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DOE OSTI2026

High magnetic field response of superconductivity dome in quantum artificial high−⁢𝑇 𝐶 superlattices with variable geometry

It is known that cuprate artificial high-𝑇 𝐶 superlattices (AHTS) with period 𝑑, composed of quantum wells confining interface space charge in stoichiometric Mott insulator layers (𝑆), with thickness 𝐿, at the interface with overdoped normal metallic cuprate layers (𝑁) show a superconducting dome by tuning the geometric 𝐿 over 𝑑 ratio of the SNSN superlattice with the top predicted by quantum material design engineering quantum size effects. Here we report high-field magnetotransport measurements up to 41 Tesla of AHTS across the entire superconducting dome. The results show the universal upward-concave behavior of the temperature-dependent upper critical magnetic field in low-𝑇 𝐶 samples at the rising edge and drop edge of the dome, providing strong evidence consistent with two-band superconductivity in agreement with multigap theory used for quantum design of the SNSN superlattices. The measured superconducting coherence length demonstrates that atomic-scale engineering controls not only the critical temperature but also the intrinsic pair size at Fano-Feshbach resonances physics paving the way toward next-generation quantum devices and shedding light on unconventional superconductivity.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2022

Nondestructive Evaluation of Stress Corrosion Cracking in a Welded Steel Plate Using Guided Ultrasonic Waves

Stress corrosion cracking (SCC) had occurred in early-generation high-level nuclear waste tanks constructed by welding carbon steel. This paper describes an ultrasonic inspection system and its fundamental ability to detect and quantify the length of SCC on thick welded steel plates. The finite element method (FEM) was applied to simulate the welding process to estimate the welding residual stress field. Growth of stress corrosion cracks is driven by crack stress intensities exceeding the subcritical cracking threshold intensity. The subject plate was experimentally inspected with ultrasonic nondestructive evaluation (NDE) techniques to characterize the extent of SCC. The NDE system uses a piezoelectric transducer to generate guided waves in the thick steel plate, and a scanning laser Doppler vibrometer (SLDV) to measure multidimensional time–space wavefield data over a user-defined scanning area in the plate surface. The measured wavefield data can show wave interactions in a localized area in the plate due to the presence of the discontinuities of the SCC. To generate an inspection image that can precisely show the crack’s location and/or the dimension, the wavefield data are further processed to generate inspection image that maps the entire sample plate so the crack can be clearly identified in the plate while its length can be readily estimated. In conclusion, the ultrasonic test results for crack length agree well with the visually estimated length and are close to that predicted by the FEM for cracks in the weld residual stress field.

36 MATERIALS SCIENCE↗

NASA NTRS1990

Tropical Rainfall Measuring Mission (TRMM) project. VI - Spacecraft, scientific instruments, and launching rocket. Part 3 - The electrically Scanning Microwave Radiometer and the Special Sensor Microwave/Imager

The two microwave radiometers for TRMM are designed to measure thermal microwave radiation upwelling from the earth. The Electrically Scanning Microwave Radiometer (ESMR) scans from 50 deg to the left through nadir to 50 deg to the right in 78 steps with no moving mechanical parts in a band centered at 19.35 GHz. The TRMM concept uses the radar to develop a climatology of rain-layer thickness which can be used for the interpretation of the radiometer data over a swath wider than the radar. The ESMR data are useful for estimating rain intensity only over an ocean background. The Special Sensor Microwave/Imager (SSM/I), which scans conically with three dual polarized channels at 19, 37, and 85 GHz and a single polarized channel at 22 GHz, provides a wider range of rainfall intensities. The SSM/I spins about an axis parallel to the local spacecraft vector and 128 uniformly spaced samples of the 85 GHz data are taken on each scan over a 112-deg scan region simultaneously with 64 samples of the other frequencies.

Wilheit, Thomas T.↗

NASA NTRS1999

Analysis of X-Ray Microradiographs of Al-Au Interface Quench Profile using Modeling of Solidification Including Double-Diffusion and Convection in the Melt

Experimental data on Al-0.8Au horizontal solidification of a 1 mm thick specimen in a BN crucible shows the effect of growth rate on the solidification interface shape. For translation rates below 0.5 micron/s the interface maintains a plain and flat shape. When the translation rate is 3 to 5 micron/s or more, the interface appearance changes to two planar zones, with the zone closer to the bottom having higher inclination. The interface shapes were measured by first quenching in place during growth. X-ray microscopy shows the interface shape within the quenched sample by viewing through the side of the specimen. In order to provide theoretical explanation of the phenomena, numerical modeling was undertaken using finite element code FIDAP. Double diffusion convection in Al-0.8Au melt and crystal-melt interface curvature during directional solidification was analyzed numerically. Actual thermophysical properties of Al-0.8Au including the binary Al-Au phase diagram were used. Although convection in the sample is weak, for the slower translation rate convection and diffusion is sufficient for the redistribution of initial compositional stratification caused by gravity. When translation rate is raised, neither convection nor diffusion can provide proper mixing so that solidification temperatures differ significantly near the bottom within the bulk of the sample. As a result, the solid-liquid interface appears to have two planar zones with different inclination.

