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NASA NTRS1995

Pinatubo Global- to Micro-Scale Evolution: A Unified Picture from Space, Air, and Ground Measurements

We combine space, air, and ground measurements to develop a composite picture of the post-Pinatubo aerosol, and assess the consistency and uncertainties of various measurement and retrieval techniques. impactor and optical counter measurements, as well as retrievals from optical depth spectra, paint a generally consistent picture of the evolution of particle effective radii, R(sub eff). In the first month after the eruption, although particle numbers increased by orders of magnitude, R(sub eff) was similar to the preeruption value of 4.2 micrometers, because both small (r less than 0.25 micrometers) and large (r greater than 0.6 micrometers) particles increased in number, Over the next 3-6 months, R(sub eff) increased rapidly to about 0.5 micrometers. In general, R(sub eff) continued to increase for about a year after the eruption. The peak wavelength of optical depth spectra increased from initial values of less than 0.42 micrometers to values between 0.78 and 1 micrometer. This coupled evolution in particle size distribution and optical depth spectra helps explain the relationship between the global maps of 0.5 and 1.0-micrometer optical depth derived from the AVHRR and SAGE satellite measurements. It also sets a context for evaluating remaining uncertainties in each of these satellite data products. We also make consensus recommendations for particle composition, shape, and temperature- and wavelength-dependent refractive index, and show how the latter effect on backscatter spectra can influence particle sizes retrieved from multiwavelength lidar measurements.

Russell, Philip B.↗
NASA NTRS1995

Binocular Convergence and Errors in Judged Distance While Using Head-mounted See-through Displays

Previous observations have shown that optical superposition of a physical backdrops at the judged depth of a stereoscopic virtual image moves the judged depth closer to the observer. This effect was more pronounced for slowly moving physical backdrops and was not enhanced when the virtual image was rendered as a flat shaded solid object rather than a open wire-frame. Since this change in rendering making the virtual image more completely occlude the backdrop did not effect its judged depth and since the motion of the backdrop which would have attracted visual attention and binocular convergence did Increase its perceptual displacement, it was concluded that the change In Judged depth was not due to the perceived occlusion. Rather it was concluded to be due to an increase in binocular convergence. An experimental test of this hypothesis using a unobtrusive nonius technique to detect absolute and relative convergence has confirmed the presence of convergence correlated with the magnitude of the change in judged position of this virtual Image. The practical implications of this cause are demonstrated by a second study using monocular, biocular and stereoscopic viewing conditions and the consequences for the design of head-mounted see-through displays for near work are discussed.

Ellis, Stephen R.↗
NASA NTRS2002

The Permanent and Inductive Magnetic Moments of Ganymede

Data acquired by the Galileo magnetometer on five passes by Ganymede have been used to characterize Ganymede's internal magnetic moments. Three of the five passes were useful for determination of the internal moments through quadrupole order. Models representing the internal field as the sum of dipole and quadrupole terms or as the sum of a permanent dipole field upon which is superimposed an induced magnetic dipole driven by the time varying component of the externally imposed magnetic field of Jupiter's magnetosphere give equally satisfactory fits to the data. The permanent dipole moment has an equatorial field magnitude 719 nT and is tilted by 176 degrees from the spin axis with the pole in the southern hemisphere rotated by 24 degrees from the Jupiter-facing meridian plane towards the trailing hemisphere. The data are consistent with an inductive response of a good electrical conductor of radius approximately 1 Ganymede radius. Although the data do not enable us to establish the presence of an inductive response beyond doubt, we favor the inductive response model because it gives a good fit to the data using only 4 parameters to describe the internal sources of fields, whereas the equally good dipole plus quadrupole fit requires 8 parameters. An inductive response is consistent with a buried conducting shell, probably liquid water with dissolved electrolytes, somewhere in the first few hundred km below Ganymede's surface. The depth at which the ocean is buried beneath the surface is somewhat uncertain, but our favored model suggests a depth of order 150 kilometers. As both temperature and pressure increase with depth and the melting temperature of pure ice decreases to a minimum at approximately 170 kilometer depth, it seems possible that near this location, a layer of water would be sandwiched between layers of ice.

