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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 163 records · Page 9
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Sustainable, degradable and malleable low-dielectric-constant thermosets derived from biomass for recyclable green electronics

In view of their excellent thermal and chemical resistance, favorable adhesion properties, high tensile strength, and other advantages, epoxy thermosets have numerous industrial applications such as coating, adhesive, and composite material production. However, bisphenol A (BPA)-based resins, which account for a significant fraction of the above thermosets, adversely affect human health by interfering with the normal functioning of the endocrine system and cannot be easily decomposed and recycled. Herein, degradable and sustainable bio-based epoxy thermosets with crosslinked network structures are prepared by the epoxidation of isosorbide with epichlorohydrin and the curing of the produced isosorbide diglycidyl ether (ISDGE) with cyclic lactones through a cationic ring-opening reaction. The ISDGE thermosets fully decompose into soluble and recyclable products under mildly basic conditions within three days, which is ascribed to the presence of ester moieties within the polymer network structure. Compared to a representative BPA-based epoxy, ISDGE-based thermosets exhibit lower dielectric constants and are more flexible. Moreover, the glass fibers in ISDGE-based prepregs can be fully recovered after on-demand degradation. Furthermore, our work provides promising eco-friendly alternatives to conventional epoxy thermosets and paves the way for the reduction of plastic waste generation and the development of recyclable green electronics.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2026

Southern Ocean Sulfate Aerosol Sources Quantified From Sulfur Isotopes in Antarctic Ice Cores

The Southern Ocean has emerged as a key region for constraining aerosol-climate interactions due to its relatively low anthropogenic influence. Sulfate is an important aerosol over the Southern Ocean, and models suggest dimethyl sulfide (DMS) is the largest source of sulfate during summer. However, sulfur isotopes of sulfate (δ 34 S(SO 4 2− )) in Antarctic ice cores suggest a significant contribution from a previously unexplained non-DMS source. Here we show that the fractional contribution from passive volcanic degassing (f volc ) explains observed δ 34 S(SO 4 2− ), and that a global chemical transport model underestimates f volc across Antarctica. Underestimated f volc implies that the model mischaracterizes sulfate sources in this important region. The discrepancy between observed and modeled sulfate sources can be reconciled by increasing passive volcanic sulfur degassing emissions and decreasing DMS emissions. Our results imply that current biases in emissions inventories could bias assessments of aerosol-cloud interactions in the Southern Ocean region and globally.

Jongebloed, Ursula A. [Univ. of Washington, Seattl↗
DOE OSTI2024

Evaluation of Technology for Dry Retrieval of Tank Waste

The Hanford Roadmap report (NNLEMS-2022-00005) identified Dry Retrieval as an opportunity to make a significant impact on accelerating the Department of Energy-Environmental Management tank waste mission. Several commercially available technologies have been identified that hold the potential to enable Single Shell Tank retrieval without large infrastructure investments. The opportunity exists to leverage the technologies of the commercial mining, food, chemical, and pharmaceutical industries with advances in robotics for the tank waste retrieval mission.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2024

A shift between mineral and nonmineral sources of iron and sulfur causes proteome-wide changes in Methanosarcina barkeri

ABSTRACT Iron (Fe) and sulfur (S) are required elements for life, and changes in their availability can limit the ecological distribution and function of microorganisms. In anoxic environments, soluble Fe typically exists as ferrous iron [Fe(II)] and S as sulfide (HS − ). These species exhibit a strong affinity that ultimately drives the formation of sedimentary pyrite (FeS 2 ). Recently, paradigm-shifting studies indicate that Fe and S in FeS 2 can be made bioavailable by methanogens through a reductive dissolution process. However, the impact of the utilization of FeS 2 , as opposed to canonical Fe and S sources, on the phenotype of cells is not fully understood. Here, shotgun proteomics was utilized to measure changes in the phenotype of Methanosarcina barkeri MS grown with FeS 2 , Fe(II)/HS − , or Fe(II)/cysteine. Shotgun proteomics tracked 1,019 proteins overall, with 307 observed to change between growth conditions. Functional characterization and pathway analyses revealed these changes to be systemic and largely tangential to Fe/S metabolism. As a final step, the proteomics data were viewed with respect to previously collected transcriptomics data to deepen the analysis. Presented here is evidence that M. barkeri adopts distinct phenotypes to exploit specific sources of Fe and S in its environment. This is supported by observed protein abundance changes across broad categories of cellular biology. DNA adjacent metabolism, central carbon metabolism methanogenesis, metal trafficking, quorum sensing, and porphyrin biosynthesis pathways are all features in the phenotypic differentiation. Differences in trace metal availability attributed to complexation with HS − , either as a component of the growth medium [Fe(II)/HS − ] or generated through reduction of FeS 2 , were likely a major factor underpinning these phenotypic differences. IMPORTANCE The methanogenic archaeon Methanosarcina barkeri holds great potential for industrial bio-mining and energy generation technologies. Much of the biochemistry of this microbe is poorly understood, and its characterization will provide a glimpse into biological processes that evolved close to life’s origin. The discovery of its ability to extract iron and sulfur from bulk, solid-phase minerals shifted a longstanding paradigm that these elements were inaccessible to biological systems. The full elucidation of this process has the potential to help scientists and engineers extract valuable metals from low-grade ore and mine waste generating energy in the form of methane while doing so.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2025