Bune, Andris V.↗

NASA NTRS1974

Grain size and the evolution of lunar soils

Grain-size data are presented for Apollo-17 soils, and the relationship is considered between grain-size distribution and the processes which pulverize the soil, reconstitute it as agglutinates, and replenish it with fresh material. It is shown that a strong inverse correlation exists between mean grain size and standard deviation and that there is a correlation between grain size and agglutinate content whereby the finest samples have the highest agglutinate content. Two evolutionary sequences are described for the soils in which (1) reworking by micrometeorites predominates over mixing with other soils and (2) mixing predominates over reworking. It is shown that the final result of soil evolution may be a steady-state soil where pulverization by micrometeorites is balanced by agglutination and replenishment of coarser grains. A model is presented for such a soil, and it is argued that its grain-size distribution may depend on regolith thickness.-

Mckay, D. S.↗

DOE OSTI2024

Weak shock compaction on granular salt

This study conducted integrated experiments and computational modeling to investigate the speeds of a developing shock within granular salt and analyzed the effect of various impact velocities up to 245 m/s. Experiments were conducted on table salt utilizing a novel setup with a considerable bore length for the sample, enabling visualization of a moving shock wave. Experimental analysis using particle image velocimetry enabled the characterization of shock velocity and particle velocity histories. Mesoscale simulations further enabled advanced analysis of the shock wave’s substructure. In simulations, the shock front’s precursor was shown to have a heterogeneous nature, which is usually modeled as uniform in continuum analyses. The presence of force chains results in a spread out of the shock precursor over a greater ramp distance. With increasing impact velocity, the shock front thickness reduces, and the precursor of the shock front becomes less heterogeneous. Furthermore, mesoscale modeling suggests the formation of force chains behind the shock front, even under the conditions of weak shock. This study presents novel mesoscale simulation results on salt corroborated with data from experiments, thereby characterizing the compaction front speeds in the weak shock regime.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1985

Vapor deposited emittance/catalysis coatings for superalloys in heatshield applications

Statically oxidized Inconel 617 and MA 956 superalloys were prepared with vapor deposited aluminosilicate layers and exposed to temperatures which simulated reentry conditions. The aluminosilicate layers were 1-2 microns thick. The trials consisted of exposures to 1500-2300 F heat while surface temperatures were monitored with pyrometers. Analyses were then performed of the catalytic activity, oxidation phenomena, and radiative properties after thermal cycling the specimens for 8 hr. Both alloys were found to be catalytic to the recombination processes of dissociated species in the reentry environment. The coatings reduced the catalytic activity by 40 percent for both alloys but did not change the emittance. An enhanced Cr depletion zone was detected in the Inconel samples, implying that the coating did not prevent diffusion loss of Cr. The coated MA 956, on the other hand, gained weight over the course of the trials.

Clark, R. K.↗

NASA NTRS1999

Bidirectional Reflectance of a Macroscopically Flat, High-Albedo Particulate Surface: An Efficient Radiative Transfer Solution and Applications to Regoliths