Kivelson, M. G.↗
NASA NTRS1997

Direct Aerosol Radiative Forcing: Calculations and Measurements from the Tropospheric

Radiative forcing is defined as the change in the net (downwelling minus upwelling) radiative flux at a given level in the atmosphere. This net flux is the radiative power density available to drive climatic processes in the earth-atmosphere system below that level. Recent research shows that radiative forcing by aerosol particles is a major source of uncertainty in climate predictions. To reduce those uncertainties, TARFOX was designed to determine direct (cloud-free) radiative forcing by the aerosols in one of the world's major industrial pollution plumes--that flowing from the east coast of the US over the Atlantic Ocean. TARFOX measured a variety of aerosol radiative effects (including direct forcing) while simultaneously measuring the chemical, physical, and optical properties of the aerosol particles causing those effects. The resulting data sets permit a wide variety of tests of the consistency, or closure, among the measurements and the models that link them. Because climate predictions use the same or similar model components, closure tests help to assess and reduce prediction uncertainties. In this work we use the TARFOX-determined aerosol, gas, and surface properties to compute radiative forcing for a variety of aerosol episodes, with inadvisable optical depths ranging from 0.07 to 0.6. We calculate forcing by several techniques with varying degrees of sophistication, in part to test the range of applicability of simplified techniques--which are often the only ones feasible in climate predictions by general circulation models (GCMs). We then compare computed forcing to that determined from: (1) Upwelling and downwelling fluxes (0.3-0.7 mm and 0.7-3.0 mm) measured by radiometers on the UK MRF C-130. and (2) Daily average cloud-free absorbed solar and emitted thermal radiative flux at the top of the atmosphere derived from the AVHRR radiometer on the NOAA- 14 satellite. The calculations and measurements all yield aerosol direct radiative forcing in the range -50 to -190 W sq m per unit inadvisable optical depth. The magnitudes are about 15 to 100 times larger than the global-average direct forcing expected for the global-average sulfate aerosol optical depth of 0.04. The reasons for the larger forcing in TARFOX include the relatively large optical depths and the focus on cloud-free, daytime conditions over the dark ocean surface. These are the conditions that produce the actual major radiative forcing events that contribute to any global-average climate effect. Detailed comparisons of calculated and measured forcings for specific events are used for more refined tests of closure.

Russell, P. B.↗
NASA NTRS1998

Radiative Flux Changes by Aerosols from North America, Europe, and Africa over the Atlantic Ocean: Measurements and Calculations from TARFOX and ACE-2

Aerosol effects on atmospheric radiative fluxes provide a forcing function that is a major source of uncertainty in understanding the past climate and predicting climate change. To help reduce this uncertainty, the 1996 Tropospheric Aerosol Radiative Forcing Experiment (TARFOX) and the 1997 second Aerosol Characterization Experiment (ACE-2) measured the properties and radiative effects of American, European, and African aerosols over the Atlantic. In TARFOX, radiative fluxes and microphysics of the American aerosol were measured from the UK C-130 while optical depth spectra, aerosol composition, and other properties were measured by the University of Washington C-131A and the CIRPAS Pelican. Closure studies show that the measured flux changes agree with those derived from the aerosol measurements using several modelling approaches. The best-fit midvisible single-scatter albedos (approx. 0.89 to 0.93) obtained from the TARFOX flux comparisons are in accord with values derived by independent techniques. In ACE-2 we measured optical depth and extinction spectra for both European urban-marine aerosols and free-tropospheric African dust aerosols, using sunphotometers on the R/V Vodyanitskiy and the Pelican. Preliminary values for the radiative flux sensitivities (Delta Flux / Delta Optical depth) computed for ACE-2 aerosols (boundary layer and African dust) over ocean are similar to those found in TARFOX. Combining a satellite-derived optical depth climatology with the aerosol optical model validated for flux sensitivities in TARFOX provides first-cut estimates of aerosol-induced flux changes over the Atlantic Ocean.

Russell, P. B.↗
NASA NTRS2002

Determining the Location and Radiative Impact of Thin Cirrus Clouds using Terra data

Thin cirrus clouds (with optical depth tau much less than 1) play a potentially important role in the Earth atmosphere. The Moderate Resolution Imaging Spectroradiometer (MODIS) onboard the Terra satellite has a channel at 1.375 microns that is specifically designed to detect these clouds. During two three-day periods from December 2000 and June 2001, I show that thin cirrus clouds are ubiquitous throughout the tropics. These thin cirrus generally have optical depths below 0.05 and appear with greater frequency and optical depth near deep convection. Regressing top-of-atmosphere outgoing longwave flux data from the Clouds and the Earth's Radiant Energy System (CERES) against optical depth, we calculate that these thin clouds decrease outgoing longwave flux by approx. 1 W/sq m/(0.01 tau). This translates into longwave forcing of several W/sq m near convection and zero away from convection. Averaging over the whole tropics, these thin cirrus decrease average longwave forcing is approx. 1.4 W/sq m.

