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At least 1,675 records · Page 93

Long-Wave Infrared Dyson Spectrometer

Preliminary results are presented for an ultra compact long-wave infrared slit spectrometer based on the dyson concentric design. The dyson spectrometer has been integrated in a dewar environment with a quantum well infrared photodetecor (QWIP), concave electron beam fabricated diffraction grating and ultra precision slit. The entire system is cooled to cryogenic temperatures to maximize signal to noise ratio performance, hence eliminating thermal signal from transmissive elements and internal stray light. All of this is done while maintaining QWIP thermal control. A general description is given of the spectrometer, alignment technique and predicated performance. The spectrometer has been designed for optimal performance with respect to smile and keystone distortion. A spectral calibration is performed with NIST traceable targets. A 2-point non-uniformity correction is performed with a precision blackbody source to provide radiometric accuracy. Preliminary laboratory results show excellent agreement with modeled noise equivalent delta temperature and detector linearity over a broad temperature range.

imaging↗

Venus Surface Power and Cooling System Design

A radioisotope power and cooling system is designed to provide electrical power for the a probe operating on the surface of Venus. Most foreseeable electronics devices and sensors simply cannot operate at the 450 C ambient surface temperature of Venus. Because the mission duration is substantially long and the use of thermal mass to maintain an operable temperature range is likely impractical, some type of active refrigeration may be required to keep certain components at a temperature below ambient. The fundamental cooling requirements are comprised of the cold sink temperature, the hot sink temperature, and the amount of heat to be removed. In this instance, it is anticipated that electronics would have a nominal operating temperature of 300 C. Due to the highly thermal convective nature of the high-density atmosphere, the hot sink temperature was assumed to be 50 C, which provided a 500 C temperature of the cooler's heat rejecter to the ambient atmosphere. The majority of the heat load on the cooler is from the high temperature ambient surface environment on Venus. Assuming 5 cm radial thickness of ceramic blanket insulation, the ambient heat load was estimated at approximately 77 watts. With an estimated quantity of 10 watts of heat generation from electronics and sensors, and to accommodate some level of uncertainty, the total heat load requirement was rounded up to an even 100 watts. For the radioisotope Stirling power converter configuration designed, the Sage model predicts a thermodynamic power output capacity of 478.1 watts, which slightly exceeds the required 469.1 watts. The hot sink temperature is 1200 C, and the cold sink temperature is 500 C. The required heat input is 1740 watts. This gives a thermodynamic efficiency of 27.48 %. The maximum theoretically obtainable efficiency is 47.52 %. It is estimated that the mechanical efficiency of the power converter design is on the order of 85 %, based on experimental measurements taken from 500 watt power class, laboratory-tested Stirling engines at GRC. The overall efficiency is calculated to be 23.36 %. The mass of the power converter is estimated at approximately 21.6 kg.

Landis, Geoffrey A.↗

Relaxation Dynamics of Zero-Field Skyrmions over a Wide Temperature Range

The promise of magnetic skyrmions in future spintronic devices hinges on their topologically enhanced stability and the ability to be manipulated by external fields. The technological advantages of nonvolatile zero-field skyrmion lattice (SkL) are significant if their stability and reliability can be demonstrated over a broad temperature range. Here in this paper, we study the relaxation dynamics including the evolution and lifetime of zero-field skyrmions generated from field cooling (FC) in an FeGe single-crystal plate via in situ Lorentz transmission electron microscopy (L-TEM). Three types of dynamic switching between zero-field skyrmions and stripes are identified and distinguished. Moreover, the generation and annihilation of these metastable skyrmions can be tailored during and after FC by varying the magnetic fields and the temperature. Finally, this dynamic relaxation behavior under the external fields provides a new understanding of zero-field skyrmions for their stability and reliability in spintronic applications and also raises new questions for theoretical models of skyrmion systems.

