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At least 1,693 records · Page 94

Material characterization and specification development for 350 F curing epoxy-graphite materials

New analytical techniques and a processability laminate have been used in the development of a material specification for 350 F curing epoxy-graphite materials. The development of the specification required the evaluation of prepregs which had variations in their processing behavior that were detected only in production. Chemical techniques were used to analyze the prepregs and establish limits on the concentrations of the various chemical constituents. A batch acceptance test laminate was designed to determine suitability of prepregs for production useage. The new specification requires that the processability laminate be ultrasonically and micrographically inspected for voids and porosity. Incorporation of these and other requirements will help to insure material consistency and processability.

Rogers, A. K.↗

A three-dimensional nonlinear analysis of cross-ply rectangular composite plates

The results of a three-dimensional, geometrically nonlinear, finite-element analysis of the bending of cross-ply laminated anisotropic composite plates are presented. Individual laminae are assumed to be homogeneous, orthotropic and linearly elastic. A fully three-dimensional isoparametric finite element with eight nodes (i.e. linear element) and 24 degrees of freedom (three displacement components per node) is used to model the laminated plate. The finite element results of the linear analysis are found to agree very well with the exact solutions of cross-ply laminated rectangular plates under sinusoidal loading. The finite element results of the three-dimensional, geometrically nonlinear analysis are compared with those obtained by using a shear deformable, geometrically nonlinear, plate theory. It is found that the deflections predicted by the shear deformable plate theory are in fair agreement with those predicted by three-dimensional elasticity theory; however stresses were found to be not in good agreement.

Kuppusamy, T.↗

The mechanics of delamination in fiber-reinforced composite materials. Part 2: Delamination behavior and fracture mechanics parameters

Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extenstion. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined.

Wang, S. S.↗

Composite structural materials

Progress and plans are reported for investigations of: (1) the mechanical properties of high performance carbon fibers; (2) fatigue in composite materials; (3) moisture and temperature effects on the mechanical properties of graphite-epoxy laminates; (4) the theory of inhomogeneous swelling in epoxy resin; (5) numerical studies of the micromechanics of composite fracture; (6) free edge failures of composite laminates; (7) analysis of unbalanced laminates; (8) compact lug design; (9) quantification of Saint-Venant's principles for a general prismatic member; (10) variation of resin properties through the thickness of cured samples; and (11) the wing fuselage ensemble of the RP-1 and RP-2 sailplanes.

Ansell, G. S.↗

Fracture surface characteristics of notched angleplied graphite/epoxy composites

Composite fracture surface characteristics and related fracture modes have been investigated through extensive microscopic inspections of the fracture surfaces of notched angleplied graphite/epoxy laminates. The investigation involved 4 ply laminates of the configuration + or - theta (s) where theta = 0 deg, 3 deg, 5 deg, 10 deg, 15 deg, 30 deg, 45 deg, 60 deg, 75 deg, and 90 deg. Two-inch wide tensile specimens with 0.25 in. by 0.05 in. through-slits centered across the width were tested to fracture. The fractured surfaces were then removed and examined using a scanning electron microscope. Evaluation of the photomicrographs combined with analytical results obtained using the CODSTRAN computer code culminated in a unified set of fracture criteria for determining the mode of fracture in notched angleplied graphite/epoxy laminates.

Ginty, C. A.↗

The mechanics of delamination in fiber-reinforced composite materials. II - The delamination behavior and fracture mechanics parameters

Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extension. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined. Previously announced in STAR as N84-13222

Wang, S. S.↗

Thermal aging of graphite/polyimide composites

Celion 6000/PMR-15, Celion 6000/LARC-160, and Celion 6000/RK-99 graphite/polyimides were aged in circulating air ovens at temperatures of 202, 232, 260, and 288 C for various times, up to 15,000 h. Three unidirectional specimens were studied: short-beam-shear (SBS), flexure, and 153-mm square panels. The interior region of the square panels exhibited little or no property degradation. Based on the individually aged SBS specimen results, the relative thermal-oxidative stability from highest to lowest is as follows: PMR-15, LARC-160, RK-99, Celion 6000/PMR-15 and Celion 6000/LARC-160 laminates retained at least 80 percent of their initial flexural strengths for the duration of aging at each temperature. Celion 6000/RK-99 laminates exhibited a 20 to 50 percent loss of flexural strength at all aging temperatures. All three graphite/polyimide laminate materials degraded preferentially at the specimen edge perpendicular to the fibers.