First Measurement of $𝜈_𝑒$ and $\bar{𝜈}_𝑒$ Charged-Current Single Charged-Pion Production Differential Cross Sections on Argon Using the MicroBooNE Detector

Understanding electron neutrino interactions is crucial for measurements of neutrino oscillations and searches for new physics in neutrino experiments. We present the first measurement of the flux-averaged $𝜈_𝑒$ + $\bar{𝜈}_𝑒$ charged-current single charged-pion production cross section on argon using the MicroBooNE detector and data from the NuMI neutrino beam. The total cross section is measured to be [0.93 ± 0.13⁢(stat) ± 0.27⁢(syst)] × 10 −39 cm 2 /nucleon at a mean $𝜈_𝑒$ + $\bar{𝜈}_𝑒$ energy of 730 MeV. Differential cross sections are also reported in electron energy, electron and pion angles, and electron-pion opening angle.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

An ICP-OES method for the precise and accurate quantification of rare earth elements in natural water: A comparative study from mine waste sites in New Mexico, USA

Inductively coupled plasma techniques such as ICP-OES and ICP-MS are routinely used to determine the concentrations of rare earth elements (REE) in water samples. However, their performance for the determination of REE concentration in mine drainage waters from epithermal vein and porphyry copper mining districts has not been evaluated extensively. In this work, we develop an REE analysis method on an Agilent 5900 ICP-OES instrument and assess the accuracy and precision for the quantification of REE in the natural waters collected from mine adits and an acid seep of mine sites in the Steeple Rock and Hillsboro mining districts, New Mexico, USA. The total REE concentrations in the water samples were measured using the methods we developed for both ICP-OES and ICP-MS. The power of the new ICP-OES method lies in routine analysis of μg/L level concentrations normally analyzed using ICP-MS, including a U.S. Geological Survey standard reference sample, laboratory blank samples spiked with a National Institute of Standards and Technology traceable standard, and surface water samples from mine waste sites. This ICP-OES method achieves low quantification limits ranging from 0.2 to 5 μg/L and excellent analytical accuracy and precision for REE analysis. The precision of light (La-Gd) and heavy (Tb-Lu) REE analysis using this method are better than 5% at average concentrations above 5 ± 4 μg/L and 3 ± 2 μg/L, respectively, and 3% at average concentrations above 10 ± 9 μg/L and 5 ± 4 μg/L, respectively. This method also shows excellent sensitivity and reproducibility for our laboratory and field samples.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

First Double-Differential Cross Section Measurement of Neutral-Current 𝜋 0 Production in Neutrino-Argon Scattering in the MicroBooNE Detector

We report the first double-differential cross section measurement of neutral-current neutral pion (NC⁢𝜋 0 ) production in neutrino-argon scattering, as well as single-differential measurements of the same channel in terms of final states with and without protons. The kinematic variables of interest for these measurements are the 𝜋 0 momentum and the 𝜋 0 scattering angle with respect to the neutrino beam. A total of 4971 candidate NC⁢𝜋 0 events fully contained within the MicroBooNE detector are selected using data collected at a mean neutrino energy of ∼0.8 GeV from 6.4 ×10 20 protons on target from the Booster Neutrino Beam at the Fermi National Accelerator Laboratory. After extensive data-driven model validation to ensure unbiased unfolding, the Wiener-singular-value-decomposition method is used to extract nominal flux-averaged cross sections. The results are compared to predictions from commonly used neutrino event generators, which tend to overpredict the measured NC⁢𝜋 0 cross section, especially in the 0.2–0.5 GeV/c 𝜋 0 momentum range and at forward scattering angles. Events with at least one proton present in the final state are also underestimated. This data will help improve the modeling of NC⁢𝜋 0 production, which represents a major background in measurements of charge-parity violation in the neutrino sector and in searches for new physics beyond the standard model.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Multiparameter Constraints on Empirical Infrasound Period-Yield Relations for Bolides and Implications for Planetary Defense