36 MATERIALS SCIENCE↗

Formation mechanism of superconducting phase and its three-dimensional architecture in pseudo-single-crystal K x Fe 2-y Se 2

Here, we report how the superconducting phase forms in pseudo-single-crystal K x Fe 2-y Se 2 . In situ scanning electron microscopy (SEM) observation reveals that, as an order-disorder transition occurs, on cooling, most of the high-temperature iron-vacancy-disordered phase gradually changes into the iron-vacancy-ordered phase whereas a small quantity of the high-temperature phase retains its structure and aggregates to the stripes with more iron concentration but less potassium concentration compared to the iron-vacancy-ordered phase. The stripes that are generally recognized as the superconducting phase are actually formed as a remnant of the high-temperature phase with a compositional change after an “imperfect” order-disorder transition. It should be emphasized that the phase separation in pseudo-single-crystal K x Fe 2-y Se 2 is caused by the iron-vacancy order-disorder transition. The shrinkage of the high-temperature phase and the expansion of the newly created iron-vacancy-ordered phase during the phase separation rule out the mechanism of spinodal decomposition proposed in an early report [Wang et al, Phys. Rev. B 91, 064513 (2015)]. Since the formation of the superconducting phase relies on the occurrence of the iron-vacancy order-disorder transition, it is impossible to synthesize a pure superconducting phase by a conventional solid state reaction or melt growth. By focused ion beam-scanning electron microscopy, we further demonstrate that the superconducting phase forms a contiguous three-dimensional architecture composed of parallelepipeds that have a coherent orientation relationship with the iron-vacancy-ordered phase.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Growth of GaAs crystals from the melt in a partially confined configuration

The experimental approach was directed along two main goals: (1) the implementation of an approach to melt growth in a partially confined configuration; and (2) the investigation of point defect interaction and electronic characteristics as related to thermal treatment following solidification and stoichiometry. Significant progress was made along both fronts. Crystal growth of GaAs in triangular ampuls was already carried out successfully and consistent with the model. In fact, pronounced surface tension phenomena which cannot be observed in ordinary confinement system were identified and should premit the assessment of Maragoni effects prior to space processing. Regarding thermal treatment, it was discovered that the rate of cooling from elevated temperatures is primarily responsible for a whole class of defect interactions affecting the electronic characteristics of GaAs and that stoichiometry plays a critical role in the quality of GaAs.

Gatos, Harry C.↗

Analysis of the NorthStar Inconel 718 Window

NorthStar Medical Radioisotopes, LLC, is planning to produce the important medical radioisotope molybdenum-99 (Mo-99) through photonuclear reactions in molybdenum-100 (Mo-100). In this approach, a target comprising multiple thin disks of enriched molybdenum metal will be bombarded with a 40-MeV electron beam. Because enriched Mo-100 is expensive, there is a desire to utilize as much beam power as possible to achieve maximum production yield and minimize the size of the target. This requirement leads to very high beam power density (heat deposition in the target), which sets challenging requirements for cooling of the target. In the latest concept developed by NorthStar, a stack of target (sintered molybdenum) disks is irradiated from two sides by a 40-MeV electron beam, with a total power of 240 kW (120 kW from each side). As shown in Figure 1, the target disks are cooled by pressurized helium gas flowing through channels between the disks. A housing encloses the target disks and helium coolant. Thinned regions on opposite sides of the housing act as windows, forming the pressure boundary between the helium within the housing and the evacuated beam tube. A pulsed (50-Hz) 40-MeV electron beam is used, with 120 kW total power and a 10% duty cycle. The pulsing beam creates a corresponding cyclic thermal load within the window material. To examine the effects of the cyclic thermal load on the window, a combination of analyses was performed, including computational fluid dynamics (CFD) and finite element analysis (FEA). The analyses presented in this report were primarily performed using the finite element method. However, because of the curved surface of the window, CFD analysis was used to calculate the convective cooling boundary included in the FEA model. Transient thermal and structural models were used to explore the window geometry, including thickness, radius of curvature, and diameter, while staying within the temperature and stress limits of the material as well as maintaining mechanical stability (i.e., avoiding buckling). Additionally, variations in the size and location of the electron beam were evaluated. Multiple parameters for the window and the electron beam were examined throughout the analysis. Upper and lower bounds were established for the window geometry parameters, and limitations were established for the size and position of the electron beam.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

Unconventional slowing down of electronic recovery in photoexcited charge-ordered La1/3Sr2/3FeO3