Nelson, J. B.↗

The effect of extreme temperatures on the elastic properties and fracture behavior of graphite/polyimide composites

The influence of elevated and cryogenic temperatures on the elastic moduli and fracture strengths of several C6000/PMR-15 and C6000/NR-15082 laminates was measured. Tests were conducted at -157 C, 24 C, and 316 C (-250 F, 75 F, and 600 F). Both notched and unnotched laminates were tested. The average stress failure criterion was used to predict the fracture strength of quasi-isotropic notched laminates.

Morris, D. H.↗

Thermoplastic-carbon fiber hybrid yarn

Efforts were directed to develop processing methods to make carbon fiber/thermoplastic fiber preforms that are easy to handle and drapeable, and to consolidate them into low void content laminates. The objectives were attained with the development of the hybrid yarn concept; whereby, thermoplastic fiber can be intimately intermixed with carbon fiber into a hybrid yarn. This was demonstrated with the intermixing of Celion 3000 with a Celanese liquid crystal polymer fiber, polybutylene terepthalate fiber, or polyetheretherketone fiber. The intermixing of the thermoplastic matrix fiber and the reinforcing carbon fiber gives a preform that can be easily fabricated into laminates with low void content. Mechanical properties of the laminates were not optimized; however, initial results indicated properties typical of a thermoplastic/carbon fiber composites prepared by more conventional methods.

Ketterer, M. E.↗

Fracture analysis of notched composites

The problem of part-through cracks emanating from a central notch in a composite laminate is considered. The composite laminate is modeled as an orthotropic plate and along the branches, it is assumed that the stresses are carried by the fibers only. The stresses along the uncracked portions are assumed to be proportional to the crack opening displacement at the point. After formulating the branched crack problem, the model is applied to a(+45 deg)25 composite laminate. The stress concentration factors for the fibers are computed for various values of the spring constant K. Sample results showing the crack opening displacement are also displayed.

Deale, F.↗

Composite structural materials

Progress is reported in studies of constituent materials composite materials, generic structural elements, processing science technology, and maintaining long-term structural integrity. Topics discussed include: mechanical properties of high performance carbon fibers; fatigue in composite materials; experimental and theoretical studies of moisture and temperature effects on the mechanical properties of graphite-epoxy laminates and neat resins; numerical investigations of the micromechanics of composite fracture; delamination failures of composite laminates; effect of notch size on composite laminates; improved beam theory for anisotropic materials; variation of resin properties through the thickness of cured samples; numerical analysis composite processing; heat treatment of metal matrix composites, and the RP-1 and RP2 gliders of the sailplane project.

Ansell, G. S.↗

Use of optimum stiffness tailoring to improve the compressive strength of composite plates with holes

A structural optimization procedure is used to tailor the cross-sectional stiffness distribution of compression-loaded composite plates with holes. Minimum mass designs are obtained for plates with cross sections consisting of two different balanced symmetric laminates with 0 deg, + or - 45 deg and 90 deg plies. The plate interior region contains the hole and is designed from a softer material system with a higher failure strain than the plate exterior region. All-graphite-epoxy plates and hybrid graphite/glass-epoxy plates were studied. Other designs with different percentages of 0 deg and + or 45 deg plies in the exterior laminate are compared with the optimum designs. Designs with uniform cross-sectional stiffnesses also are compared with the tailored cross-sectional stiffness designs. Specimens of each design were tested to verify the analytical predictions. The results show that cross-sectional stiffness tailoring can increase the compressive strength and decrease the mass of compression-loaded laminated plates with holes.

Haftka, R. T.↗

Optimal design of a thermally stable composite optical bench

The Lidar Atmospheric Sensing Experiment will be performed aboard an ER-2 aircraft; the lidar system used will be mounted on a lightweight, thermally stable graphite/epoxy optical bench whose design is presently subjected to analytical study and experimental validation. Attention is given to analytical methods for the selection of such expected laminate properties as the thermal expansion coefficient, the apparent in-plane moduli, and ultimate strength. For a symmetric laminate in which one of the lamina angles remains variable, an optimal lamina angle is selected to produce a design laminate with a near-zero coefficient of thermal expansion. Finite elements are used to model the structural concept of the design, with a view to the optical bench's thermal structural response as well as the determination of the degree of success in meeting the experiment's alignment tolerances.

