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At least 1,639 records · Page 91
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

In situ synchrotron diffraction of pressure-induced phase transition in DyPO 4 under variable hydrostaticity

In situ synchrotron x-ray diffraction was conducted on polycrystalline DyPO 4 to elucidate the details of the pressure-induced transition from the xenotime polymorph to the monazite polymorph. We used three different pressure-transmitting media (neon, a 16:3:1 methanol-ethanol-water mixture, and potassium chloride) to investigate the effect of hydrostaticity on the phase behavior. Specifically, our data clearly show a hydrostatic onset pressure of the xenotime-monazite transition of 9.1 GPa, considerably lower than the 15.3 GPa previously determined by Raman spectroscopy. Based on (quasi)hydrostatic data taken in a neon environment, third-order Birch-Murnaghan equation-of-state fits give a xenotime bulk modulus of 144 GPa and a monazite bulk modulus of 180 GPa (both with pressure derivatives of 4.0). Structural data and axial compressibilities show that DyPO 4 is sensitive to shear and has an anisotropic response to pressure. More highly deviatoric conditions cause the onset of the transition to shift to pressures at least as low as 7.0 GPa. We attribute early transition to shear-induced distortion of the PO4 tetrahedra. Finally, our characterization of the high-pressure behavior of DyPO 4 under variable hydrostaticity is critical for advancing rare earth orthophosphate fiber coating applications in ceramic matrix composites and may inform future tailoring of phase composition for controlled shear and pressure applications.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2020

Report on partially complete post-irradiation-examination of the INL samples

Ferritic-martensitic steels (NF616 and T91), and austenitic stainless steel 800H and its Grain Boundary Engineering (GBE)-treated version 800H-TMP (ThermoMechanical Processing) were irradiated in the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) and their microstructures and mechanical properties were characterized. Ferritic-martensitic steels were irradiated up to 8.16 dpa in the irradiation temperatures ranging from 241 °C to 447.5 °C. Selected 800H and 800H-TMP samples were also irradiated up to 9.12 dpa at 359°C to 431°C. Vickers hardness measurement, fractography, and microstructural characterization were performed on the selected samples in the LAMDA lab. Radiation-induced hardening of NF616 and T91 was observed in the hardness measurements which show ~37% to ~65% increases, depending on irradiation dose and irradiation temperature. Within the irradiation conditions studied in this work, samples with a higher dose had a higher hardness. All the tested alloy 800H and 800H-TMP in this work showed irradiation-hardening by ~96±7% to ~152±10%. Alloy 800HTMP tended to have slightly smaller irradiation-hardening than alloy 800H. The fractography of NF616 samples D2 (2.96 dpa at 291.5°C), D4 (5.91 dpa at 359°C), and D6 (8.16 dpa at 431°C) indicated loss of ductility with negligible necking for the sample D2, yet obvious ductile failure for samples D4 and D6. Fractography of alloy 800H samples N4 (7.27 dpa at 359°C), N5 (3.9 dpa at 451.5°C), and N6 (9.01 dpa at 431°C), and alloy 800H-TMP samples P4 (7.36 dpa at 359°C), P5 (3.95 dpa at 451.5°C), and P6 (9.12 dpa at 431°C) indicated that all samples failed in a ductile mode, with obvious necking. Dimples were observed where large Ti-containing particles were observed for the samples. TEM characterization was performed on alloy 800H (N4, N5, N6) and 800H-TMP (P4, P5 and P6). Accumulation of M23C6 precipitates at grain boundaries was observed in all samples, and the presence of Ti(C,N) precipitates at grain boundaries and in the matrix was observed in alloy 800H-TMP. M23C6 precipitates were found to have the cube-on-cube orientation relationship with the matrix. In addition, nanoscale Si-rich clusters were observed in the matrix of all samples. Atom probe tomography was conducted on the same samples, and their results are being analyzed to be integrated with the TEM results for a confident description of the clustering behavior. Due to the low irradiation temperature (up to 451.5°C), dislocation loops formed in all samples, with the density and the average size of dislocation loops in the order of 1022 – 1023 m-3 and 11.7 – 15.9 nm, respectively. The loop densities in alloy 800H were higher than that in alloy 800H-TMP under the same irradiation conditions. Further systematic data analyses, together with some complementary experiments, will be pursued for these samples to foster peer-reviewed journal article publications.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2021