Dessler, A. E.↗
NASA NTRS2002

Global Summary MGS TES Data and Mars-Gram Validation

Mars Global Reference Atmospheric Model (Mars-GRAM 2001) is an engineering-level Mars atmosphere model widely used for many Mars mission applications. From 0-80 km, it is based on NASA Ames Mars General Circulation Model (MGCM), while above 80 km it is based on University of Arizona Mars Thermospheric General Circulation Model. Mars-GRAM 2001 and MGCM use surface topograph$ from Mars Global Surveyor Mars Orbiting Laser Altimeter (MOLA). Validation studies are described comparing Mars-GRAM with a global summary data set of Mars Global Surveyor Thermal Emission Spectrometer (TES) data. TES averages and standard deviations were assembled from binned TES data which covered surface to approx. 40 km, over more than a full Mars year (February, 1999 - June, 2001, just before start of a Mars global dust storm). TES data were binned in 10-by-10 degree latitude-longitude bins (i.e. 36 longitude bins by 19 latitude bins), 12 seasonal bins (based on 30 degree increments of Ls angle). Bin averages and standard deviations were assembled at 23 data levels (temperature at 21 pressure levels, plus surface temperature and surface pressure). Two time-of day bins were used: local time near 2 or 14 hours local time). Two dust optical depth bins wereused: infrared optical depth either less than or greater than 0.25 (which corresponds to visible optical depth either less than or greater than about 0.5). For interests in aerocapture and precision entry and landing, comparisons focused on atmospheric density. TES densities versus height were computed from TES temperature versus pressure, using assumptions of perfect gas law and hydrostatics. Mars-GRAM validation studies used density ratio (TES/Mars-GRAM) evaluated at data bin center points in space and time. Observed average TES/Mars-GRAM density ratios were generally 1+/-0.05, except at high altitudes (15-30 km, depending on season) and high latitudes (> 45 deg N), or at most altitudes in the southern hemisphere at Ls approx. 90 and 180deg). Compared to TES averages for a given latitude and season, TES data had average density standard deviation about the mean of approx. 65-10.5% (varying with height) for all data, or approx. 5-12%, depending on time of day and dust optical depth. Average standard deviation of TES/Mars-GRAM density ratio was 8.9% for local time 2 hours and 7.1% for local time 14 hours. Thus standard deviation of observed TES/Mars-GRAM density ratio, evaluated at matching positions and times, is about the same as the standard deviation of TES data about the TES mean value at a given position and season.

Justus, C.↗
NASA NTRS2003

Effect of Resonator Axis Skew on Normal Incidence Impedance

High by-pass turbofan engines have fewer fan blades and lower rotation speeds than their predecessors. Consequently, the noise suppression at the low frequency end of the noise spectra has become an increasing concern. This has led to a renewed emphasis on improving noise suppression efficiency of passive, duct liner treatments at the lower frequencies. For a variety of reasons, passive liners are comprised of locally-reacting, resonant absorbers. One reason for this design choice is to satisfy operational and economic requirements. The simplest liner design consists of a single layer of honeycomb core sandwiched between a porous facesheet and an impervious backing plate. These resonant absorbing structures are integrated into the nacelle wall and are very ef- ficient over a limited bandwidth centered on their resonance frequency. Increased noise suppression bandwidth and greater suppression at lower frequencies is typically achieved for conventional liners by increasing the liner depth and incorporating thin porous septa into the honeycomb core. However, constraints on liner depth in modern high by-pass engine nacelles severely limit the suppression bandwidth extension to lower frequencies. Also, current honeycomb core liners may not be suitable for irregular geometric volumes heretofore not considered. It is of interest, therefore, to find ways to circumvent liner depth restrictions and resonator cavity shape constraints. One way to increase effective liner depth is to skew the honeycomb core axis relative to the porous facesheet surface. Other possibilities are to alter resonator cavity shape, e.g. high aspect ratio, narrow channels that possibly include right angle bends, 180. channel fold-backs, and splayed channel walls to conform to irregular geometric constraints. These possibilities constitute the practical motivation for expanding impedance modeling capability to include unconventional resonator orientations and shapes. The work reported in this paper is in the nature of a progress report and is limited to examining the implications of resonator axis skew on the composite normal incidence impedance of an array of resonator channels. Specifically, experimental results are compared with a modified impedance prediction model for highaspect- ratio, rectangular, resonator channels with varying amounts of skew relative to the incident particle velocity. It is shown that for resonator channel widths of 1 to 2 mm, aspect ratios of 25 to 50, and skew angles of zero to sixty degrees, the surface impedance of test models can be predicted with good accuracy. Predicted resistances and reactances are particularly well correlated through the first resonance and first anti-resonance for all six test models investigated. Beyond the first anti-resonance, the impedance prediction model loses the ability to predict details of resistance and reactance but still predicts the mean trends very well.

