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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 163 records · Page 9

Computational Fluid Dynamics Models of the NASA White Sands Test Facility Particle Impact Test Nozzles

The particle impact ignition mechanism is considered to be the most effective means for igniting metals in gaseous oxygen environments and is a concern for every oxygen system. For this reason, the National Aeronautics and Space Administration (NASA) commits a large amount of resources attempting to understand and defend against this phenomenon. The most practical means of accomplishing this is through extensive of testing. To this end, over the years NASA has developed and built a facility and various apparatuses to test material or component vulnerability to a particle impact ignition. In testing materials, NASA uses sub-sonic and supersonic nozzles to replicate the conditions that a material is expected to experience in service. However, challenges include obtaining an understanding of the gas dynamics and of the particle behavior through and up to the point of impact at the material under test. One means of addressing these challenges is the use of computational fluid dynamics (CFD). If a CFD model can be built and validated, the model can then be used to confidently interrogate changes to inlet conditions and particle geometries, as well as changes to nozzle geometries to better simulate a material’s in-situ conditions and greatly reduce or eliminate trial-and-error approaches in testing. This paper will show NASA’s approach to and results of using CFD to better understand their particle impact nozzles.

Computational Fluid Dynamics↗

Thermal monitoring, measurement, and control system for a Volatile Condensable Materials (VCM) test apparatus

A thermal monitoring and control concept is described for a volatile condensable materials (VCM) test apparatus where electric resistance heaters are employed. The technique is computer based, but requires only proportioning ON/OFF relay control signals supplied through a programmable scanner and simple quadrac power controllers. System uniqueness is derived from automatic temperature measurements and the averaging of these measurements in discrete overlapping temperature zones. Overall control tolerance proves to be better than + or - 0.5 C from room ambient temperature to 150 C. Using precisely calibrated thermocouples, the method provides excellent temperature control of a small copper VCM heating plate at 125 + or - 0.2 C over a 24 hr test period. For purposes of unattended operation, the programmable computer/controller provides a continual data printout of system operation. Real time operator command is also provided for, as is automatic shutdown of the system and operator alarm in the event of malfunction.

Ives, R. E.↗

Seal material development test program

A program designed to characterize an experimental fluoroelastomer material designated AF-E-124D, is examined. Tests conducted include liquid nitrogen load compression tests, flexure tests and valve seal tests, ambient and elevated temperature compression set tests, and cleaning and flushing fluid exposure tests. The results of these tests indicate the AF-E-124D is a good choice for a cryogenic seal, since it exhibits good low temperature sealing characteristics and resistance to permanent set. The status of this material as an experimental fluorelastomer is stressed and recommended. Activity includes definition and control of critical processing to ensure consistent material properties. Design, fabrication and test of this and other materials is recommended in valve and static seal applications.

Source record↗

Analysis of PICA-NuSil at the Hypersonic Materials Environmental Test System (HyMETS)

Phenolic Impregnated Carbon Ablator (PICA) gained heritage during theStardust mission and is the baseline thermal protection system (TPS) material for missions to Mars. However, PICA is friable, so a thin layer of siloxane resin (NuSil) is applied to the surface of the heat shield to suppress the spread of particulate matter during cleanroom activities. Until recently, the thermochemical response of NuSil had not been accounted for in material response models. Therefore, a test campaign was executed at the Hypersonic Materials Environmental Test System (HyMETS) facility to investigate the material response of NuSil and provide crucial insight for model development. Finally, salient results from an experiment supported by the AsteroidThreat Assessment Project (ATAP) will be discussed, which probed the materialr esponse of the Tamdakht meteorite and notable analogs.

Brody K. Bessire↗

Notch sensitivity of space shuttle tile materials

Tests were conducted at room temperature to determine the notch sensitivity of the thermal protection tile for the space shuttle. Two types of RSI tile were studied: LI-900 and LI-2200. Three point bend specimens were cut from discarded tiles in the in-plane (ip) and through-the-thickness (ttt) directions. They were tested with or without a sharp notch. The LI-900 (ip and ttt) specimens were not very notch sensitive, but the LI-2200 (ip and ttt) specimens were. The LI-2200 material showed about a 35 percent reduction in strength due to the presence of the notch. This reduction in strength should be considered in the design of mechanically fastened tile concepts.