How effective are methods for estimating bolide energies from infrasound signal period-yield relationships? A single global period–energy relation can obscure significant variability introduced by parameters such as the atmospheric Doppler wind profile and the bolide’s energy deposition profile as a function of altitude. Bolide speed, entry angle, burst altitude, and multiepisode fragmentation may all play a role in defining the detected period of the shockwave. By leveraging bolide light-curve data from the Center for Near Earth Object Studies, we re-examined the period–energy relation as a function of these parameters. Through a bootstrap approach, we show that various event subsets can deviate from widely cited period–energy models and we identify which specific conditions most strongly reshape the period–energy scaling. The results define both the fidelity and reliability of period–energy relations when no additional data beyond the infrasound record is available and improve the outcome when supporting data from bolide trajectories and light curves are included. Ultimately, these findings expand the scope of earlier models, providing a nuanced and robust framework for infrasound-only yield estimation under a range of bolide scenarios.

Planetary science↗
DOE OSTI2025

First study of neutrino angle reconstruction using quasielasticlike interactions in MicroBooNE

We investigate the expected precision of the reconstructed neutrino direction using a 𝜈 𝜇 -argon quasielasticlike event topology with one muon and one proton in the final state and the reconstruction capabilities of the MicroBooNE liquid argon time projection chamber. This direction is of importance in the context of DUNE sub-GeV atmospheric oscillation studies. MicroBooNE allows for a data-driven quantification of this resolution by investigating the deviation of the reconstructed muon-proton system orientation with respect to the well-known direction of neutrinos originating from the Booster Neutrino Beam with an exposure of 1.3 ×10 21 protons on target. Using simulation studies, we derive the expected sub-GeV DUNE atmospheric-neutrino reconstructed simulated spectrum by developing a reweighting scheme as a function of the true neutrino energy. We further report flux-integrated single- and double-differential cross section measurements of charged-current 𝜈 𝜇 quasielasticlike scattering on argon as a function of the muon-proton system angle using the full MicroBooNE data sets. We also demonstrate the sensitivity of these results to nuclear effects and final state hadronic reinteraction modeling.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

Search for the production of Higgs-portal scalar bosons in the NuMI beam using the MicroBooNE detector

We present the strongest experimental limits to date on the mixing angle, 𝜃, with which a new scalar particle, 𝑆, mixes with the Higgs field in the mass range 110 MeV < 𝑚 𝑆 <155 MeV. This result uses the MicroBooNE liquid argon time projection chamber to search for decays of these Higgs-portal scalar particles through the 𝑆 → 𝑒 + ⁢𝑒 − channel with the decays of kaons in the NuMI neutrino beam acting as the source of the scalar particles. The analysis uses an exposure of 2.01 × 10 21 protons on target of NuMI beam data including periods when the beam focusing system was configured to focus positively charged hadrons and separate periods when negatively charged hadrons were focused. The analysis searches for scalar particles produced from kaons decaying in flight in the beam’s decay volume and at rest in the target and absorber. At 𝑚 𝑆 =125 MeV (𝑚 𝑆 =150 MeV) we set a limit of 𝜃 < 3.19 ×10 −4 (𝜃 < 2.79 ×10 −4 ) at the 95% confidence level.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Demonstration of new MeV-scale capabilities in large neutrino LArTPCs using ambient radiogenic and cosmogenic activity in MicroBooNE

Large neutrino liquid argon time projection chamber (LArTPC) experiments can broaden their physics reach by reconstructing and interpreting MeV-scale energy depositions, or blips, present in their data. We demonstrate new calorimetric and particle discrimination capabilities at the MeV energy scale using reconstructed blips in data from the MicroBooNE LArTPC at Fermilab. We observe a concentration of low-energy (<3 MeV) blips around fiberglass mechanical support struts along the time projection chamber edges with energy spectrum features consistent with the Compton edge of 2.614 MeV 208 Tl decay 𝛾 rays. These features are used to verify proper calibration of electron energy scales in MicroBooNE’s data to few percent precision and to measure the specific activity of 208 Tl in the fiberglass composing these struts, (11.7 ± 0.2⁢(stat) ± 3.1⁢(syst)) Bq/kg. Cosmogenically produced blips above 3 MeV in reconstructed energy are used to showcase the ability of large LArTPCs to distinguish between low-energy proton and electron energy depositions. An enriched sample of low-energy protons selected using this new particle discrimination technique is found to be smaller in data than in dedicated corsika cosmic-ray simulations, suggesting either incorrect corsika modeling of incident cosmic fluxes or particle transport modeling issues in geant4.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Data-driven model validation for neutrino-nucleus cross section measurements

