS1991

Heat transfer and core neutronics considerations of the heat pipe cooled thermionic reactor

The authors summarize the results of detailed neutronic and thermal-hydraulic evaluations of the heat pipe cooled thermionic (HPTI) reactor design, identify its key design attributes, and quantify its performance characteristics. The HPTI core uses modular, liquid-metal core heat transfer assemblies to replace the liquid-metal heat transport loop employed by in-core thermionic reactor designs of the past. The nuclear fuel, power conversion, heat transport, and heat rejection functions are all combined into a single modular unit. The reactor/converter assembly uses UN fuel pins to obtain a critical core configuration with in-core safety rods and reflector controls added to complete the subassembly. By thermally bonding the core heat transfer assemblies during the reactor core is coupled neutronically, thermally, and electrically into a modular assembly of individual power sources with cross-tied architecture. A forward-facing heat pipe radiator assembly extends from the reactor head in the shape of a frustum of a cone on the opposite side of the power system from the payload. Important virtues of the concept are the absence of any single-point failures and the ability of the core to effectively transfer the TFE waste heat load laterally to other in-core heat transfer assemblies in the event of multiple failures in either in-core and radiator heat pipes.

Determan, W. R.↗
NASA NTRS1992

Binaries in globular clusters

Recent observations have shown that globular clusters contain a substantial number of binaries most of which are believed to be primordial. We discuss different successful optical search techniques, based on radial-velocity variables, photometric variables, and the positions of stars in the color-magnitude diagram. In addition, we review searches in other wavelengths, which have turned up low-mass X-ray binaries and more recently a variety of radio pulsars. On the theoretical side, we give an overview of the different physical mechanisms through which individual binaries evolve. We discuss the various simulation techniques which recently have been employed to study the effects of a primordial binary population, and the fascinating interplay between stellar evolution and stellar dynamics which drives globular-cluster evolution.

Hut, Piet↗
NASA NTRS1937

Strain measurements on small duralumin box beams in bending

Extensive strain-gage measurements were made chiefly on the tension side of five small rectangular box beams constructed of sheet duralumin. The main conclusion was that within the test range the tension cover may be considered as being fully effective but that at any given point on the beam there may be unaccountable variations of 5 percent from the calculated stresses on the thicker sheets tested (0.044 and 0.023 inch) and of 10 percent or more on the thinnest sheet tested (0.014 inch).

Kuhn, Paul↗
NASA NTRS1993

Ridge belt-related scarps and troughs: Compressional crustal bending on Venus

Cytherean ridge arcs resulted in crustal shortening in places with either the strongest compression or weakest surface layers. Arcuate scarps on or close to the edge of the ridge arcs were compressional fronts formed by overthrust over or subduction of adjacent lowland. These ridge arcs became wider due to the propagation of new ridge formation close to previous one(s). As this process repeated itself with time, the crust became thicker and the foreland was bent either due to the excess load, overthrust or subduction event. The Salme Dorsa arc measures 100 km in width and 600 km in length. It consists of a horseshoe-like set of ridges and grooves on a gently sloping lowland. The westward arcuate ridge belt indicates lateral compressional stresses and crustal deformation from SE against the southern Ishtar Terra foreland plain. The trough on the western side of the ridge belt and tensional grabens close to the crest of the bulge to the west of the trough are due to the crustal bending and indicate effects of the load and thrust. Compression and relative movement from southeast against and over the foreland planitia have resulted in ridge belt, trough and bulge formation. The load- and/or stress-induced bending of the uppermost crust allows some estimations of the uppermost elastic lithosphere thickness. Repeated folding and thrust faulting of surface layers due to compression are indicated by four more ridge belts located close to Salme Dorsa. The northeasternmost one has short ridges located in troughs. The west-opening arcuate ridge belt interlocks with the Salme Dorsa horseshoe.

Raitala, J.↗
NASA NTRS1997

Effects of Buoyancy on Laminar and Turbulent Premixed V-Flame

Turbulent combustion occurs naturally in almost all combustion systems and involves complex dynamic coupling of chemical and fluid mechanical processes. It is considered as one of the most challenging combustion research problems today. Though buoyancy has little effect on power generating systems operating under high pressures (e.g., IC engines and turbines), flames in atmospheric burners and the operation of small to medium furnaces and boilers are profoundly affected by buoyancy. Changes in burner orientation impacts on their blow-off, flash-back and extinction limits, and their range of operation, burning rate, heat transfer, and emissions. Theoretically, buoyancy is often neglected in turbulent combustion models. Yet the modeling results are routinely compared with experiments of open laboratory flames that are obviously affected by buoyancy. This inconsistency is an obstacle to reconciling experiments and theories. Consequently, a fundamental understanding of the coupling between turbulent flames and buoyancy is significant to both turbulent combustion science and applications. The overall effect of buoyancy relates to the dynamic interaction between the flame and its surrounding, i.e., the so-called elliptical problem. The overall flame shape, its flowfield, stability, and mean and local burning rates are dictated by both upstream and downstream boundary conditions. In steady propagating premixed flames, buoyancy affects the products region downstream of the flame zone. These effects are manifested upstream through the mean and fluctuating pressure fields to influence flame stretch and flame wrinkling. Intuitively, the effects buoyancy should diminish with increasing flow momentum. This is the justification for excluding buoyancy in turbulent combustion models that treats high Reynolds number flows. The objectives of our experimental research program is to elucidate flame-buoyancy coupling processes in laminar and turbulent premixed flames, and to characterize microgravity (micro g) premixed flames. The results are used to derive appropriate scaling parameters for guiding the development of theoretical models to include the effects of buoyancy. Knowledge gain from the analysis will also contribute to further understanding of the elliptical nature of premixed flames. Our current emphasis is to examine the momentum limit above which the effects of buoyancy would become insignificant. This is accomplished by comparing the flowfields and the mean properties of normal gravity flames (+g), and reversed gravity flames (-g, up-side-down flames) at different flow velocities and turbulence intensities. Microgravity (micro g) flames experiments provide the key reference data to reconcile the differences between flames in +g and -g. As flame configuration has significant impact on premixed flames characteristics we have studied axi-symmetric conical flames and plane-symmetric rod-stabilized v-flames. The two configurations produce distinct features that dictates how the flames couple with buoyancy. In a conical flame, the hot products plume completely envelopes the flame cone and shields the flame from direct interaction with the ambient air. The plume originates at the burner rim and generates a divergent flowfield. In comparison, the products region of v-flames forms between the twin flame sheets and it is convergent towards the center-plane. Interaction with ambient air is limited to the two end regions of the stabilized rod and beyond the flame sheets.