Gray, C. E., Jr.↗

A comparison of finite-difference and finite-element methods for calculating free edge stresses in composites

It is pointed out that edge delamination is a serious failure mechanism for laminated composite materials. Various numerical methods have been utilized in attempts to calculate the interlaminar stress components which precede delamination in a laminate. There are, however, discrepancies regarding the results provided by different methods, taking into account a finite-difference procedure, a perturbation procedure, and finite element approaches. The present investigation has the objective to assess the capacity of a finite difference method to predict the character and magnitude of the interlaminar stress distributions near an interface corner. A second purpose of the investigation is to determine if predictions by finite element method in-plane, interlaminar stress components near an interface corner represent actual laminate behavior.

Bauld, N. R., Jr.↗

Surface protection of graphite fabric/PMR-15 composites subjected to thermal oxidation

Graphite fabric/PMR-15 laminates develop matrix cracks during long-term exposure in air at temperatures in the range of 500 to 600 F. This study was performed to demonstrate the effectiveness of incorporating graphite mat surface plies as a means of reducing the developing of matrix cracks. Celion 3000 graphite fabric/PMR-15 laminates were fabricated with graphite or graphite mat/325-mesh boron powder surface plies. Laminates without mat surface plies were also fabricated for control purposes. Composite flexural strength, flexural modulus, and interlaminar shear strength were determined at 288 C before and after long-term exposure (up to 1500 hr) in air at 316 C. The results of this study showed that the incorporation of graphite mat surface plies reduces matrix cracking and improves the elevated temperature mechanical property retention characteristics of the composites.

Hanson, M. P.↗

Ultrasonic stress wave characterization of composite materials

The work reported covers three simultaneous projects. The first project was concerned with: (1) establishing the sensitivity of the acousto-ultrasonic method for evaluating subtle forms of damage development in cyclically loaded composite materials, (2) establishing the ability of the acousto-ultrasonic method for detecting initial material imperfections that lead to localized damage growth and final specimen failure, and (3) characteristics of the NBS/Proctor sensor/receiver for acousto-ultrasonic evaluation of laminated composite materials. The second project was concerned with examining the nature of the wave propagation that occurs during acoustic-ultrasonic evaluation of composite laminates and demonstrating the role of Lamb or plate wave modes and their utilization for characterizing composite laminates. The third project was concerned with the replacement of contact-type receiving piezotransducers with noncontacting laser-optical sensors for acousto-ultrasonic signal acquisition.

Duke, J. C., Jr.↗

Temperature dependent nonlinear metal matrix laminae behavior

An analytical method is described for computing the nonlinear thermal and mechanical response of laminated plates. The material model focuses upon the behavior of metal matrix materials by relating the nonlinear composite response to plasticity effects in the matrix. The foundation of the analysis is the unidirectional material model which is used to compute the instantaneous properties of the lamina based upon the properties of the fibers and matrix. The unidirectional model assumes that the fibers properties are constant with temperature and assumes that the matrix can be modelled as a temperature dependent, bilinear, kinematically hardening material. An incremental approach is used to compute average stresses in the fibers and matrix caused by arbitrary mechanical and thermal loads. The layer model is incorporated in an incremental laminated plate theory to compute the nonlinear response of laminated metal matrix composites of general orientation and stacking sequence. The report includes comparisons of the method with other analytical approaches and compares theoretical calculations with measured experimental material behavior. A section is included which describes the limitations of the material model.

Barrett, D. J.↗

Fracture analysis of notched composites

In this study the problem of part-through cracks emanating from a central notch in a composite laminate is considered. The composite laminate is modeled as an orthotropic plate and along the branches, it is assumed that the stresses are carried by the fibers only. The stresses along the uncracked portions are assumed to be proportional to the crack opening displacement at that point. After formulating the branched crack problem, the model is applied to a (4 + or - 45 deg) 2s composite laminate. The stress concentration factors for the fibers are computed for various values of the spring constant K.

Delale, F.↗