Many remote sensing applications rely on accurate knowledge of the bidirectional reflection function (BRF) of surfaces composed of discrete, randomly positioned scattering particles. Theoretical computations of BRFs for plane-parallel particulate layers are usually reduced to solving the radiative transfer equation (RTE) using one of existing exact or approximate techniques. Since semi-empirical approximate approaches are notorious for their low accuracy, violation of the energy conservation law, and ability to produce unphysical results, the use of numerically exact solutions of RTE has gained justified popularity. For example, the computation of BRFs for macroscopically flat particulate surfaces in many geophysical publications is based on the adding-doubling (AD) and discrete ordinate (DO) methods. A further saving of computer resources can be achieved by using a more efficient technique to solve the plane-parallel RTE than the AD and DO methods. Since many natural particulate surfaces can be well represented by the model of an optically semi-infinite, homogeneous scattering layer, one can find the BRF directly by solving the Ambartsumian's nonlinear integral equation using a simple iterative technique. In this way, the computation of the internal radiation field is avoided and the computer code becomes highly efficient and very accurate and compact. Furthermore, the BRF thus obtained fully obeys the fundamental physical laws of energy conservation and reciprocity. In this paper, we discuss numerical aspects and the computer implementation of this technique, examine the applicability of the Henyey-Greenstein phase function and the sigma-Eddington approximation in BRF and flux calculations, and describe sample applications demonstrating the potential effect of particle shape on the bidirectional reflectance of flat regolith surfaces. Although the effects of packing density and coherent backscattering are currently neglected, they can also be incorporated. The FORTRAN implementation of the technique is available on the World Wide Web, and can be applied to a wide range of remote sensing problems. BRF computations for undulated (macroscopically rough) surfaces are more complicated and often rely on time consuming Monte Carlo procedures. This approach is especially inefficient for optically thick, weakly absorbing media (e.g., snow and desert surfaces at visible wavelengths since a photon may undergo many internal scattering events before it exists the medium or is absorbed. However, undulated surfaces can often be represented as collections of locally flat tilted facets characterized by the BRF found from the traditional plane parallel RTE. In this way the MOnte Carlo procedure could be used only to evaluate the effects of surface shadowing and multiple surface reflections, thereby bypassing the time-consuming ray tracing inside the medium and providing a great savings of CPU time.

Mishchenko, Michael I.↗

NASA NTRS2001

Experimental Structural Dynamic Response of Plate Specimens Due to Sonic Loads in a Progressive Wave Tube

The objective of the current study was to assess the repeatability of experiments at NASA Langley's Thermal Acoustic Fatigue Apparatus (TAFA) facility and to use these experiments to validate numerical models. Experiments show that power spectral density (PSD) curves were repeatable except at the resonant frequencies, which tended to vary between 5 Hz to 15 Hz. Results show that the thinner specimen had more variability in the resonant frequency location than the thicker sample, especially for modes higher than the first mode in the frequency range. Root Mean Square (RMS) tended to be more repeatable. The RMS behaved linearly through the SPL range of 135 to 153 dB. Standard Deviations (STDs) of the results tended to be relatively low constant up to about 147 dB. The RMS results were more repeatable than the PDS results. The STD results were less than 10% of the RMS results for both the 0.125 in (0.318 cm) and 0.062 in (0.1588 cm) thick plate. The STD of the PSD results were around 20% to 100% of the mean PSD results for non-resonant and resonant frequencies, respectively, for the 0.125 in (0.318 cm) thicker plate and between 25% to 125% of the mean PSD results, for nonresonant and resonant frequencies, respectively, for the thinner plate.

Betts, Juan F.↗

NASA NTRS2010

The Epiregolith

The physical properties of the lunar regolith were originally inferred from remotely sensed data, first from the Earth and later from orbiting spacecraft. The Surveyor landings and the Apollo surface explorations produced a more concrete characterization of the macroscopic properties. In general, the upper regolith consists of a loosely consolidated layer centimeters thick underlain by a particulate but extremely compacted layer to depths of meters or tens of meters. The median particle size as determined by mechanical sieving in terrestrial laboratories is several tens of micrometers. However, the comminuting processes that form the layer produce particles in all sizes down to manometers. The smallest particles, having a high surface to volume ratio, tend to be electrostatically bound to larger particles and are quite difficult to separate mechanically in the laboratory. Particle size distributions determined from lunar soil samples often group particles smaller than 10 micrometers.

Mendell, Wendell W.↗

NASA NTRS1980

Variations in interior morphology of 15-20 km lunar craters - Implications for a major subsurface discontinuity

Craters vary in morphology as a function of crater diameter, age, and mode of origin. This study concentrates on the morphology of young lunar impact craters within a limited size range. Elimination of morphologic variations generally attributed to crater size or age leaves a small population which should nearly reflect the varying properties of the lunar substrate. The sample consists of 17 craters 15-20 km in diameter with both simple and complex morphologies. While depth/diameter ratios do not obviously differ between mare and highland subsets, apparent depth, rim height, and profile data do differ distinctly. Highland craters tend to be deep, simple, and bowl-shaped. Mare craters tend to be shallow and flat-floored. Rim heights of complex mare craters are typically greater than those of simple craters. Differences of highland and mare crater morphologies are attributed to variations in the thickness of the lunar megaregolith. Highland craters in this size range do not penetrate the megaregolith. The depth and morphology of complex craters are controlled by the discontinuity at the transition from highly brecciated megaregolith to more coherent crystalline material of the upper crust.