Leveraging Spin-Orbit Coupling in Ge/SiGe Heterostructures for Quantum Information Transfer

Hole spin qubits confined to lithographically - defined lateral quantum dots in Ge/SiGe heterostructures show great promise. On reason for this is the intrinsic spin - orbit coupling that allows all - electric control of the qubit. That same feature can be exploited as a coupling mechanism to coherently link spin qubits to a photon field in a superconducting resonator, which could, in principle, be used as a quantum bus to distribute quantum information. The work reported here advances the knowledge and technology required for such a demonstration. We discuss the device fabrication and characterization of different quantum dot designs and the demonstration of single hole occupation in multiple devices. Superconductor resonators fabricated using an outside vendor were found to have adequate performance and a path toward flip-chip integration with quantum devices is discussed. The results of an optical study exploring aspects of using implanted Ga as quantum memory in a Ge system are presented.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2022

2022 AI Testbed Expeditions Report

By exploiting the coherent properties of a light source, coherent diffraction imaging (CDI) is able to obtain the sample image at a nanoscale resolution using the measured diffraction pattern. Bragg Coherent Diffraction Imaging (BCDI) has become valuable for recovering the displacement and strain field of crystals, providing a valuable tool in material science and solid-state physics. X-ray ptychography is another emerging CDI technique that can produce a high-resolution image of the extended sample and has become popular in many research areas (e.g., materials science, biology, electronics, and optics characterization). CDI including BCDI and ptychography has become an established technique in Synchrotron Facilities including the Advanced Photon Source (APS) and will greatly benefit from the 100x coherent flux increase of the upcoming APS Upgrade (APSU). The current image formation process in CDI employs iterative phase retrieval algorithms, which is a time-consuming and computationally expensive process. Especially after APSU, the traditional iterative methods will not be able to match the experimental data acquisition speed. We employ deep learning (DL) approach to replace the iterative approaches, therefore allowing hundreds of times faster recovery of the object. We developed AutoPhaseNN, a DL-based approach which learns to solve the inverse problem without labeled data. Taking 3D BCDI as a representative technique, AutoPhaseNN has been demonstrated to be one hundred times faster than traditional iterative phase retrieval methods while providing comparable image quality. The current network is trained with 64 x 64 x 64 data size, to achieve higher resolution imaging, we will need to scale the network to input and train/infer 3D arrays of size 256 x 256 x 256 (today) and of size 2560x2560x2560 (APSU). However, the scalability of the network is restricted due to the memory-intensive training process. To perform the training for a 256 x 256 x 256 data size, the required memory exceeds the capacity of the current machine. In this project, we explore using Sambanova system to train the network for the direct data inversion for CDI.

36 MATERIALS SCIENCE↗
DOE OSTI2022

New NDA Methods for Thorium Fuel Cycle Safeguards (Mid-Project Report)

This project is developing new Non-Destructive Assay (NDA) safeguards techniques for emergent thorium fuel cycles based on Neutron Resonance Transmission Analysis (NRTA), which can assay 233 U and 235 U when they are present together in a sample with potentially high gamma-ray backgrounds from fission products and 232 U. Existing passive techniques face large challenges for this task so new active interrogation methods are needed. This effort is also exploring how gamma-ray signatures can complement NRTA for enhanced assayed performance. This project leverages an NRTA system being developed at PNNL in collaboration with MIT, which uses a commercially available deuterium-tritium neutron generator at short standoff (~2 m). We aim to assess the feasibility and performance of these new NDA techniques for the range of relevant samples in thorium fuel cycles. Key advancements described in this mid-project report include NRTA system design for thorium safeguards measurements, characterization of 233 U oxide powder at PNNL, a survey of detector technologies suitable for NRTA in high gamma background environments, successful preliminary demonstration of a quantitative isotopic estimation algorithm, and first NRTA measurements of a thorium sample.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1979