Parrott, Tony L.↗
NASA NTRS2004

Ground Ice at the Phoenix Landing Site: A Preflight Assessment

One of the objectives of the Mars Scout mission, Phoenix, is to characterize the present state of water in the martian environment, in a location where water may play a significant role in the present and past habitability of Mars. Given the generally dry and cold climate of Mars today any substantial amount of water is expected to occur in the form of ground ice (subsurface ice) within the regolith. The Mars Odyssey Gamma Ray Spectrometer has indicated abundant subsurface hydrogen and inferred ground ice at high latitudes. Therefore, the Phoenix mission will be targeted to land in the northern high latitudes (approximately 65 degrees N - 75 degrees N) where ground ice is expected to be abundantly available for analysis. The lander will be capable of excavating, sampling, and analyzing, dry and water-rich/icy soils. The location and depth of excavation necessary to achieve the goals of sampling and analysis of icy material become important parameters to assess. In the present work we ask two key questions: 1) At what depth within the regolith do we expect to find ice? 2) How might this depth vary over the region of potential landing sites? Numerous lines of evidence can be employed to provide an indication of the presence or absence of shallow ground ice at the potential landing sites. For example geomorphology, neutrons, gamma rays, and theory each contribute clues to an overall understanding of the distribution of ice. Orbital observations provide information on a variety of spatial scales, typically 10 s of meters (patterned ground) to 100 s of kilometers (gamma rays). While information on all of these scales are important, of particular interest is how the presence and depth of ground ice might vary on spatial scales comparable to the lander and its work area. While ground ice may be stable (and present) on a regional scale, local-scale slopes and changes in the physical characteristics of soils can result in significant variations in the distribution of ice.

Mellon, M. T.↗
NASA NTRS1996

Independent Pixel and Two Dimensional Estimates of LANDSAT-Derived Cloud Field Albedo

A theoretical study has been conducted on the effects of cloud horizontal inhomogeneity on cloud albedo bias. A two-dimensional (2D) version of the Spherical Harmonic Discrete Ordinate Method (SHDOM) is used to estimate the albedo bias of the plane parallel (PP-IPA) and independent pixel (IPA-2D) approximations for a wide range of 2D cloud fields obtained from LANDSAT. They include single layer trade cumulus, open and closed cell broken stratocumulus, and solid stratocumulus boundary layer cloud fields over ocean. Findings are presented on a variety of averaging scales and are summarized as a function of cloud fraction, mean cloud optical depth, cloud aspect ratio, standard deviation of optical depth, and the gamma function parameter Y (a measure of the width of the optical depth distribution). Biases are found to be small for small cloud fraction or mean optical depth, where the cloud fields under study behave linearly. They are large (up to 0.20 for PP-IPA bias, -0.12 for IPA-2D bias) for large v. On a scene average basis PP-IPA bias can reach 0.30, while IPA-2D bias reaches its largest magnitude at -0.07. Biases due to horizontal transport (IPA-2D) are much smaller than PP-IPA biases but account for 20% RMS of the bias overall. Limitations of this work include the particular cloud field set used, assumptions of conservative scattering, constant cloud droplet size, no gas absorption or surface reflectance, and restriction to 2D radiative transport. The LANDSAT data used may also be affected by radiative smoothing.