We report the coupled slowing down of electronic and structural dynamics in a charge-ordered antiferromagnetic insulating oxide directly measured in the time domain. Following optical excitation, the recovery time of both transient optical reflectivity and x-ray diffraction intensity from a charge-ordered superstructure in a La1/3Sr2/3FeO3 thin film increases by orders of magnitude when the sample temperature approaches the phase transition temperature. The recovery time becomes much longer than the independently measured lattice cooling time, indicating a nonthermal origin of the slowing down. The combined experimental and theoretical investigations show that the slowing down of electronic recovery corresponds to the pseudo-critical dynamics that originates from magnetic interactions close to a weakly first-order phase transition.

Zhu, Yi↗

Beam Physics of Integrable Optics Test Accelerator at Fermilab

Fermilab's Integrable Optics Test Accelerator (IOTA) is an electron storage ring designed for testing advanced accelerator physics concepts, including implementation of nonlinear integrable beam optics and experiments on optical stochastic cooling. The machine is currently under construction at the Advanced Superconducting Test Accelerator facility. In this report we present the goals and the current status of the project, and describe the details of machine design. In particular, we concentrate on numerical simulations setting the requirements on the design and supporting the choice of machine parameters.

43 PARTICLE ACCELERATORS↗

Isothermal annealing behaviour of nuclear grade 20Cr-25Ni austenitic stainless steel

Highlights: • At 930 °C recrystallisation of deformed 20/25 Nb steel is completed after 120 s. • Recrystallisation proceeds by strain induced boundary migration. • An increase of cube oriented grains at the expense of S oriented is observed. • The boundary migration induced the precipitation of niobium carbides. • The grain size is limited by the particle dispersion according to Zener pinning. - Abstract: We have performed an in-depth characterisation of the microstructure evolution of 20Cr-25Ni Nb-stabilised austenitic stainless steel during isothermal annealing at 930 °C using scanning and transmission electron microscopy. This steel grade is used as cladding material in advanced gas-cooled fission reactors, due to its resistance to thermal creep and water corrosion. The initial deformed microstructure undergoes recrystallisation via a strain-induced boundary migration mechanism, attaining a fully recrystallised microstructure after 120 s of annealing. The transition from low-to-high grain boundaries has already occurred after 15 s, together with an increase in the cube grain orientation at the expense of the S texture component. After 120 s, the grain boundary migration induces the formation of new fine Nb(C,N) particles, whereas the pre-existing particles become enriched in Ni and Si. The resulting particle population limits the grain growth in the austenitic matrix, based on the Zener pinning model, resulting in relatively small recrystallised austenite grains and a high density of high-angle and special coincidence-lattice-site grain boundaries, together with a large number of particle/matrix interfaces.

36 MATERIALS SCIENCE↗

Hypermetallic polar molecules for precision measurements

Laser cooling is a powerful method to control molecules for applications in precision measurement, as well as quantum information, many-body physics, and fundamental chemistry. However, many optically-active metal centers in valence states which are promising for these applications, especially precision measurement, are difficult to laser cool. In order to extend the control afforded by laser cooling to a wider array of promising atoms, we consider the use of small, hypermetallic molecules that contain multiple metal centers. We provide a detailed analysis of YbCCCa and YbCCAl as prototypical examples with different spin multiplicities, and consider their feasibility for precision measurements making use of the heavy Yb atom. We find that these molecules are linear and feature metal-centered valence electrons, and study the complex hybridization and spin structures that are relevant to photon cycling and laser cooling. Our findings suggest that this hypermetallic approach may be a versatile tool for experimental control of metal species that do not otherwise efficiently cycle photons, and could present a new polyatomic platform for state-of-the-art precision measurements.