Delamination crack growth in unidirectional fiber-reinforced composites under static and cyclic loading

An investigation of delamination crack growth in a unidirectional composite laminate under static and fatigue loading conditions is presented. An experimental program was conducted to study failure mechanisms and characterize the crack growth rate; analytical modeling based on microscopic observations was carried out using an advanced singular finite element method of the hybrid-stress model. Using a mixed-mode failure criterion, the delamination growth under a monotonically increasing load can be predicted; the rate of delamination crack propagation under fatigue loading is directly related to the amplitudes of cyclic opening and shearing mode stress intensity factors by a power law relationship.

Wang, S. S.↗
NASA NTRS1985

Space station data system analysis/architecture study. Task 2: Options development DR-5. Volume 1: Technology options

The second task in the Space Station Data System (SSDS) Analysis/Architecture Study is the development of an information base that will support the conduct of trade studies and provide sufficient data to make key design/programmatic decisions. This volume identifies the preferred options in the technology category and characterizes these options with respect to performance attributes, constraints, cost, and risk. The technology category includes advanced materials, processes, and techniques that can be used to enhance the implementation of SSDS design structures. The specific areas discussed are mass storage, including space and round on-line storage and off-line storage; man/machine interface; data processing hardware, including flight computers and advanced/fault tolerant computer architectures; and software, including data compression algorithms, on-board high level languages, and software tools. Also discussed are artificial intelligence applications and hard-wire communications.

Source record↗
NASA NTRS1991

Effect of LEO cycling on 125 Ah advanced design IPV nickel-hydrogen flight cells. An update

Validation testing of the NASA Lewis 125 Ah advanced design individual pressure vessel (IPV) nickel-hydrogen flight cells was conducted. Work consisted of characterization, storage, and cycle life testing. There was no capacity degradation after 52 days of storage with the cells in the discharged state, an open circuit, 0 C, and a hydrogen pressure of 14.5 psia. The catalyzed wall wick cells were cycled for over 11,000 cycles with no cell failures in the continuing test. One of the noncatalyzed wall wick cells failed.

Smithrick, John J.↗
NASA NTRS1992

A comparative study of advanced shock-capturing schemes applied to Burgers' equation

A systematic evaluation is conducted of all extant numerical schemes for nonlinear scalar transport problems, and several advanced shock-capturing schemes are used to solve the nonlinear Burgers' equation in order to characterize their ability to resolve the sharp discontinuity, expansion zone, and propagation and collision features of shocks. For discontinuous functions, the Warming-Beam scheme generates preshock wiggles, while the Lax-Wendroff scheme generates postshock ones. Such limiters as the MUSCL or the superbee are more compressive than minimod or monotonic limiters. The performance of such TVD schemes as the upwind, the symmetric, and the Roe-Sweby, resemble each other.

Yang, H. Q.↗
NASA NTRS1994

Handling qualities of the High Speed Civil Transport

The low speed handling qualities of a High Speed Civil Transport class aircraft have been investigated by using data of the former Advanced Supersonic Transport (AST) 105. The operation of such vehicles in the airport terminal area is characterized by 'backside' performance. Main objectives of this research effort were: (Q) determination of the nature and magnitude of the speed instability associated with the backside of the thrust required curve; (2) confirmation of the validity of existing MIL-SPEC handling qualities criteria; (3) safety of operation of the vehicle in the event of autothrottle failure; and (4) correlation of required engine responsiveness with level of speed instability. Preliminary findings comprise the following: (1) The critical velocity for speed instability was determined to be 196 knots, well above the projected approach speed of 155 knots. This puts the vehicle far on the backside of its thrust required curve. While the aircraft can be configured to have static and dynamic stability at this trim point, a significant speed instability emerges, if a pilot or autopilot attempts flight path control with elevator and/or canard control surfaces only. This requires a properly configured autothrottle and/or variable aerodynamic drag devices which can provide speed stability; (2) An AST 105 type vehicle meets MIL-SPEC criteria only in part. While the damping criteria for phugoid and short period motion are met easily, the AST 105 falls short of the required minimum short period frequency, meaning that the HSCT is too sluggish in pitch to meet the military criteria. Obviously the military specification do not consider a vehicle with such high pitch inertia. With regard to speed stability and flight path stability criteria, the vehicle meets levels 2 and 3 of the military requirements, indicating that it would be landed safety with manual controls in case of an autothrottle failure, even though the pilot workload would be high; and (3) This requires quick thrust response to throttle adjustment, however. If the engine responsiveness is slow, the aircraft handling qualities are further deteriorated. Progress has been made in correlating required engine responses dyanmics with the given level of speed instability of the vehicle.