Chambers, L. H.↗
NASA NTRS2004

Nucleation in Synoptically Forced Cirrostratus

Formation and evolution of cirrostratus in response to weak, uniform and constant synoptic forcing is simulated using a one-dimensional numerical model with explicit microphysics, in which the particle size distribution in each grid box is fully resolved. A series of tests of the model response to nucleation modes (homogeneous-freezing-only/heterogeneous nucleation) and heterogeneous nucleation parameters are performed. In the case studied here, nucleation is first activated in the prescribed moist layer. A continuous cloud-top nucleation zone with a depth depending on the vertical humidity gradient and one of the nucleation parameters is developed afterward. For the heterogeneous nucleation cases, intermittent nucleation zones in the mid-upper portion of the cloud form where the relative humidity is on the rise, because existent ice crystals do not uptake excess water vapor efficiently, and ice nuclei (IN) are available. Vertical resolution as fine as 1 m is required for realistic simulation of the homogeneous-freezing-only scenario, while the model resolution requirement is more relaxed in the cases where heterogeneous nucleation dominates. Bulk microphysical and optical properties are evaluated and compared. Ice particle number flux divergence, which is due to the vertical gradient of the gravity-induced particle sedimentation, is constantly and rapidly changing the local ice number concentration, even in the nucleation zone. When the depth of the nucleation zone is shallow, particle number concentration decreases rapidly as ice particles grow and sediment away from the nucleation zone. When the depth of the nucleation zone is large, a region of high ice number concentration can be sustained. The depth of nucleation zone is an important parameter to be considered in parametric treatments of ice cloud generation.

Lin, R.-F.↗
NASA NTRS2005

X-Ray Fluorescence Solvent Detection at the Substrate-Adhesive Interface

With environmental regulations limiting the use of volatile organic compounds, low-vapor pressure solvents have replaced traditional degreasing solvents for bond substrate preparation. When used to clean and prepare porous bond substrates such as phenolic composites, low vapor pressure solvents can penetrate deep into substrate pore networks and remain there for extended periods. Trapped solvents can interact with applied adhesives either prior to or during cure, potentially compromising bond properties. Currently, methods for characterizing solvent time-depth profiles in bond substrates are limited to bulk gravimetric or sectioning techniques. While sectioning techniques such as microtome allow construction of solvent depth profiles, their depth resolution and reliability are limited by substrate type. Sectioning techniques are particularly limited near the adhesive-substrate interface where depth resolution is further limited by adhesive-substrate hardness and, in the case of a partially cured adhesive, mechanical properties differences. Additionally, sectioning techniques cannot provide information about lateral solvent diffusion. Cross-section component mapping is an alternative method for measuring solvent migration in porous substrates that eliminates the issues associated with sectioning techniques. With cross-section mapping, the solvent-wiped substrate is sectioned perpendicular rather than parallel to the wiped surface, and the sectioned surface is analyzed for the solvent or solvent components of interest using a two-dimensional mapping or imaging technique. Solvent mapping can be performed using either direct or indirect methods. With a direct method, one or more solvent components are mapped using red or Raman spectroscopy together with a moveable sample stage and/or focal plane array detector. With an indirect method, an elemental "tag" not present in the substrate is added to the solvent before the substrate is wiped. Following cross sectioning, the tag element can then be mapped by its characteristic x-ray emission using either x-ray fluorescence, or electron-beam energy-and wavelength-dispersive x-ray spectrometry. The direct mapping techniques avoid issues of different diffusion or migration rates of solvents and elemental tags, while the indirect techniques avoid spectral resolution issues in cases where solvents and substrates have adjacent or overlapping peaks. In this study, cross-section component indirect mapping is being evaluated as a method for measuring migration of d-limonene based solvents in glass-cloth phenolic composite (GCP) prior to and during subsequent bonding and epoxy adhesive cure.

Wurth, Laura↗
NASA NTRS2005

Thermographic Characterization of Impact Damage in SiC/SiC Composite Materials

SiC/SiC composite materials targeted as turbine components for next-generation aero-engines are being investigated at NASA Glenn Research Center. In order to examine damage mechanisms in these materials, SiC/SiC coupons were impacted with 1.59 mm diameter steel spheres at increasing velocities from 115 m/s to 400 m/s. Pulsed thermography, a nondestructive evaluation technique that monitors the thermal response of a sample over time, was utilized to characterize the impact damage. A thermal standard of similar material was fabricated to aid in the interpretation of the thermographic data and to provide information regarding thermography system detection capabilities in 2.4 mm thick SiC/SiC composite materials. Flat bottom holes at various depths with aspect ratios greater than 2.5 were detectable in the thermal images. In addition, the edges of holes at depths of 1.93 mm into the sample were not as resolvable as flat bottom holes closer to the surface. Finally, cooling behavior was characterized in SiC/SiC materials and used to determine impact damage depth within an 8.5% error of a known depth.