Newman, J. C., Jr.↗

Materials, processes, and environmental engineering network

The Materials, Processes, and Environmental Engineering Network (MPEEN) was developed as a central holding facility for materials testing information generated by the Materials and Processes Laboratory. It contains information from other NASA centers and outside agencies, and also includes the NASA Environmental Information System (NEIS) and Failure Analysis Information System (FAIS) data. Environmental replacement materials information is a newly developed focus of MPEEN. This database is the NASA Environmental Information System, NEIS, which is accessible through MPEEN. Environmental concerns are addressed regarding materials identified by the NASA Operational Environment Team, NOET, to be hazardous to the environment. An environmental replacement technology database is contained within NEIS. Environmental concerns about materials are identified by NOET, and control or replacement strategies are formed. This database also contains the usage and performance characteristics of these hazardous materials. In addition to addressing environmental concerns, MPEEN contains one of the largest materials databases in the world. Over 600 users access this network on a daily basis. There is information available on failure analysis, metals and nonmetals testing, materials properties, standard and commercial parts, foreign alloy cross-reference, Long Duration Exposure Facility (LDEF) data, and Materials and Processes Selection List data.

White, Margo M.↗

Investigations of the Deterioration of 22 Refractory Materials in a Mach Number 2 Jet at a Stagnation Temperature of 3,800 F

A limited investigation of the deterioration characteristics of 22 refractory materials was conducted by exposing them to a stagnation temperature of 3,800 F in a Mach number 2 ceramic-heated jet at the Langley Research Center. The materials tested were six materials whose major constituent was silicon carbide, five cermets whose major constituent was titanium carbide, six materials whose major constituents were metal borides, four cermets containing alumina, and one silicon nitride model. Tests consisted of obtaining weight change and appearance changes for 1/2-inch-diameter hemispherical-nose cylindrical models exposed to the air jet for 30 seconds at a time for a total of four runs or 2 minutes exposure. Curves of weight changes plotted against the number of 30-second tests in the jet were obtained. Estimates of average surface temperature near the stagnation point of the model were obtained by use of a special temperature-measuring camera. The models were examined before and after the completion of the tests for possible changes in microstructure; no significant changes were found. The data obtained were analyzed with the view that the oxidation characteristics of the materials were the main factor in deterioration of the materials under the conditions of the tests. It was concluded that only those materials which changed in weight the least could be recommended for further extensive application-oriented evaluations. The following materials fell in this category: silicon carbide - silicon, chromium - 28-percent alumina cermet, titanium boride - 5-percent boron carbide. The remainder of the materials tested had oxidation characteristics which appeared to be too severely limiting of their general applications to flight vehicles.

Lewis, B. W.↗

Ultrasonic Studies of Composites Undergoing Thermal and Fatigue Loading

New composite materials possess attractive properties for use in advanced aircraft. A necessary requirement for their introduction into aeronautic use is an accurate understanding of their long term aging processes so that proper design criteria can be established. In order to understand those properties, these composites must be exposed to thermal and load cycles that are characteristic of flight conditions. Additionally, airline companies will require nondestructive evaluation (NDE) methods that can be used in the field to assess the condition of these new materials as they age. As part of an effort to obtain the required information about new composites for aviation use, we are performing ultrasonic measurements both in the NDE laboratory and in the materials testing laboratory at NASA. The materials testing laboratory is equipped with environmental chambers mounted on load frames so that composite samples can be exposed to thermal and loading cycles representative of flight protocols. Applying both temperature and load simultaneously will help to highlight temperature and load interactions during the aging of these composite materials. This study reports on our initial ultrasonic attenuation results from thermoset and thermoplastic composite samples. Ultrasonic attenuation measurements have been used reliably to assess the effects of material degradation. For example, recently, researchers have shown that by using frequencies of ultrasound on the order of 24 MHz, they could obtain adequate contrast in the evaluation of thermal degradation in these composites. This paper will present data that shows results at a lower frequency range. In addition, we report results on the frequency dependence of attenuation as the slope of attenuation with respect to frequency, beta = delta alpha (f) / delta f. The slope of attenuation is an attractive parameter since it is quantitative, yet does not require interface corrections like conventional quantitative attenuation measurements. This is a consequence of the assumption that interface correction terms are frequently independent. Uncertainty in those corrections terms compromises the value of conventional quantitative attenuation data.

Madaras, Eric I.↗

Impact Testing for Materials Science at NASA - MSFC

The Impact Testing Facility (ITF) at NASA - Marshall Space Flight Center is host to different types of guns used to study the effects of high velocity impacts. The testing facility has been and continues to be utilized for all NASA missions where impact testing is essential. The Facility has also performed tests for the Department of Defense, other corporations, as well as universities across the nation. Current capabilities provided by Marshall include ballistic guns, light gas guns, exploding wire gun, and the Hydrometeor Impact Gun. A new plasma gun has also been developed which would be able to propel particles at velocities of 20km/s. This report includes some of the guns used for impact testing at NASA Marshall and their capabilities.