Solies, U. Peter↗
NASA NTRS1996

Least Squares Best Fit Method for the Three Parameter Weibull Distribution: Analysis of Tensile and Bend Specimens with Volume or Surface Flaw Failure

Material characterization parameters obtained from naturally flawed specimens are necessary for reliability evaluation of non-deterministic advanced ceramic structural components. The least squares best fit method is applied to the three parameter uniaxial Weibull model to obtain the material parameters from experimental tests on volume or surface flawed specimens subjected to pure tension, pure bending, four point or three point loading. Several illustrative example problems are provided.

Gross, Bernard↗
NASA NTRS1997

A New Foil Air Bearing Test Rig for Use to 700 C and 70,000 rpm

A new test rig has been developed for evaluating foil air bearings at high temperatures and speeds. These bearings are self acting hydrodynamic air bearings which have been successfully applied to a variety of turbomachinery operating up to 650 C. This unique test rig is capable of measuring bearing torque during start-up, shut-down and high speed operation. Load capacity and general performance characteristics, such as durability, can be measured at temperatures to 700 C and speeds to 70,000 rpm. This paper describes the new test rig and demonstrates its capabilities through the preliminary characterization of several bearings. The bearing performance data from this facility can be used to develop advanced turbomachinery incorporating high temperature oil-free air bearing technology.

DellaCorte, Chris↗
NASA NTRS2006

Nanomaterials for Space Exploration Applications

Nano-engineered materials are multi-functional materials with superior mechanical, thermal and electrical properties. Nanomaterials may be used for a variety of space exploration applications, including ultracapacitors, active/passive thermal management materials, and nanofiltration for water recovery. Additional applications include electrical power/energy storage systems, hybrid systems power generation, advanced proton exchange membrane fuel cells, and air revitalization. The need for nanomaterials and their growth, characterization, processing and space exploration applications is discussed. Data is presented for developing solid-supported amine adsorbents based on carbon nanotube materials and functionalization of nanomaterials is examined.

Moloney, Padraig G.↗
NASA NTRS2009

Effective Materials Property Information Management for the 21st Century

This paper discusses key principles for the development of materials property information management software systems. There are growing needs for automated materials information management in various organizations. In part these are fueled by the demands for higher efficiency in material testing, product design and engineering analysis. But equally important, organizations are being driven by the need for consistency, quality and traceability of data, as well as control of access to sensitive information such as proprietary data. Further, the use of increasingly sophisticated nonlinear, anisotropic and multi-scale engineering analyses requires both processing of large volumes of test data for development of constitutive models and complex materials data input for Computer-Aided Engineering (CAE) software. And finally, the globalization of economy often generates great needs for sharing a single "gold source" of materials information between members of global engineering teams in extended supply chains. Fortunately, material property management systems have kept pace with the growing user demands and evolved to versatile data management systems that can be customized to specific user needs. The more sophisticated of these provide facilities for: (i) data management functions such as access, version, and quality controls; (ii) a wide range of data import, export and analysis capabilities; (iii) data "pedigree" traceability mechanisms; (iv) data searching, reporting and viewing tools; and (v) access to the information via a wide range of interfaces. In this paper the important requirements for advanced material data management systems, future challenges and opportunities such as automated error checking, data quality characterization, identification of gaps in datasets, as well as functionalities and business models to fuel database growth and maintenance are discussed.