Neutrino-nucleus cross section measurements are needed to improve interaction modeling to meet the precision needs of neutrino experiments in efforts to measure oscillation parameters and search for physics beyond the Standard Model. We review the difficulties associated with modeling neutrino-nucleus interactions that lead to a dependence on event generators in oscillation analyses and cross section measurements alike. We then describe data-driven model validation techniques intended to address this model dependence. The method relies on utilizing various goodness-of-fit tests and the correlations between different observables and channels to probe the model for defects in the phase space relevant for the desired analysis. These techniques shed light on relevant mismodeling, allowing it to be detected before it begins to bias the cross section results. We compare more commonly used model validation methods which directly validate the model against alternative ones to these data-driven techniques and show their efficacy with fake data studies. These studies demonstrate that employing data-driven model validation in cross section measurements represents a reliable strategy to produce robust results that will stimulate the desired improvements to interaction modeling.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Search for an Anomalous Production of Charged-Current 𝜈 𝑒 Interactions without Visible Pions across Multiple Kinematic Observables in MicroBooNE

This Letter presents an investigation of low-energy electron-neutrino interactions in the Fermilab Booster Neutrino Beam by the MicroBooNE experiment, motivated by the excess of electron-neutrino-like events observed by the MiniBooNE experiment. This is the first measurement to use data from all five years of operation of the MicroBooNE experiment, corresponding to an exposure of 1.11 × 10 21 protons on target, a 70% increase on past results. Two samples of electron neutrino interactions without visible pions are used, one with visible protons and one without any visible protons. The MicroBooNE data show reasonable agreement with the nominal prediction, with 𝑝 values ≥26.7% when the two 𝜈 𝑒 samples are combined, though the prediction exceeds the data in limited regions of phase space. The data are further compared to two empirical models that modify the predicted rate of electron-neutrino interactions in different variables in the simulation to match the unfolded MiniBooNE low energy excess. In the first model, this unfolding is performed as a function of electron neutrino energy, while the second model aims to match the observed shower energy and angle distributions of the MiniBooNE excess. This measurement excludes an electronlike interpretation of the MiniBooNE excess based on these models at >99% CLs in all kinematic variables.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

JWST Observations of Starbursts: Dust Processing in the M82 Superwind

We present JWST MIRI and NIRCam imaging of the inner ∼5 kpc of the M82 superwind at ~ $0''_{.}05 - 0''_{.}375$(∼0.9–6.5 pc) resolution. Targeted filters probe emission from polycyclic aromatic hydrocarbons (PAHs; F335M, F360M, F770W, F1130W) and continuum (F250M, F360M) The images reveal a network of cool wind filaments traced by PAHs. PAH surface brightness declines with the inverse square of distance to the midplane, suggesting that the incident radiation field from the starburst drives the observed PAH intensity out to ±2.5 kpc. The 3.3/11.3 and 3.3/7.7 μm band ratios show uniformity with distance from the starburst, though comparisons with mid-IR dust emission models indicate a modest shift toward larger PAHs. Outside the disk, 11.3/7.7 μm increases moderately, reflecting that PAHs become more neutral with distance from the starburst as they are exposed to a declining radiation field and ionization parameter. Overall, PAHs in the wind are consistent with standard-to-large sizes and standard-to-high ionization states. Including Spitzer and Herschel data, PAH abundance (q PAH ) is set at ∼1% in the starburst and remains unchanging out to ±5 kpc off the disk. This flat q PAH profile suggests that PAHs are shielded from the hot wind, perhaps residing in the surface layers of cool clouds, with possible replenishment from cloud interiors and enrichment of the halo from previous bursts. In this picture, clouds are not dense enough to promote PAH growth, and they likely undergo radiative cooling and mixing with the hot phase to survive the gauntlet for at least ∼20 Myr.