Sikapizye, Mitch↗

The MECA Payload as an Exobiology Laboratory on the MSP 2001 Lander

The "Mars Environmental Compatibility Assessment" (MECA) payload for Mars Surveyor Project 2001 (MSP 2001) is comprised of a multifunctional laboratory equipped to assess martian soil properties with wet chemistry, camera imagery, optical microscopy (potentially with UV fluorescence capability), atomic force microscopy (AFM; potentially with mineral-discrimination capabilities), electrometry, active & passive external materials-test panels, mineral hardness testing, and electrostatic and magnetic materials testing. Additionally, evaluation of soil chemical and physical properties as a function of depth down to -50 cm will be facilitated by the Lander/MECA robot arm on which the camera (RAC) and electrometer are mounted. MECA was designed as a NASA Human Exploration and Development of Space (HEDS) payload for determining the properties of martian soil that may be detrimental to human exploration. It is, however, well equipped to address exobiology questions in the following areas: (1)Geochemical clues to Aqueous Mineralogy and Oxidant formation; (2) Soil structures and microfabrics as indicators of water-volatiles migration; (3) Minerals and rocks as clues to ancient hydrology; (4) Grain textures as indicators of aqueous activity and weathering. Additional information is contained in the original.

Marshall, J.↗

Investigation of Test Methods, Material Properties and Processes for Solar Cell Encapsulants

The evaluation of potentially useful low cost encapsulation materials is discussed. The goal is to identify, evaluate, test and recommend encapsulant materials and processes for the production of cost effective, long life solar cell modules. Technical investigations concerned the development of advanced cure chemistries for lamination type pottants; the continued evaluation of soil resistant surface treatment, and the results of an accelerated aging test program for the comparison of material stabilities. New compounds were evaluated for efficiency in curing both ethylene/vinyl acetate and ethylene/methyl acrylate pottants intended for vacuum bag lamination of solar cells. Two component aliphatic urethane casting syrups were evaluated for suitability as solar module pottants on the basis of optical, physical and fabrication characteristics.

Willis, P.↗

Quick release acoustic sensor holding fixture

Quick-release spring holder secures acoustic sensor to test material surface eliminating adhesive bonding to test material and achieving acoustic emission evaluation from tensile tests. Reusability of sensors reduces test cost.

Mcmahon, W.↗

GRC MILab Software: Quick Start Guide

This document provides detailed installation and operating instructions for the GRC MILab Excel Add-In software developed at the NASA Glenn Research Center. The software described has been implemented to facilitate the process of importing into Microsoft Excel and analyzing materials test data from a wide range of materials tests. All resulting data is then ready for automated upload to the relevant table of the GRC Materials Intelligence (MI) database. This new software represents an update to the original MILab software developed by Granta Design Ltd.—a company specializing in materials software, data, and databases—for members of the Materials Data Management Consortium (MDMC), a collaboration between Granta, ASM International, NASA Glenn, and several other materials-oriented corporations and government agencies in the aerospace and defense industries. The updated software consists of the addition of two test type modules, the Generic and Generic Cyclic modules, with both representing a generalization of the original software. The Generic module supports the import and analysis of multiaxial data from any sequence of tensile, compression, relaxation, and/or creep test stages; and the Generic Cyclic module expands the functionality to include repeated sequences during cyclic testing. During processing, all imported data and analysis results are formatted by the software so as to be ready for immediate automated upload to the MI database, ensuring minimal overhead on the part of the user and access to persistent and reliable data for all relevant personnel.

Quick Start Guide↗

Nitric Oxide PLIF Measurements in the Hypersonic Materials Environmental Test System (HYMETS)

A nonintrusive laser-based measurement system has been applied for the first time in the HYMETS (Hypersonic Materials Environmental Test System) 400 kW arc-heated wind tunnel at NASA Langley Research Center. Planar laser-induced fluorescence of naturally occurring nitric oxide (NO) has been used to obtain instantaneous flow visualization images, and to make both radial and axial velocity measurements. Results are presented at selected facility run conditions, including some in simulated Earth atmosphere (75% nitrogen, 20% oxygen, 5% argon) and others in simulated Martian atmosphere (71% carbon dioxide, 24% nitrogen, 5% argon), for bulk enthalpies ranging from 6.5 MJ/kg to 18.4 MJ/kg. Flow visualization images reveal the presence of large scale unsteady flow structures, and indicate nitric oxide fluorescence signal over more than 70% of the core flow for bulk enthalpies below about 11 MJ/kg, but over less than 10% of the core flow for bulk enthalpies above about 16 MJ/kg. Axial velocimetry was performed using molecular tagging velocimetry (MTV). Axial velocities of about 3 km/s were measured along the centerline. Radial velocimetry was performed by scanning the wavelength of the narrowband laser and analyzing the resulting Doppler shift. Radial velocities of 0.5km/s were measured.