Ren, Weiju↗
NASA NTRS2011

CO2 Washout Testing of the REI and EM-ACES Space Suits

Requirements for using a space suit during ground testing include providing adequate carbon dioxide (CO2) washout for the suited subject. Acute CO2 exposure can lead to symptoms including headache, dyspnea, lethargy and eventually unconsciousness or even death. Symptoms depend on several factors including partial pressure of CO2 (ppCO2), duration of exposure, metabolic rate of the subject and physiological differences between subjects. The objective of this test was to characterize inspired oronasal ppCO2 in the Rear Entry I-Suit (REI) and the Enhanced Mobility Advanced Crew Escape Suit (EM-ACES) across a range of workloads and flow rates for which ground testing is nominally performed. Three subjects were tested in each suit. In all but one case, each subject performed the test twice to allow for comparison between tests. Suit pressure was maintained at 4.3 psid. Subjects wore the suit while resting, performing arm ergometry, and walking on a treadmill to generate metabolic workloads of approximately 500 to 3000 BTU/hr. Supply airflow was varied at 6, 5 and 4 actual cubic feet per minute (ACFM) at each workload. Subjects wore an oronasal mask with an open port in front of the mouth and were allowed to breathe freely. Oronasal ppCO2 was monitored real-time via gas analyzers with sampling tubes connected to the oronasal mask. Metabolic rate was calculated from the total CO2 production measured by an additional gas analyzer at the air outlet from the suit. Real-time metabolic rate was used to adjust the arm ergometer or treadmill workload to meet target metabolic rates. In both suits, inspired CO2 was primarily affected by the metabolic rate of the subject, with increased metabolic rate resulting in increased inspired ppCO2. Suit flow rate also affected inspired ppCO2, with decreased flow causing small increases in inspired ppCO2. The effect of flow was more evident at metabolic rates greater than or equal to 2000 BTU/hr. Results were consistent between suits, with the EM-ACES demonstrating slightly better CO2 washout than the REI suit, but not statistically significant. Regression equations were developed for each suit to predict the mean inspired ppCO2 as a function of metabolic rate and suit flow rate. This paper provides detailed descriptions of the test hardware, methodology and results, as well as implications for future ground testing in the REI and EM-ACES.

Mitchell, Kate↗
NASA NTRS2003

Wavelet-Based Real-Time Diagnosis of Complex Systems

A new method of robust, autonomous real-time diagnosis of a time-varying complex system (e.g., a spacecraft, an advanced aircraft, or a process-control system) is presented here. It is based upon the characterization and comparison of (1) the execution of software, as reported by discrete data, and (2) data from sensors that monitor the physical state of the system, such as performance sensors or similar quantitative time-varying measurements. By taking account of the relationship between execution of, and the responses to, software commands, this method satisfies a key requirement for robust autonomous diagnosis, namely, ensuring that control is maintained and followed. Such monitoring of control software requires that estimates of the state of the system, as represented within the control software itself, are representative of the physical behavior of the system. In this method, data from sensors and discrete command data are analyzed simultaneously and compared to determine their correlation. If the sensed physical state of the system differs from the software estimate (see figure) or if the system fails to perform a transition as commanded by software, or such a transition occurs without the associated command, the system has experienced a control fault. This method provides a means of detecting such divergent behavior and automatically generating an appropriate warning.