74 ATOMIC AND MOLECULAR PHYSICS↗

X-RAYS FROM SUPERNOVA SHOCKS IN DENSE MASS LOSS

Type IIn and related supernovae show evidence for an interaction with a dense circumstellar medium that produces most of the supernova luminosity. X-ray emission from shock heated gas is crucial for the energetics of the interaction and can provide diagnostics on the shock interaction. Provided that the shock is at an optical depth {tau}{sub w} {approx}< c/v{sub s} in the wind, where c is the speed of light and v{sub s} is the shock velocity, a viscous shock is expected that heats the gas to a high temperature. For {tau}{sub w} {approx}> 1, the shock wave is in the cooling regime; inverse Compton cooling dominates bremsstrahlung at higher densities and shock velocities. Although {tau}{sub w} {approx}> 1, the optical depth through the emission zone is {approx}< 1 so that inverse Compton effects do not give rise to significant X-ray emission. The electrons may not reach energy equipartition with the protons at higher shock velocities. As X-rays move out through the cool wind, the higher energy photons are lost to Compton degradation. If bremsstrahlung dominates the cooling and Compton losses are small, the energetic radiation can completely photoionize the preshock gas. However, inverse Compton cooling in the hot region and Compton degradation in the wind reduce the ionizing flux, so that complete photoionization is not obtained and photoabsorption by the wind further reduces the escaping X-ray flux. We conjecture that the combination of these effects led to the low observed X-ray flux from the optically luminous SN 2006gy.

79 ASTRONOMY AND ASTROPHYSICS↗

Gamma-Ray Spectra and Variability of Cygnus Z-1 Observed by BATSE

We present new BATSE earth occultation observations of the 25 keV-1.8 MeV spectrum and variability of Cygnus X-1 made between August 1993 and May 1994. We observed that the normal soft gamma ray spectrum (gamma2) of Cygnus X-1 has two components: a Comptonized part seen below 300 keV, and a high-energy tail in the 0.3 - 2 MeV range. We interpret it in terms of a two-layer region, consisting of a high-energy core (with an equivalent electron temperature of approximately 210-250 keV) near the event horizon, embedded in an about 50 keV corona. In this scenario, the observed 25-300 keV photons were produced by Compton scattering of soft photons (about 0.5 keV) by the hot electrons in the outer corona. These same hard x rays were further up-scattered by a population of energetic electrons in the inner core, producing the spectral tail above 300 keV. Cygnus X-1 went through an extended sequence of transitions between August 1993 and May 1994, when the 45-140 keV flux first decreased steadily from approximately gamma2 to roughly one-quarter of its intensity over a period of about 140 days. The flux remained at this low level for about 40 days before returning, swiftly (approximately 20 days) to approximately the initial gamma2 level. During the transition, the spectrum evolved to a shape consistent with either a power law with photon index of about 2.6 or a single temperature Compton model with electron temperature kT = 110 +/- 11 keV, and optical depth t = 0.40 +/- 0.06, and then returned essentially to the original gamma2 spectrum at the end of the active period. The overall cooling of the system during the low flux period may be due to an increase in the soft photon population which effectively quenched the hot electrons in these regions through Compton scattering.

Ling, J. C.↗

Dynamically polarized target for the g p 2 and G p E experiments at Jefferson Lab

We describe a dynamically polarized target that has been utilized for two electron scattering experiments in Hall A at Jefferson Lab. The primary components of the target are a new, high cooling power 4 He evaporation refrigerator, and a re-purposed, superconducting split-coil magnet. It has been used to polarize protons in irradiated NH 3 at a temperature of 1 K and at fields of 2.5 and 5.0 Tesla. The performance of the target material in the electron beam under these conditions will be discussed. The maximum polarizations of 28% and 95% were obtained at those fields, respectively. To satisfy the requirements of both experiments, the magnet had to be routinely rotated between angles of 0, 6, and 90 degrees with respect to the incident electron beam. This was accomplished using a new rotating vacuum seal which permits rotations to be performed in only a few minutes.

43 PARTICLE ACCELERATORS↗

Next Generation Robust Polarization Photocathodes for EIC

Cornell group developed and characterized robust photocathodes dedicated to generation of spin-polarized electrons by employing a thin protective activation layer of a robust material in place of the conventional cesiation, which is extremely prone to the damage by ions and chemical poisoning. Various thicknesses of Cs2Te and of other materials on III-V semiconductors were studied to understand their effect on the cathode longevity and the polarization state. These photocathodes, as well as new alternative materials, will be eventually tested with high beam current for their operational (lifetime) performance in the Cornell HV DC guns, including a brand- new photoemission high voltage gun that features a cryogenically cooled photocathode holder. The research conducted opens a new and robust way to reach the negative electron affinity for a large class of photocathodes specifically designed to maximize their accelerator performance. It particular, it benefits the future EIC by improving the lifetime available from spin-polarized electron photoemission sources.