De Hon, R. A.↗

NASA NTRS1986

Effect of intervening galaxies on quasar counts and colors

Ostriker and Heisler (1984) suggested that optically thick dust in galaxies could reduce the number of high-redshift quasars without reddening the observed quasars, because the only observed quasars would be those seen through no intervening galaxies. However, Ostriker and Heisler assumed that galaxies were hard-edged uniform disks, and the fuzzy edges of real galaxies significantly change this conclusion. The quasar distribution observed through more realistic galaxy models is calculated, and it is found that dust cannot significantly reduce the high-redshift quasar counts without also reddening the observed sample. But this reddening could be consistent with past studies of quasar reddening; improved studies of quasar reddening using new UV and IR data are needed.

Wright, Edward L.↗

NASA NTRS2008

Climate Quality Broadband and Narrowband Solar Reflected Radiance Calibration Between Sensors in Orbit

vAs the potential impacts of global climate change become more clear [1], the need to determine the accuracy of climate prediction over decade-to-century time scales has become an urgent and critical challenge. The most critical tests of climate model predictions will occur using observations of decadal changes in climate forcing, response, and feedback variables. Many of these key climate variables are observed by remotely sensing the global distribution of reflected solar spectral and broadband radiance. These "reflected solar" variables include aerosols, clouds, radiative fluxes, snow, ice, vegetation, ocean color, and land cover. Achieving sufficient satellite instrument accuracy, stability, and overlap to rigorously observe decadal change signals has proven very difficult in most cases and has not yet been achieved in others [2]. One of the earliest efforts to make climate quality observations was for Earth Radiation Budget: Nimbus 6/7 in the late 1970s, ERBE in the 1980s/90s, and CERES in 2000s are examples of the most complete global records. The recent CERES data products have carried out the most extensive intercomparisons because if the need to merge data from up to 11 instruments (CERES, MODIS, geostationary imagers) on 7 spacecraft (Terra, Aqua, and 5 geostationary) for any given month. In order to achieve climate calibration for cloud feedbacks, the radiative effect of clear-sky, all-sky, and cloud radiative effect must all be made with very high stability and accuracy. For shortwave solar reflected flux, even the 1% CERES broadband absolute accuracy (1-sigma confidence bound) is not sufficient to allow gaps in the radiation record for decadal climate change. Typical absolute accuracy for the best narrowband sensors like SeaWiFS, MISR, and MODIS range from 2 to 4% (1-sigma). IPCC greenhouse gas radiative forcing is approx. 0.6 W/sq m per decade or 0.6% of the global mean shortwave reflected flux, so that a 50% cloud feedback would change the global reflected flux by approx. 0.3 W/sq m or 0.3% per decade in broadband SW calibration change. Recent results comparing CERES reflected flux changes with MODIS, MISR, and SeaWiFS narrowband changes concluded that only SeaWiFS and CERES were approaching sufficient stability in calibration for decadal climate change [3]. Results using deep convective clouds in the optically thick limit as a stability target may prove very effective for improving past data sets like ISCCP. Results for intercalibration of geostationary imagers to CERES using an entire month of regional nearly coincident data demonstrates new approaches to constraining the calibration of current geostationary imagers. The new Decadal Survey Mission CLARREO is examining future approaches to a "NIST-in-Orbit" approach of very high absolute accuracy reference radiometers that cover the full solar and infrared spectrum at high spectral resolution but at low spatial resolution. Sampling studies have shown that a precessing CLARREO mission could calibrate other geo and leo reflected solar radiation and thermal infrared sensors.

Wielicki, Bruce A.↗

DOE OSTI2026

Identifying Strain Stacking Boundaries between Multiphase Domains in Atomically Thin Two-Dimensional Magnets

Stacking engineering of van der Waals materials is an important strategy to control the materials’ properties, such as electronic correlations, ferroelectricity, and layer-dependent two-dimensional magnetism. A timely testbed for the study of the latter is atomically thin chromium trihalides (CrX 3 , X = Cl, Br, I). Notably, by understanding the sliding mechanism between different stacking sequences, control of the stacking arrangement, and thus magnetic properties in CrX 3 , can be achieved. Such insight, however, is currently lacking. Here, in this study, advanced electron microscopy methods are used to identify multiple stacking sequences corresponding to different bulk phases in atomically thin CrX 3 (X = Cl and Br) down to bilayer thickness and with lateral domain sizes as small as tens of nanometers. Indications of nanometer scale transitions and interactions at the stacking boundaries are found, including a universally preferred sliding direction that is consistent with density functional theory calculations and the strain fields at lateral heterostructure boundaries. This study demonstrates the necessity to consider local stacking structures when interpreting averaged magnetic properties measured with macroscale probes. Additionally, the preferred sliding direction insight from this study provides a strategy to control stacking sequence in atomically thin CrX 3 samples during the exfoliation and sample fabrication process.

