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NASA NTRS1991

Effect of fiber reinforcements on thermo-oxidative stability and mechanical properties of polymer matrix composites

A number of studies have investigated the thermo-oxidative behavior of polymer matrix composites. Two significant observations have been made from these research efforts: (1) fiber reinforcement has a significant effect on composite thermal stability; and (2) geometric effects must be considered when evaluating thermal aging data. A compilation of some results from these studies is presented, and this information shows the influence of the reinforcement fibers on the oxidative degradation of various polymer matrix composites. The polyimide PMR-15 was the matrix material that was used in these studies. The control composite material was reinforced with Celion 6000 graphite fiber. T-40R graphite fibers, along with some very stable ceramic fibers were selected as reinforcing fibers because of their high thermal stability. The ceramic fibers were Nicalon (silicon carbide) and Nextel 312 (alumina-silica-boron oxide). The mechanical properties of the two graphite fiber composites were significantly different, probably owing to variations in interfacial bonding between the fibers and the polyimide matrix. The Celion 6000/PMR-15 bond is very tight but the T-40/PMR-15 bond is less tight. Three oxidation mechanisms were observed: (1) the preferential oxidation of the Celion 6000 fiber ends at cut surfaces, leaving a surface of matrix material with holes where the fiber ends were originally situated; (2) preferential oxidation of the composite matrix; and (3) interfacial degradation by oxidation. The latter two mechanisms were also observed on fiber end cut surfaces. The fiber and interface attacks appeared to initiate interfiber cracking along these surfaces.

Bowles, Kenneth J.↗

NASA NTRS1989

The effect of hydrogen on the deformation behavior of a single crystal nickel-base superalloy

The effect of hydrogen on the tensile deformation behavior of PWA 1480 is presented. Tensile tests were interrupted at different plastic strain levels to observe the development of the dislocation structure. Transmission electron microscopy (TEM) foils were cut perpendicular to the tensile axis to allow the deformation of both phases to be simultaneously observed as well as parallel to zone axes (III) to show the superdislocations on their slip planes. Similar to other nickel-base superalloys, hydrogen was detrimental to the room temperature tensile properties of PWA 1480. There was little effect on strength, however the material was severely embrittled. Even without hydrogen, the elongation-to-failure was only approximately 3 percent. The tensile fracture surface was made up primarily of ductile voids with regions of cleavage fracture. These cleavage facets are the eutectic (gamma') in the microstructure. It was shown by quantitative fractography that hydrogen embrittles the eutectic (gamma') and causes the crack path to seek out and fracture through the eutectic (gamma'). There was two to three times the amount of cleavage on the fracture surface of the hydrogen-charged samples than on the surface of the uncharged samples. The effect of hydrogen can also be seen in the dislocation structure. There is a marked tendency for dislocation trapping in the gamma matrix with and without hydrogen at all plastic strain levels. Without hydrogen there is a high dislocation density in the gamma matrix leading to strain exhaustion in this region and failure through the matrix. The dislocation structure at failure with hydrogen is slightly different. The TEM foils cut parallel to zone axes (III) showed dislocations wrapping around gamma precipitates. Zone axes (001) foils show that there is a lower dislocation density in the gamma matrix which can be linked to the effects of hydrogen on the fracture behavior. The primary activity in the gamma precipitates is in the form of superlattice intrinsic stacking faults (SISFs). These faults have also been reported in other ordered alloys and superalloys.

Walston, W. S.↗

NASA NTRS1989

Minimum length Pb/SCIN detector for efficient cosmic ray identification

A study was made of the performance of a minimal length cosmic ray shower detector that would be light enough for space flight and would provide efficient identification of positions and protons. Cosmic ray positions are mainly produced in the decay chain of: Pion yields Muon yields Positron and they provide a measure of the matter density traversed by primary protons. Present positron flux measurements are consistent with the Leaky Box and Halo models for sources of cosmic rays. Abundant protons in the space environment are a significant source of background that would wash out the positron signal. Protons and positrons produced very distictive showers of particles when they enter matter; many studies have been published on their behavior on large calorimeter detectors. The challenge is to determine the minimal material necessary (minimal calorimeter depth) for positive particles identification. The primary instrument for the investigation is the Monte Carlo code GEANT, a library of programs from CERN that can be used to model experimental geometry, detector responses and particle interaction processes. The use of the Monte Carlo approach is crucial since statistical fluctuations in shower shape are significant. Studies conducted during the 1988 summer program showed that straightforward approaches to the problem achieved 85 to 90 percent correct identification, but left a residue of 10 to 15 percent misidentified particles. This percentage improved to a few percent when multiple shower-cut criteria were applied to the data. This summer, the same study was extended to employ several physical and statistical methods of identifying response of the calorimeter and the efficiency of the optimal shower cuts to off-normal incidence particle was determined.