43 PARTICLE ACCELERATORS↗

Power Electronics Thermal Management

Thermal modeling was conducted to evaluate and develop thermal management strategies for high-temperature wide-bandgap (WBG)-based power electronics systems. WBG device temperatures of 175 degrees C to 250 degrees C were modeled under various under-hood temperature environments. Modeling result were used to identify the most effective capacitor cooling strategies under high device temperature conditions.

30 DIRECT ENERGY CONVERSION↗

Effect of alloying elements, cold work, and hydrogen on the irradiation-induced growth behavior of zirconium alloy variants - 2016-0040

In-reactor dimensional changes in zirconium-based alloys result from a complex interplay of many factors, such as (1) alloy type and composition, including the addition of elements such as niobium, iron, and tin; (2) fabrication process, including cold work, texture, and residual stresses; (3) irradiation temperature; and (4) hydrogen levels. In many cases, the observed dimensional changes in light water reactor fuel-assembly components-especially at high exposures-cannot be fully explained based on current growth and creep models. Therefore, a systematic approach was taken in this multi-year (2005-2011) Nuclear Fuel Industry Research Program investigation. The objective was to measure stress-free irradiation-induced growth (IIG) of specially fabricated alloys through irradiation under controlled conditions in the BOR-60 fast-flux test reactor up to a high fluence of approximately 2X10{sup 26} m{sup -2} (E>1 MeV)-equivalent to maximum of approximately 37 dpa exposure-followed by postirradiation examinations (PIEs). Irradiation temperature was within a narrow temperature range (320±10 deg. C). The PIEs included dimensional-change and microhardness measurements, metallography and hydride etching, and scanning transmission electron microscopy (STEM) or transmission electron microscopy (TEM). All irradiation samples (typically flat rectangular coupons or curvilinear cutouts of cladding tubes sized 35 by 6.5 by 0.8 mm) were pre-filmed to avoid the uptake of impurity hydrogen from sodium-cooled BOR-60. A wide variety of samples representing standard LWR cladding alloys with and without pre-hydriding (approximately 116 to approximately 718 ppm) as well as special compositions with iron contents (100 to 4,000 ppm) were irradiated. The irradiation in BOR-60 was done in five different stages (eight micro-cycles) and lasted approximately 18 months with interim and final growth measurements made using a high precision-length measurement device. Results of the extensive investigation include: significant effects of Fe, Nb, and hydrogen additions; quantification of growth rates from low to very high fluences (dpas); measurement of volume changes; and correlation of growth with -component dislocation densities. (authors)

36 MATERIALS SCIENCE↗

Integrated Pump Assembly - An Active Cooling System for Mars Pathfinder Thermal Control

The Mars Pathfinder spacecraft which will be launched in December 1996 features an active cooling system for controlling the temperature of the spacecraft. This will be the first time that such a mechanical pump cooling system is used on an interplanetary or long duration flight (over two weeks) in space. The major element of the cooling system is the Integrated Pump Assembly (IPA). It uses centrifugal pumps to circulate liquid Freon to transfer heat from spacecraft electronics to an external radiator. This paper describes the design, fabrication, assembly, and testing of the IPA.

cooling↗

A Cooling System for the EAPU Shuttle Upgrade

The Shuttle orbiter currently uses hydrazine-powered APU's for powering its hydraulic system pumps. To enhance vehicle safety and reliability, NASA is pursuing an APU upgrade where the hydrazine powered turbine is replaced by an electric motor pump and battery power supply. This EAPU (Electric APU) upgrade presents several thermal control challenges most notably the new requirement for moderate temperature control of high-power electron ics at 132 of (55.6 C). This paper describes how the existing Water Spray Boiler (WSB), which currently cools the hydraulic fluid and APU lubrication oil, is being modified to provide EAPU thermal management.

Tongue, Stephen↗