Fox, Dennis S.↗
NASA NTRS2001

High-Frequency Focused Water-Coupled Ultrasound Used for Three-Dimensional Surface Depression Profiling

To interface with other solids, many surfaces are engineered via methods such as plating, coating, and machining to produce a functional surface ensuring successful end products. In addition, subsurface properties such as hardness, residual stress, deformation, chemical composition, and microstructure are often linked to surface characteristics. Surface topography, therefore, contains the signatures of the surface and possibly links to volumetric properties, and as a result serves as a vital link between surface design, manufacturing, and performance. Hence, surface topography can be used to diagnose, monitor, and control fabrication methods. At the NASA Glenn Research Center, the measurement of surface topography is important in developing high-temperature structural materials and for profiling the surface changes of materials during microgravity combustion experiments. A prior study demonstrated that focused air-coupled ultrasound at 1 MHz could profile surfaces with a 25-m depth resolution and a 400-m lateral resolution over a 1.4-mm depth range. In this work, we address the question of whether higher frequency focused water-coupled ultrasound can improve on these specifications. To this end, we employed 10- and 25-MHz focused ultrasonic transducers in the water-coupled mode. The surface profile results seen in this investigation for 25-MHz water-coupled ultrasound, in comparison to those for 1-MHz air-coupled ultrasound, represent an 8 times improvement in depth resolution (3 vs. 25 m seen in practice), an improvement of at least 2 times in lateral resolution (180 vs. 400 m calculated and observed in practice), and an improvement in vertical depth range of 4 times (calculated).

Roth, Don J.↗
NASA NTRS2003

Characterization of a Ultra-high Temperature Ceramic Composite

Ultra-high temperature ceramics (UHTC) are of interest for hypersonic vehicle leading edge applications. Monolithic UHTCs are of concern because of their low fracture toughness and brittle behavior. UHTC composites (UHTCC) are being investigated as a possible approach to overcome these deficiencies. In this study a small sample of a UHTCC was evaluated by limited mechanical property tests, furnace oxidation exposures, and oxidation exposures in a flowing environment. The composite was prepared from a carbon fiber perform using ceramic particulates and a preceramic polymer. The as-received composite plate was non-uniform from front to back surface. Plate dimensions were 150 x 150 x 6 mm. The back surface had a fibrous, uniform appearance; XRD analysis revealed the presence of Sic and C. The front surface was smooth and non-uniform in appearance with evidence of a coarse grain structure produced by a liquid phase; XRD analysis revealed the presence of HfB2. Microcracks were present throughout the thickness as one might expect from a carbon fiber reinforced composite with attendant large thermal expansion mismatch between the matrix phases and the fibers. The HfB2 phase on the front surface was comparable in thickness to a fiber ply or about 0.6 mm, and surface microcracks were evident. Limited four point flexural tests were carried out at span to depth ratios of approximately 14 and 16 with markedly different results. Tests were run with the front or the back surface in tension. At the shorter span to depth failures occurred under a loading pin for both orientations. At a span to depth of 16 failures occurred in the center of the span with fracture clearly initiating from a tensile failure. Ultimate flexural strength, strain at ultimate stress, stress and strain at deviation from linear elastic behavior are reported. Strains at ultimate stress ranged from about 0.6 to 0.7 % for the back surface in tension, and 0.4 to 0.6 for the front surface in tension. At constant span to depth the strain at ultimate stress was about 0.2% greater for the back surface in tension and the ultimate strength was also higher. Strengths were in line with predictions from theory. Furnace oxidation studies were carried out at 1627 and 1927OC in a static furnace environment using ten minute cycles and one, five, and ten cycles. Limited oxidation studies were also carried out in a flowing oxyacetylene torch environment. Specimens were photographed, and weight and dimensional changes were determined. XRD and SEM characterizations were performed. Weight losses were attributed primarily to carbon fiber oxidation. The composite survived the torch test with little visible distress. Further details will be determined once metallographic studies are completed.