Gulati, Sandeep↗
NASA NTRS2012

CO2 Washout Testing of the REI and EM-ACES Space Suits

When a space suit is used during ground testing, adequate carbon dioxide (CO2) washout must be provided for the suited subject. Symptoms of acute CO2 exposure depend on partial pressure of CO2 (ppCO2), metabolic rate of the subject, and other factors. This test was done to characterize inspired oronasal ppCO2 in the Rear Entry I-Suit (REI) and the Enhanced Mobility Advanced Crew Escape Suit (EM-ACES) for a range of workloads and flow rates for which ground testing is nominally performed. Three subjects were tested in each suit. In all but one case, each subject performed the test twice. Suit pressure was maintained at 4.3 psid. Subjects wore the suit while resting, performing arm ergometry, and walking on a treadmill to generate metabolic workloads of about 500 to 3000 BTU/hr. Supply airflow was varied between 6, 5, and 4 actual cubic feet per minute (ACFM) at each workload. Subjects wore an oronasal mask with an open port in front of the mouth and were allowed to breathe freely. Oronasal ppCO2 was monitored in real time by gas analyzers with sampling tubes connected to the mask. Metabolic rate was calculated from the total CO2 production measured by an additional gas analyzer at the suit air outlet. Real-time metabolic rate was used to adjust the arm ergometer or treadmill workload to meet target metabolic rates. In both suits, inspired CO2 was affected mainly by the metabolic rate of the subject: increased metabolic rate significantly (P < 0.05) increased inspired ppCO2. Decreased air flow caused small increases in inspired ppCO2. The effect of flow was more evident at metabolic rates . 2000 BTU/hr. CO2 washout values of the EM-ACES were slightly but not significantly better than those of the REI suit. Regression equations were developed for each suit to predict the mean inspired ppCO2 as a function of metabolic rate and suit flow rate. This paper provides detailed descriptions of the test hardware, methodology, and results as well as implications for future ground testing in the REI-suit and EM-ACES.

Mitchell, Kathryn C.↗
NASA NTRS2012

DRAGONS - A Micrometeoroid and Orbital Debris Impact Sensor

The Debris Resistive/Acoustic Grid Orbital Navy Sensor (DRAGONS) is intended to be a large area impact sensor for in-situ measurements of micrometeoroids and orbital debris (MMOD) in the approx.0.2 to 1 mm size regime. These MMOD particles are too small to be detected by groundbased radars and optical telescopes, but still large enough to be a safety concern for human space activities and robotic missions in the low Earth orbit (LEO) region. The nominal detection area of DRAGONS is 1 sq m, consisting of four 0.5 m x 0.5 m independently operated panels. The concept of the DRAGONS design is to combine three different detection technologies to maximize information extracted from each detected impact. The first technology is a resistive grid consisting of 62.5-microns-wide resistive lines, coated in parallel and separated by 62.5 micron gaps on a Kapton film. When a particle a few hundred micrometers or larger strikes the grid, it world penetrate the film and sever some resistive lines. The size of the damage area can be estimated from the increased resistance. The second technology employs a dual-layer, 25-microns-thick Kapton film with a 10 cm separation. By measuring the time difference between impacts on the two films, the impact speed can be calculated. The third technology is based on polyvinylidene fluoride (PVDF) acoustic impact sensors. Multiple PVDF sensors are attached to the backside of both Kapton films to provide impact timing measurements. The impact location on each film can be identified from the triangulation of signals received at different PVDF sensors and provides an estimate of the impact direction. The development of DRAGONS is supported by the NASA Orbital Debris Program Office. The project is led by the U.S. Naval Academy (USNA), with additional collaboration from the U.S. Naval Research Laboratory (NRL), the University of Kent at Canterbury in Great Britain, and Virginia Tech (VT). The short-term goal of DRAGONS is to advance its Technology Readiness Level to 9 and to demonstrate the system capabilities of detecting and characterizing submillimeter MMOD impacts. The long-term goal is to deploy a large detection area (>1 sq m) DRAGONS to 700-1000 km altitude and collect sufficient data for better environment definition of MMOD in the 0.2- to 1-mm size regime. The Preliminary Design Review (PRD) of DRAGONS was held at the USNA in June 2012. The Critical Design Review (CDR) is scheduled for early 2013. A flight-ready unit with a 0.25 sq m detection area will be completed and tested by the end of September 2013. The biggest challenge for the project, however, is to identify a demonstration opportunity on the International Space Station in the coming years.

Liou, J. C.↗