Inman, Jennifer A.↗

Analysis of PICA-NuSil at the Hypersonic Materials Environmental Test System (HyMETS)

Phenolic Impregnated Carbon Ablator (PICA) gained heritage during the stardust mission and is the baseline material for missions to Mars. The phenolic phase of PICA is friable, and therefore the surface is treated with a siloxane resin (NuSil) to mitigate the shedding of particulate matter. Historically, material response models have not accounted for the presence of this coating. Therefore, a test campaign was executed at the Hypersonic Materials Environmental Test System (HyMETS) to investigate the performance of NuSil under multiple heating rates and gas composition. Sphere-cone models were instrumented with thermocouples to measure the in-depth temperature response, and surface temperatures were monitored with a pyrometer. Furthermore, emission spectrometers were used to collect spectra from species emitting at the surface of the test article and the post-shock stagnation region. Post-test analysis suggests that the coating decomposes according to multiple stages. Inspection of silicon emission data reveals a rapid rise and decline in intensity within the first couple of seconds of testing, which is attributed to pyrolysis of NuSil. Pyrolysis is followed by a stagnation in silicon emission and surface temperature which are attributed to the formation of a thin layer of oxidation-resistant silicon oxycarbide. Moreover, the presence of the silicon oxycarbide layer significantly reduces the in-depth thermal response when compared to the baseline material. Eventually, the silicon oxycarbide layer decomposes via high-temperature reactions, which expose the underlying char layer to a highly reactive flow.

PICA-NuSil↗

Simultaneous Laser-induced Fluorescence of Nitric Oxide and Atomic Oxygen in the Hypersonic Materials Environment Test System Arcjet Facility

Simultaneous nitric oxide (NO) and atomic oxygen (O) laser induced fluorescence (LIF) experiments were performed in the Hypersonic Materials Environmental Test System (HYMETS) facility at the NASA Langley Research Center. The data serves as an experimental database for validation for chemical and thermal nonequilibrium models used in hypersonic flows. Measurements were taken over a wide range of stagnation enthalpies (6.7 - 18.5 MJ/kg) using an Earth atmosphere simulant with a composition of 75% N2, 20% O2, and 5% Ar (by volume). These are the first simultaneous measurements of NO and O LIF to be reported in literature for the HYMETS facility. The maximum O LIF mean signal intensity was observed at a stagnation enthalpy of approximately 12 MJ/kg while the maximum NO LIF mean signal intensity was observed at a stagnation enthalpy of 6.7 MJ/kg. Experimental results were compared to simple fluorescence model that assumes equilibrium conditions in the plenum and frozen chemistry in the isentropic nozzle expansion (Mach 5). The equilibrium calculations were performed using CANTERA v2.1.1 with 16 species. The fluorescence model captured the correlation in mean O and NO LIF signal intensities over the entire range of stagnation enthalpies tested. Very weak correlations between single-shot O and NO LIF intensities were observed in the experiments at all of the stagnation enthalpy conditions.

Johansen, Craig↗

NASA Glenn Research Center Support of the ASRG Project

A high efficiency radioisotope power system is being developed for long-duration NASA space science missions. The U.S. Department of Energy (DOE) managed a flight contract with Lockheed Martin Space Systems Company (LMSSC) to build Advanced Stirling Radioisotope Generators (ASRGs), with support from NASA Glenn Research Center (GRC). Sunpower Inc. held two parallel contracts to produce Advanced Stirling Convertors (ASCs), one with DOELockheed Martin to produce ASC-F flight units, and one with GRC for the production of ASC-E3 engineering unit pathfinders that are built to the flight design. In support of those contracts, GRC provided testing, materials expertise, government furnished equipment, inspections, and related data products to DOELockheed Martin and Sunpower. The technical support includes material evaluations, component tests, convertor characterization, and technology transfer. Material evaluations and component tests have been performed on various ASC components in order to assess potential life-limiting mechanisms and provide data for reliability models. Convertor level tests have been used to characterize performance under operating conditions that are representative of various mission conditions. Technology transfers enhanced contractor capabilities for specialized production processes and tests. Despite termination of flight ASRG contract, NASA continues to develop the high efficiency ASC conversion technology under the ASC-E3 contract. This paper describes key government furnished services performed for ASRG and future tests used to provide data for ongoing reliability assessments.

Technology Transfer↗