Levine, Stanley R.↗
NASA NTRS2006

Molecular Substrate Alteration by Solar Wind Radiation Documented on Flown Genesis Mission Array Materials

The Genesis spacecraft sampling arrays were exposed to various regimes of solar wind during flight that included: 313.01 days of high-speed wind from coronal holes, 335.19 days of low-speed inter-stream wind, 191.79 days of coronal mass ejections, and 852.83 days of bulk solar wind at Lagrange 1 orbit. Ellipsometry measurements taken at NASA s Johnson Space Center show that all nine flown array materials from the four Genesis regimes have been altered by solar wind exposure during flight. These measurements show significant changes in the optical constant for all nine ultra-pure materials that flew on Genesis when compared with their non-flight material standard. This change in the optical constant (n and k) of the material suggests that the molecular structure of the all nine ultra-pure materials have been altered by solar radiation. In addition, 50 samples of float-zone and czochralski silicon bulk array ellipsometry results were modeled with an effective medium approximation layer (EMA substrate layer) revealing a solar radiation molecular damage zone depth below the SiO2 native oxide layer ranging from 392 to 613 . This bulk solar wind radiation penetration depth is comparable to the depth of solar wind implantation depth of Mg measured by SIMS and SARISA.

Calaway, Michael J.↗
NASA NTRS2006

Grain Growth and Silicates in Dense Clouds

Interstellar silicates are likely to be a part of all grains responsible for visual extinction (Av) in the diffuse interstellar medium (ISM) and dense clouds. A correlation between Av and the depth of the 9.7 micron silicate feature (measured as optical depth, tau(9.7)) is expected if the dust species are well 'mixed. In the di&se ISM, such a correlation is observed for lines of sight in the solar neighborhood. A previous study of the silicate absorption feature in the Taurus dark cloud showed a tendency for the correlation to break down at high Av (Whittet et al. 1988, MNRAS, 233,321), but the scatter was large. We have acquired Spitzer Infrared Spectrograph data of several lines of sight in the IC 5 146, Barnard 68, Chameleon I and Serpens dense clouds. Our data set spans an Av range between 2 and 35 magnitudes. All lines of sight show the 9.7 micron silicate feature. The Serpens data appear to follow the diffuse ISM correlation line whereas the data for the other clouds show a non-linear correlation between the depth of the silicate feature relative to Av, much like the trend observed in the Taurus data. In fact, it appears that for visual extinctions greater than about 10 mag, tau(9.7) begins to level off. This decrease in the growth of the depth of the 9.7 micron feature with increasing Av could indicate the effects of grain growth in dense clouds. In this poster, we explore the possibility that grain growth causes an increase in opacity (Av) without causing a corresponding increase in tau(9.7).

Pendeleton, Yvonne J.↗
NASA NTRS2006

Calibration of the EU Oxybarometer for Nakhlites

Martian meteorites have various characteristics, which are direct clues to understanding the petrogenesis of Mars rocks. The variation in oxidation state among the Martian meteorites must have important implications for redox conditions of the Martian crust/mantle and overall differentiation on Mars. Wadhwa [1] and Herd et al. [2] reported that Martian basalts were formed under a range of oxidation states, suggesting complex petrogenesis processes. The nakhlites, which have rather different characteristics from basaltic shergottites, may give us additional clues to Martian petrogenesis. The oxidation states of meteorites are usually described by the oxygen fugacity (fO2) under which the meteorites crystallized. One of the methods to estimate the oxygen fugacity is the depth of Eu anomaly. Eu(2+)/Eu(3+) is determined by the oxygen fugacity and partitioning is different for Eu(2+) and Eu(3+). Therefore, the depth of Eu anomaly in a mineral is a function of the oxygen fugacity and the Eu2+/Eu3+ in the melt from which the mineral crystallized. This method has some advantages over another major method, the two-oxide oxybarometer [3], which can more easily be affected by subsolidus processes. The Eu oxybarometer can analyze the cores of the earliest formed crystals in Martian meteorites, which means it can give us a better indication of the oxygen fugacity of the parent melt. The calibration of the Eu oxybarometer has been done with the basaltic shergottites before [4]. However, it has never been applied to nakhlites (Oe et al. [5] measured the depth of Eu anomaly in the synthetic pyroxene only at QFM). Partition coefficients are strongly affected by phase compositions, especially pyroxene Ca content and melt Al content [e.g., 5,6]. The composition of nakhlite pyroxene is rather different from basaltic shergottite pyroxene. Thus, there may be problems in applying the Eu oxybarometer calibration for the basaltic shergottites [7] to nakhlites. Thus, we report in this abstract preliminary results of our experimental calibration of the depth of Eu anomaly in pyroxene vs. oxygen fugacity for nakhlites.

Makishima, J.↗