Snyder, H. David↗

NASA NTRS1989

Dielectric image-resonator multiplexer

A two, three or four channel multiplexer can be operated in the TE 01δ or HE 11δ modes, each channel of the multiplexer has one bandpass filter, with each filter usually having a plurality of cavities. One cavity of each filter is a common cavity with all of the other filters of the multiplexer. The common cavity contains one independent dielectric quarter-cut or half-cut image resonator for each filter representing a channel- of the multiplexer. Each resonator is mounted on a suitable support the common cavity provides a common junction and contains a loop coupling to couple electromagnetic energy between the various· channels. The multiplexer has at least one input and at least one output. Previous microwave multiplexers have a plurality of bandpass filters arranged on a coaxial manifold. With the multiplexer of the present invention, the manifold can be eliminated. Further, at the S-band or L-band, substantial weight and volume savings can be achieved using the multiplexer of the present invention without sacrificing performance. This can be very important for space applications.

Wai-Cheung Tang↗

NASA NTRS1990

CO2 lasers and applications II; Proceedings of the Third European Congress on Optics, The Hague, Netherlands, Mar. 12-14, 1990

Recent advances in CO2 laser technology and its applications are examined. Topics discussed include the excitation of CO2 lasers by microwave discharge, a compact RF-excited 12-kW CO2 laser, a robotic laser for three-dimensional cutting and welding, three-dimensional CO2-laser material processing with gantry machine systems, and a comparison of hollow metallic waveguides and optical fibers for transmitting CO2-laser radiation. Consideration is given to an aerodynamic window with a pump cavity and a supersonic jet, cutting and welding Al using a high-repetition-rate pulsed CO2 laser, speckle reduction in CO2 heterodyne laser radar systems, high-power-laser float-zone crystal growth, melt dynamics in surface processing with laser radiation, laser hardfacing, surface melting of AlSi10Mg with CO2 laser radiation, material processing with Cu-vapor lasers, light-induced flow at a metal surface, and absorption measurements in high-power CW CO2-laser processing of materials.

Opower, Hans↗

NASA NTRS1990

Defect sensitivity of filament-wound structures in compression

Compression testing of 12-ply graphite/bismaleimide laminated plates with induced and natural defects is discussed, and emphasis is placed on resultant changes in strength and stiffness. Ply drops, ply cuts, and fiber crossovers are studied by comparison with a quasi-isotropic control group. It is observed that, as expected, failure initiates at the defects and progresses via delamination, sublaminate buckling, angle-ply cracking, and longitudinal ply failure. The ultimate stress is reduced by approximately 40 percent for all types of defects except the unsymmetrical cut-ply specimens which averages a 54-percent reduction. The average stiffness reduction of 10 percent is observed for specimens with induced defects. Fiber crossovers are found to reduce the laminate strength and stiffness significantly.

Jensen, David W.↗

NASA NTRS1991

Procedure for computer-controlled milling of accurate surfaces of revolution for millimeter and far-infrared mirrors

A simple method for milling accurate off-axis parabolic mirrors with a computer-controlled milling machine is discussed. For machines with a built-in circle-cutting routine, an exact paraboloid can be milled with few computer commands and without the use of the spherical or linear approximations. The proposed method can be adapted easily to cut off-axis sections of elliptical or spherical mirrors.

Emmons, Louisa↗

NASA NTRS1992

Precise Countersinking Tool

Tool countersinks holes precisely with only portable drill; does not require costly machine tool. Replaceable pilot stub aligns axis of tool with centerline of hole. Ensures precise cut even with imprecise drill. Designed for relatively low cutting speeds.