Cheng, Robert K.↗
NASA NTRS1999

Wheat Response to Differences In Water and Nutritional Status Between Zeoponic and Hydroponic Growth Systems

Hydroponic culture has traditionally been used for controlled environment life support systems (CELSS) because the optimal environment for roots supports high growth rates. Recent developments in zeoponic substrate and microporous tube irrigation (ZPT) also offer high control of the root environment. This study compared the effect of differences in water and nutrient status of ZPT or hydroponic culture on growth and yield of wheat (Triticum aestivum L., CV 'USU-Apogee'). In a side-by-side test in a controlled environment, wheat was grown in ZPT and recirculating hydroponics to maturity. Water use by plants grown in both culture systems peaked at 15-20 L per square meters per d up to day 40, after which it declined more rapidly for plants grown in ZPT culture due to earlier senescence of leaves. No consistent differences were noted in water status between plants grown in the two culture systems. Although yield was similar, harvest index was 28% lower for plants grown in ZPT versus hydroponic culture. Sterile green tillers made up 12% and 0% of the biomass of plants grown in ZPT and hydroponic culture, respectively. Differences in biomass partitioning were attributed primarily to NH4 -N nutrition of plants grown in ZPT as compared with NO3-N in hydroponic nutrient solution. It was likely that NH4-N induced Ca deficiency produced excess tillering and lower harvest index for plants grown in ZPT culture. These results suggest that further refinements in zeoponic substrate would make ZPT culture a viable alternative for achieving high productivity in a CELSS.

Steinberg, Susan L.↗
NASA NTRS2000

Wheat response to differences in water and nutritional status between zeoponic and hydroponic growth systems

Hydroponic culture has traditionally been used for controlled environment life support systems (CELSS) because the optimal environment for roots supports high growth rates. Recent developments in zeoponic substrate and microporous tube irrigation (ZPT) also offer high control of the root environment. This study compared the effect of differences in water and nutrient status of ZPT or hydroponic culture on growth and yield of wheat (Triticum aestivum L. cv. USU-Apogee). In a side-by-side test in a controlled environment, wheat was grown in ZPT and recirculating hydroponics to maturity. Water use by plants grown in both culture systems peaked at 15 to 20 L m-2 d-1 up to Day 40, after which it declined more rapidly for plants grown in ZPT culture due to earlier senescence of leaves. No consistent differences in water status were noted between plants grown in the two culture systems. Although yield was similar, harvest index was 28% lower for plants grown in ZPT than in hydroponic culture. Sterile green tillers made up 12 and 0% of the biomass of plants grown in ZPT and hydroponic culture, respectively. Differences in biomass partitioning were attributed primarily to NH4-N nutrition of plants grown in ZPT compared with NO3-N in hydroponic nutrient solution. It is probable that NH4-N-induced Ca deficiency produced excess tillering and lower harvest index for plants grown in ZPT culture. These results suggest that further refinements in zeoponic substrate would make ZPT culture a viable alternative for achieving high productivity in a CELSS.

NASA Center JSC↗
NASA NTRS2005

Documentation: No Substitute for Communication

SO WHAT IS AN RFI? IT WAS ONE OF THE FIRST THINGS I learned about back when I started my project management career with my first large construction firm. I learned how to use these forms as a convenient and effective means of documenting the many legitimate clarifications needed on a major project. However, like most other young engineers, I also learned to use the RFI as a weapon in the ongoing battle between owners. or their designer and the construction contractors. Recently, our project team has done a few simple things to greatly reduce the waste and frustration that comes from this type of battle. The RFI form can be a great tool if used properly, and I certainly don t recommend that they be eliminated entirely. The RFI form was created to document the many clarifications that are commonly required on projects. Typically, the contractor uses the top half of the form to clarify-or request permission to vary from-the contract documents. The bottom half of the form is used to record the answer. But this seemingly simple process is plagued by a number of problems. From the contractor s perspective, RFIs are needed to secure information that should have been in the contract documents in the first place. The missing information keeps their crews from working effectively, and it makes hitting already demanding cost and schedule targets even more difficult. Owners, or their design firms, often view the RFI as a means of harassment. Both sides of the issue have legitimate complaints, and both sides cause most of their own pain.

Strickland, John↗