Drilled-core storage heater for a hypersonic tunnel
Graphite drilled-core storage heater for supplying heated nitrogen gas to supersonic tunnel
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Graphite drilled-core storage heater for supplying heated nitrogen gas to supersonic tunnel
Low cost graphite powder and phenolic resin molding compounds for use in rocket engine nozzles
Design, characteristics, and test firing of radiation and film cooled 25 pound thrust graphitic thrust chamber with liquid cryogenic propellants
Analysis of reacting flow of pyrolysis products through char layer of low density, nylon phenolic resin, charring ablators and porous graphite
Interstellar molecular hydrogen formation by physical adsorption on grains, determining H atoms adsorptive potentials on silicates, graphite, solid hydrogen and ice
Thermal emission from IR star shells calculated from circumstellar graphite dust model
Diffuse interstellar bands polarization and extinction based on silicate and graphite grain composition and sizes
Meteoritic graphite, silicon carbide and silicates to explain observed interstellar grains properties
Thermally stable polyimide graphite fiber reinforced composites from solutions of monomeric reactions, comparing amide acid prepolymers
Graphitic ablative heat shield fractions and forebody configurations for probe entry into atmospheres of Saturn, Uranus and Neptune
Depositing carbon on high-temperature substrate that is kept in motion by vibration produces isotropic pyrolytic graphite or carbon without using fluidized beds.
Self-supporting membrane electrode structures, in which active ingredients and graphite are incorporated in a polymeric matrix, improve performance of electrodes in miniature, sealed, alkaline storage batteries.
Computer program has been specifically developed to handle, in an efficient and cost effective manner, planar wound pressure vessels fabricated of either boron-epoxy or graphite-epoxy advanced composite materials.
Fracture energies of WC-6Co, Boride 5 (ZrB2+SiC), Boride 8(ZrB2+SiC+C) and Boride 8-M2(ZrB2+SiC+C) were measured by slow bend and impact tests of notched charpy bars. Cobalt bonded tungsten carbide exhibited impact energies of 0.76 ft-lb or 73.9 in-lb/square inch. Boride 5 and the Boride 8 exhibit impact energies one third and one quarter of that observed for WC-6Co comparing favorably with measurements for SiC and Si3N4. Slow bend-notched bar-fracture energies for WC-6Co were near 2.6 in-lb/square inch or 1/20 the impact energies. Slow bend energies for Boride 8-M2, Boride 8 and Boride 5 were 58%, 42% and 25% of the value observed for WC-6Co. Fractograph showed differences for WC-6Co where slow bend testing resulted in smooth transgranular cleavage while samples broken by impact exhibited intergranular failures. By contrast the boride fractures showed no distinction based on testing method. Fabrication studies were conducted to effect alteration of the boride composites by alloying and introduction of graphite cloth.
A method for preparing thermally stable resin-fiber-reinforced composites by using solutions of appropriate monomers is described. Solutions containing a dimethyl ester of an aryl tetracarboxylic acid, the monomethyl ester of nadic acid, and an aryl diamine were used to impregnate graphite fibers. Composites fabricated from these prepregs exhibited excellent thermo-oxidative stability and retention of mechanical properties at 315 C (600 F). These results compare favorably to those obtained from composites made from amide-acid prepolymers capped with reactive alicyclic rings. Monomeric solutions provide excellent shelf life and improved solubility compared to amide-acid prepolymer solutions.
Improved thermally stable laminating resins were developed based on the addition-type pyrolytic polymerization. Detailed monomer and polymer synthesis and characterization studies identified formulations which facilitate press molding processing and autoclave fabrication of glass and graphite fiber reinforced composites. A specific resin formulation, termed P10P was utilized to prepare a Courtaulds HMS reinforced simulated airfoil demonstration part by an autoclave molding process.
High temperature resin matrices suitable for use in advanced graphite fiber composites for jet engine applications were evaluated. A series of planned, sequential screening experiments with resin systems in composite form were performed to reduce the number of candidates to a single A-type polyimide resin that repetitively produced void-free, high strength and modulus composites acceptable for use in the 550 F range for 1000 hours. An optimized processing procedure was established for this system. Extensive mechanical property studies characterized this single system, at room temperature, 500 F, 550 F and 600 F, for various exposure times.
Materials development topics include: development of analysis techniques to adjust heterogeneous data; determination of thermal conductivity for AISI 347 stainless steel and elastic moduli and Poisson's ratio for Inconel 718 and Ti 5Al-2.5Sn; embrittlement effects of 1400 psi gaseous hydrogen for alloy 718 and Ti 5Al-2.5Sn; cryogenic radiation damage of Ti 5Al-2.5Sn; and evaluation of prepreg, impregnation, and fabric materials for optimum fibrous graphite properties. Component support topics include: tensile design allowable development of Ti 5Al-2.5Sn for turbopump applications; evaluation of fatigue, fracture toughness, and stress corrosion properties of AA 7039-T63 for pressure vessel applications; development of AISI 347 sheet tensile and creep properties for nozzle applications; evaluation of orbital weld techniques for aluminum line fabrication; material selection of shield materials; development of high load friction and wear properties of hard chrome/gold plate combinations; and evaluation of weld processes for NASS duct coolant channel fabrication.