Jenkins, Eric S.↗

NASA NTRS1991

Studies of the charging of a thin dust layer in a plasma

The present study is designed to extend Wilson's model to include refinements in the actual operational design of the simulation code itself and to include additional physics in order to assess the resulting electric field structure and grain charges. Most of the initial phases of the work have focussed on the fact that the code, though in principle reliable, suffers from severe time constraints, requiring as must as 10-50 hours of CPU time for typical runs on a VAX computer. It is likely that by staging the code into steps in which early steps are carried out crudely and later steps successively fine tuned the total CPU time can be cut significantly. Preliminary results indicate the possibility to cut CPU time to as much as 1/3 or 1/5 the former time. The original Wilson code has been carefully examined, tested and documented. Shortcuts and staging systems have been introduced and tested which should make the code produce more accurate results with a finer grid system than would have been feasible heretofor. Continued testing and implementation of these refinements will be carried out at the author's home institution in the near future. In addition to the effort at reducing CPU time to a manageable amount, work is in progress to include a dust-size distribution instead of assuming all dust grains have the same size.

Peterson, Lennart R.↗

NASA NTRS1992

Effect of fiber reinforcement on thermo-oxidative stability and mechanical properties of polymer matrix composites

A number of studies have investigated the thermooxidative behavior of polymer matrix composites. Two significant observations have been made from these research efforts: (1) fiber reinforcement has a significant effect on composite thermal stability; and (2) geometric effects must be considered when evaluating thermal aging data. The polyimide PMR-15 was the matrix material used in these studies. The control composite material was reinforced with Celion 6000 graphite fiber. T-4OR graphite fibers, along with some very stable ceramic fibers were selected as reinforcing fibers because of their high thermal stability. The ceramic fibers were Nicalon (silicon carbide) and Nextel 312 (alumina-silica-boron oxide). The mechanical properties of the two graphite fiber composites were significantly different, probably owing to variations in interfacial bonding between the fibers and the polyimide matrix. Three oxidation mechanisms were observed: (1) the preferential oxidation of the Celion 6000 fiber ends at cut surfaces, leaving a surface of matrix material with holes where the fiber ends were originally situated; (2) preferential oxidation of the composite matrix; and (3) interfacial degradation by oxidation. The latter two mechanisms were also observed on fiber end cut surfaces. The fiber and interface attacks appeared to initiate interfiber cracking along these surfaces.

Bowles, K. J.↗

NASA NTRS1992

Automatic translation of digraph to fault-tree models

The author presents a technique for converting digraph models, including those models containing cycles, to a fault-tree format. A computer program which automatically performs this translation using an object-oriented representation of the models has been developed. The fault-trees resulting from translations can be used for fault-tree analysis and diagnosis. Programs to calculate fault-tree and digraph cut sets and perform diagnosis with fault-tree models have also been developed. The digraph to fault-tree translation system has been successfully tested on several digraphs of varying size and complexity. Details of some representative translation problems are presented. Most of the computation performed by the program is dedicated to finding minimal cut sets for digraph nodes in order to break cycles in the digraph. Fault-trees produced by the translator have been successfully used with NASA's Fault-Tree Diagnosis System (FTDS) to produce automated diagnostic systems.

Iverson, David L.↗

NASA NTRS1993

Electrical-Discharge Machining Of Curved Passages

Electrical-discharge machining (EDM) used to cut deep hole with bends. EDM process done with articulating segmented electrode. Originally straight, electrode curved as it penetrates part, forming long, smoothly curving hole. After hole cut, honed with slurry to remove thin layer of recast metal created by EDM. Breakage of tools, hand deburring, and drilling debris eliminated.

Guirguis, Kamal S.↗

NASA NTRS1992

Acoustic Mode Measurements in the Inlet of a Model Turbofan Using a Continuously Rotating Rake

Comprehensive measurements of the spinning acoustic mode structure in the inlet of the Advanced Ducted Propeller (ADP) have been completed. These measurements were taken using a unique and previously untried method which was first proposed by T.G. Sofrin. A continuously rotating microphone system was employed. The ADP model was designed and built by Pratt & Whitney and tested in the NASA Lewis 9- by 15-foot Anechoic Wind Tunnel. Three inlet configurations were tested with cut-on and cutoff stator vane sets. The cutoff stator was designed to suppress all modes at the blade passing frequency. Rotating rake measurements indicate that several extraneous circumferential modes were active. The mode orders suggest that their source was an interaction between the rotor and small interruptions in the casing tip treatment. The cut-on stator produced the expected circumferential modes plus higher levels of the unexpected modes seen with the cutoff stator.