DFT calculations↗

DOE OSTI2020

Atomic force microscopy phase imaging of epitaxial graphene films

Abstract Dynamic mode atomic force microscopy phase imaging is known to produce distinct contrast between graphene areas of different atomic thickness. But the intrinsic complexity of the processes controlling the tip motion and the phase angle shift excludes its use as an independent technique for a quantitative type of analysis. By investigating the relationship between the phase shift, the tip-surface interaction, and the thickness of the epitaxial graphene areas grown on silicon carbide, we shed light on the origin of such phase contrast, and on the complex energy dissipation processes underlying phase imaging. In particular, we study the behavior of phase shift and energy dissipation when imaging the interfacial buffer layer, single-layer, and bilayer graphene regions as a function of the tip-surface separation and the interaction forces. Finally, we compare these results with those obtained on differently-grown quasi free standing single- and bilayer graphene samples.

Lavini, Francesco (ORCID:0000000257223040)↗

NASA NTRS1973

Elastic wave velocities in anorthosite and anorthositic gabbros from Apollo 15 and 16 landing sites

Laboratory measurements of ultrasonic velocities in lunar samples 15065, 15555, 15415, 60015, and 61016 as well as in synthetic materials corresponding to compositions of anorthositic gabbros are presented as a function of hydrostatic pressure to about 7 kb. The author examined the seismic velocity distributions in the moon with reference to the variations to be expected in a homogeneous medium. The lunar mantle begins about 60 km, and the velocity of P waves in this area is about 7.7 km/sec. Variation of the seismic parameter with depth in the upper crust (about 20 km thick) is much too rapid to be explained by compression of a uniform material and the departure from expectation is so great that no reasonable adjustment of the material parameters can bring agreement; therefore, this author concludes that this result in this region of the moon is not due to self-compression but to textural gradients. In the lower crust (about 40 km thick), the region is shown to be relatively homogeneous, consisting probably of anorthositic rocks.

Chung, D. H.↗

NASA NTRS1982

Sigma/deg/ signature of the Amazon rain forest obtained from the Seasat scatterometer

Scatterometer data from Seasat of the Amazon rain forest were examined to determine if the region is suitable to use as a reference for calibration of radars. The consistency of Skylab data viewing the Amazon region prompted the analyses, and the Seasat-A scatterometer system (SASS) gathered data of the same region at varying angles. The instrument employed a 100 W 14.6 GHz signal with the reflected power sampled 61 times during each 1.89 sec measurement period. Doppler filters were used in 15 parallel channels of reception, and represented areas 20 km by 50-70 km. Tests were made of regional and temporal stability of the Amazon area, with five measurement angles averaged at different incidence angles to find the mean deviation, which was found to be less than 0.5 dB. Diurnal effects were confined to early morning, and further tests are recommended to obtain results for an entire year, to develop screening methods for thick clouds and rain, and to determine the deviation more precisely.

Birrer, I. J.↗

NASA NTRS2002

Parameterization of Cloud Optical Properties for a Mixture of Ice Particles for use in Atmospheric Models

Based on the single-scattering optical properties that are pre-computed using an improve geometric optics method, the bulk mass absorption coefficient, single-scattering albedo, and asymmetry factor of ice particles have been parameterized as a function of the mean effective particle size of a mixture of ice habits. The parameterization has been applied to compute fluxes for sample clouds with various particle size distributions and assumed mixtures of particle habits. Compared to the parameterization for a single habit of hexagonal column, the solar heating of clouds computed with the parameterization for a mixture of habits is smaller due to a smaller cosingle-scattering albedo. Whereas the net downward fluxes at the TOA and surface are larger due to a larger asymmetry factor. The maximum difference in the cloud heating rate is approx. 0.2 C per day, which occurs in clouds with an optical thickness greater than 3 and the solar zenith angle less than 45 degrees. Flux difference is less than 10 W per square meters for the optical thickness ranging from 0.6 to 10 and the entire range of the solar zenith angle. The maximum flux difference is approximately 3%, which occurs around an optical thickness of 1 and at high solar zenith angles.

Chou, Ming-Dah↗