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At least 163 records · Page 9

Optical transmittance of fused silica during irradiation processes.

The level of irradiation-induced optical absorption and the resulting heat deposition in the transparent fused-silica wall of a nuclear light bulb engine during normal operation are investigated by means of a series of related experiments using available radiation sources, each of which simulates some aspect of the radiation flux or dose of the engine. A comparison of the results obtained in electron and reactor experiments indicates that the generation of optical absorption is due to ionizing effects and that neutron-caused displacement effects do not contribute significantly to optical absorption. The implications of these and other results obtained are discussed.

Palma, G. E.↗

Artificial microfossils - Experimental studies of permineralization of blue-green algae in silica.

A technique has been developed to artificially fossilize microscopic algae in crystalline silica under conditions of moderately elevated temperature and pressure. The technique is designed to simulate geochemical processes thought to have resulted in the preservation of organic microfossils in Precambrian bedded cherts. In degree of preservation and mineralogic setting, the artificially permineralized microorganisms are comparable to naturally occurring fossil algae.

Oehler, J. H.↗

Silica reinforcement and char reactions in the Apollo heat shield.

Reactions of the silica reinforcement fiber and ablation char of the Apollo heat shield have been investigated by laboratory tests in an arc image furnace (at temperature levels up to 5000 R, pressures up to 0.7 atm, and heat flux similar to reentry) and by an actual reentry test. Microchemical analyses and X-ray diffraction studies have been made to determine the presence of SiC formation in the char. Experimental data and analytical predictions of thermal and density profiles have been compared for the ablation of virgin heat shield and precharred materials to determine the effects of SiC formation on ablation performance. In all analyses, general agreement was found between chemical composition and the thermal predictions for laboratory tests and reentry materials. In all ablated materials, SiC was formed in the front surface of the char. The highest SiC content found was 58% by weight and found in a high-pressure environment. The SiC formed was found to act as a heat sink in the ablation process and can lower the front surface temperature by 300 R.

Cagliostro, D. E.↗

Fabrication and Improvement of Lmsc's All-silica RSI

The LI-1500 and LI-900 all silica RSI materials have made the transition from laboratory to manufacturing operation. Improvements in both quality and reproducibility have been achieved. The LI-1500 material has displayed superior reliability in evaluations conducted at various facilities. The dependable performance of the material is attributed to the adherence to the stringent requirements of the numerous material, process, and product control evaluations and inspection points performed during manufacture.

Beasley, R. M.↗

Environmental compatibility of the all-silica rigid surface insulation

Testing has demonstrated the compatibility of the all-silica surface insulation system to a variety of space shuttle orbiter environmental aspects for launch, on-orbit, and special reentry conditions. Among the more important results are the success of the cold soak tests, which indicate the suitability of the foam/bond attachment system with a 2 mm thick foam pad for strain isolation, and the reentry temperature overshoot tests (to 1924 K), which show that this system can tolerate considerable dispersion in reentry heating environment.

Housten, S. J.↗

Improved coating for silica fiber based ceramic Reusable Surface Insulation (CRSI)

A series of coatings was developed for the space shuttle type silica fiber insulation system and characterized for optical and physical properties. Reentry simulation tests were run using a radiant panel and also using a hypersonic plasma arc. The coatings produced had improved physical and optical properties as well as greater reuse capability over the GE version of the JSC-0042 coating.

Ormiston, T. J.↗

Dimensional stability of fused silica and several ultralow expansion materials

Description of a program of measurements of the dimensional stability of fused silica and several ultralow thermal expansion materials. The two techniques used are: (1) Fizeau interferometry employed by NBS-Corning, and (2) Fabry-Perot interferometry employed by the Optical Science Center, University of Arizona. In the latter, a measurement accuracy of one part in a billion is sought.

Jacobs, S. F.↗

Reflecting heat shields made of microstructured fused silica

Heat sheidls constructed from selected monodisperse distributions of high-purity fused-silica particles are efficient reflectors of visible and near-UV radiation generated in shock-layer of space probe during atmospheric entry.

Congdon, W. M.↗

Thermal conductivity measurements on Mullite and Silica REI for the Space Shuttle - Complementary guarded hot plate and radical outflow measurements

The materials studied are described along with the apparatus and the experimental techniques employed. The results of the measurements involving two REI Silica materials and a Mod 1 B REI Mullite are listed in a table. Measurements were conducted at unusually high temperature differences to detect 'shine-through' radiation transparency. Photographs are presented of the high-temperature guarded hot plate assembly.