Heidelberg, Laurence J.↗

NASA NTRS1992

An interferometer having fused optical fibers, and apparatus and method using the interferometer

An interferometer includes a first optical fiber coupled to a second optical fiber by fusing. At a fused portion, the first and second optical fibers are cut to expose respective cores. The cut or fused end of the first and second optical fibers is arranged to oppose a diaphragm or surface against which a physical phenomenon such as pressure or stress, is applied. In a first embodiment, a source light which is generally single-mode monochromatic, coherent light, is input to the first optical fiber and by evanescence, effectively crosses to the second optical fiber at the fused portion. Source light from the second optical fiber is reflected by the diaphragm or surface, and received at the second optical fiber to generate an output light which has an intensity which depends upon interference of reference light based on the source light, and the reflected light reflected from the diaphragm or surface. The intensity of the output light represents a positional relationship or displacement between the interferometer and the diaphragm or surface.

Hellbaum, Richard F.↗

NASA NTRS1993

Acoustic mode measurements in the inlet of a model turbofan using a continuously rotating rake

Heidelberg, Laurence J.↗

NASA NTRS1946

Correlation between strength properties in standard test specimens and molded phenolic parts

This report describes an investigation of the tensile, flexural, and impact properties of 10 selected types of phenolic molding materials. The materials were studied to see in what ways and to what extent their properties satisfy some assumptions on which the theory of strength of materials is based: namely, (a) isotropy, (b) linear stress-strain relationship for small strains, and (c) homogeneity. The effect of changing the dimensions of tensile and flexural specimens and the span-depth ratio in flexural tests were studied. The strengths of molded boxes and flexural specimens cut from the boxes were compared with results of tests on standard test specimens molded from the respective materials. The nonuniformity of a material, which is indicated by the coefficient of variation, affects the results of tests made with specimens of different sizes and tests with different methods of loading. The strength values were found to depend on the relationship between size and shape of the molded specimen and size and shape of the fillers. The most significant variations observed within a diversified group of materials were found to depend on the orientation of fibrous fillers. Of secondary importance was the dependence of the variability of test results on the pieces of filler incorporated into the molding powder as well as on the size of the piece. Static breaking strength tests on boxes molded from six representative phenolic materials correlated well with falling-ball impact tests on specimens cut from molded flat sheets. Good correlation was obtained with Izod impact tests on standard test specimens prepared from the molding materials. The static breaking strengths of the boxes do not correlate with the results of tensile or flexural tests on standard specimens.

MATERIALS, MONSANTO RESINOX↗

NASA NTRS1931

The N.A.C.A. Apparatus for Studying the Formation and Combustion of Fuel Sprays and the Results from Preliminary Tests

Described here is an apparatus for studying the formation and combustion of fuel sprays under conditions closely simulating those in a high speed compression-ignition engine. The apparatus consists of a single-cylinder modified test engine, a fuel injection system so designed that a single charge of fuel can be injected into the combustion chamber, an electric driving motor, and a high-speed photographic apparatus. The cylinder head of the engine has a vertical disk form of combustion chamber whose sides are glass windows. When the fuel is injected into the combustion chamber, motion pictures at the rate of 2000 per second are taken of the spray formation by means of spark discharges. When combustion takes place, the light of combustion is recorded on the same photographic film as the spray photographs. Included here are the results of some tests to determine the effect of air temperature, air flow, and nozzle design on the spray formation. The results show that the compression temperature has little effect on the penetration of the fuel spray, but does not affect the dispersion, that air velocities of about 300 feet per second are necessary to destroy the core of the spray, and that the effect of air flow on the spray is controlled to a certain extent by the design of the injection nozzle. The results on the combustion of the spray show that when ignition does not take place until after spray cut-off, the ignition may start almost simultaneously throughout the combustion chamber or at different points throughout the chamber. When ignition takes place before spray cut-off, the combustion starts around the edge of the spray and then spreads throughout the chamber.

Rothrock, A M↗

NASA NTRS1940

The Lateral Stability of Equal-flanged Aluminum-alloy I-beams Subjected to Pure Bending

Equal-flange beams of a special extruded I-section of 27ST aluminum alloy were tested in pure bending. Complete end fixity was not attained. Loading was continued until a definite maximum value had been reached. Tensile tests were made on specimens cut from the flanges and the web of each beam. Compressive stress-strain characteristics were determined by pack compression tests on specimens cut from the flanges. Values computed from an equation previously suggested by one of the authors for the critical stress at which such beams become unstable were found to be in good agreement with values computed from experimentally determined critically bending moments.

Dumont, C↗