Cronin, Serena A. [University of Maryland, College↗
DOE OSTI2025

Measurement of single- and double-differential cross sections for mesonless charged-current muon neutrino interactions on argon with final-state protons using the MicroBooNE detector

Charged-current neutrino interactions with final states containing zero mesons and at least one proton are of high interest for current and future accelerator-based neutrino oscillation experiments. Using the Booster Neutrino Beam and the MicroBooNE detector at Fermi National Accelerator Laboratory, we have obtained the first double-differential cross-section measurements of this channel for muon neutrino scattering on an argon target with a leading proton momentum threshold of 0.25 GeV/𝑐. We also report a flux-averaged total cross section of 𝜎 = (11.8±1.2) × 10 −38 cm 2 /Ar and several single-differential measurements which extend and improve upon previous results. Statistical and systematic uncertainties are quantified with a full treatment of correlations across 359 kinematic bins, including correlations between distributions describing different observables. The resulting dataset provides the most detailed information obtained to date for testing models of mesonless neutrino-argon scattering.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Enhanced search for neutral current Δ radiative single-photon production in MicroBooNE

We report results from an updated search for neutral current (NC) resonant Δ⁡(1232) baryon production and subsequent Δ radiative decay (NC Δ → 𝑁⁢𝛾). We consider events with and without final state protons; events with a proton can be compared with the kinematics of a Δ⁡(1232) baryon decay, while events without a visible proton represent a more generic phase space. In order to maximize sensitivity to each topology, we simultaneously make use of two different reconstruction paradigms, Pandora and Wire-Cell, which have complementary strengths, and select mostly orthogonal sets of events. Considering an overall scaling of the NC Δ → 𝑁⁢𝛾 rate as an explanation of the MiniBooNE anomaly, our data exclude this hypothesis at 94.4% CL. When we decouple the expected correlations between NC Δ → 𝑁⁢𝛾 events with and without final state protons, our data exclude an interpretation in which all excess events have associated protons at 2.0⁢𝜎, and are consistent with an interpretation in which all excess events have no associated protons at 0.63⁢𝜎.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

First Search for Dark Sector 𝑒 + ⁢𝑒 − Explanations of the MiniBooNE Anomaly at MicroBooNE

We present MicroBooNE’s first search for dark sector 𝑒 + ⁢𝑒 − explanations of the long-standing MiniBooNE anomaly. The MiniBooNE anomaly has garnered significant attention over the past 20 years including previous MicroBooNE investigations into both anomalous electron and photon excesses, but its origin still remains unclear. In this Letter, we provide the first direct test of dark sector models in which dark neutrinos, produced through neutrino-induced scattering, decay into missing energy and visible 𝑒 + ⁢𝑒 − pairs comprising the MiniBooNE anomaly. Many such models have recently gained traction as a viable solution to the anomaly while evading past bounds. Using an exposure of 6.87 × 10 20 protons-on-target in the Booster Neutrino Beam, we implement a selection targeting forward-going, coherently produced 𝑒 + ⁢𝑒 − events. After unblinding, we observe 95 events, which we compare with the constrained background-only prediction of 69.7 ±17.3. This analysis sets the world’s first direct limits on these dark sector models and, at the 95% confidence level, excludes the entirety of the single dark neutrino and majority of the dual dark neutrino, parameter space that is viable as a solution to the MiniBooNE anomaly.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2026

Inclusive Search for Anomalous Single-Photon Production in MicroBooNE

We present an inclusive search for anomalous production of single-photon events from neutrino interactions in the MicroBooNE experiment. The search and its signal definition are motivated by the previous observation of a low-energy excess of electromagnetic shower events from the MiniBooNE experiment. We use the Wire-Cell reconstruction framework to select a sample of inclusive single-photon final-state interactions with a final efficiency and purity of 7.0% and 40.2%, respectively. We leverage simultaneous measurements of sidebands of charged current 𝜈 𝜇 interactions and neutral current interactions producing 𝜋 0 mesons to constrain signal and background predictions and reduce uncertainties. We perform a blind analysis using a dataset collected from February 2016 to July 2018, corresponding to an exposure of 6.34 × 10 20 protons on target from the Booster Neutrino Beam at Fermilab. In the full signal region, we observe agreement between the data and the prediction, with a goodness-of-fit 𝑝 value of 0.11. We then isolate a subsample of these events containing no visible protons, and observe 93 ± 22⁢(stat) ±35⁢(syst) data events above prediction, corresponding to just above 2⁢𝜎 local significance, concentrated at shower energies below 600 MeV.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