Brazel, J. P.↗

Dimensional stability of fused silica, Invar, and several ultralow thermal expansion materials

A method is developed for testing the long-term dimensional stability of an iodine-stabilized He-Ne laser, using a technique whereby thermal expansion coefficients are measured by forming a Fabry-Perot etalon from the sample and monitoring the optical resonant frequencies with tunable sidebands impressed on a laser beam from a frequency-stabilized He-Ne laser. A change of 1 ppm over a 3-yr period on the part of fused silica dimensions and the differential thermal expansion of Invar LR-35 and Super Invar materials are noted. The method is of interest for the metrology of extremely stable structures such as telescopes and optical resonators.

Berthold, J. W., III↗

Entry into outer planet environments. I - The radiating shock layer with coupled ablation for carbon and silica

Fully coupled solutions of shock layer equations for the stagnation region are obtained, comprising a set of converged benchmark flowfield solutions for silica and carbon heat shields entering modeled atmospheres of Saturn and Uranus. Model atmospheres and entry trajectories providing significant radiative heating to the entry probes so that the heating environment and effects of mass addition on the heating environment are clearly defined are emphasized. Results referable to the carbon heat shield are questioned because of the high (sublimation) wall temperature assumed and the relatively low shock layer temperature.

Liu, C.-H.↗

Silica heat shield sizing

The sensitivity of silica heat shield requirements to gap width, tile edge radius, and heat transfer distribution within tile gaps was investigated. A two-dimensional thermal model was modified and used to determine the effect of two dimensional heat transfer distributions at high temperature reusable surface insulation edges on shuttle thermal protection system (TPS) requirements. The sensitivity of TPS requirements to coating thickness, emissivity, substructure thickness, and changes in gap heating for several locations on shuttle was also studied. An inverse solution technique was applied to temperature data obtained in the Ames 20 MW turbulent duct in order to examine the effect of tile edge radius on TPS requirements. The derived heating values were then used to predict TPS requirements. Results show that increasing tile radius reduces TPS requirements.

Ebbesmeyer, L. H.↗

High purity silica reflective heat shield development

Measurements were made of reflectance in the vacuum ultraviolet down to 0.15 micron. Scattering coefficients (S) and absorption coefficients (K) were also measured. These coefficients express the optical properties and are used directly in a thermodynamic analysis for sizing a heat shield. The effect of the thin silica melt layer formed during entry was also studied from the standpoint of trapped radiant energy.

Blome, J. C.↗

Temperature dependence of the absorption edge of vitreous silica

During an investigation of the optical properties of high-purity vitreous silica (fused quartz), which is being developed by NASA as a reflective and ablative heat shield, some interesting properties of theoretical and experimental nature have become apparent which otherwise may have remained unnoticed. Of particular interest for the NASA application is the shift of the absorption edge toward longer wavelengths with increasing temperature. The results of studies of this shift and of the spectral dependence of the absorption edge are summarized in the present paper. Plots of the absorption edge and the absorption spectrum of fused quartz vs temperature are given and discussed.

Bates, C. W., Jr.↗

Accelerated purification of colloidal silica sols

Accelerated purification process for colloidal sols using heat/deionization scheme, sharply reduces waiting time between deionization cycles from several months to a few days. Process produces same high purity silica sols as conventional methods.

Bahnsen, E. B.↗

The system anorthite-forsterite-fayalite-silica to 2 kbar with lunar petrologic applications

Near-liquidus phase relations in the magnesium-rich portion of the system anorthite-forsterite-fayalite-silica have been determined from synthesis experiments at 1 atm and 2 kbar at oxygen fugacities near the iron-wuestite buffer. The major-element chemistries of KREEP basalts are similar to peritectic liquids, L/ol,px,an/, produced experimentally. The reaction L/ol,px,an/ is well-located at low pressures. It intersects the join anorthite-enstatite-ferrosilite at Fe/(Fe+Mg) equals 0.45 (atomic ratio), and is peritectic only for Fe/(Fe+Mg) not greater than 0.45. Although positions of the equilibria, L/an,ol/ and L/ol,px/, differ significantly at 1 atm from their positions at 2 kbar, the position of the piercing point, L/ol,px,an/, on the anorthite-enstatite-ferrosilite join is not sensitive to pressure. The composition of liquids produced by partial melting of troctolites and pyroxenites in the lunar crustal environment will be affected by pressure, whereas liquids derived from gabbroic assemblages will not.

Merrill, R. B.↗

Opacified silica reusable surface insulation /RSI/ for thermal protection of the Space Shuttle Orbiter

A reusable surface insulation (RSI) material adopted for use on limited areas of the Orbiter's heat shield is described. The RSI is a rigid sintered fibrous silica material containing about 3% by weight of 1200-grit silicon carbide powder. RSI manufacture is described; strength characteristics and thermal conductivity of the final product can be tailored by controlling the isotropy, and the density, coefficient of thermal expansion, and specific heat are reported. Data establishing that opacification of RSI with silicon carbide lowers the thermal conductivity are presented.

Goldstein, H. E.↗