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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 163 records · Page 9
All sourcesNASA NTRSDOE OSTI
NASA NTRS2006

A Silent Safety Program

NASA's Columbia Accident Investigation Board (CAIB) referred 8 times to the NASA "Silent Safety Program." This term, "Silent Safety Program" was not an original observation but first appeared in the Rogers Commission's Investigation of the Challenger Mishap. The CAIB on page 183 of its report in the paragraph titled 'Encouraging Minority Opinion,' stated "The Naval Reactor Program encourages minority opinions and "bad news." Leaders continually emphasize that when no minority opinions are present, the responsibility for a thorough and critical examination falls to management. . . Board interviews revealed that it is difficult for minority and dissenting opinions to percolate up through the agency's hierarchy. . ." The first question and perhaps the only question is - what is a silent safety program? Well, a silent safety program may be the same as the dog that didn't bark in Sherlock Holmes' "Adventure of the Silver Blaze" because system safety should behave as a devil's advocate for the program barking on every occasion to insure a critical review inclusion. This paper evaluates the NASA safety program and provides suggestions to prevent the recurrence of the silent safety program alluded to in the Challenger Mishap Investigation. Specifically targeted in the CAM report, "The checks and balances the safety system was meant to provide were not working." A silent system safety program is not unique to NASA but could emerge in any and every organization. Principles developed by Irving Janis in his book, Groupthink, listed criteria used to evaluate an organization's cultural attributes that allows a silent safety program to evolve. If evidence validates Jams's criteria, then Jams's recommendations for preventing groupthink can also be used to improve a critical evaluation and thus prevent the development of a silent safety program.

Goodin, James Ronald↗
NASA NTRS2019

Advanced Colloids Experiment (Temperature Controlled) – ACE-T5

The attached will be presented at the JSC Science Symposium as a preview of the ACE-T5 flight experiment. The Principal Investigator (PI) for this experiment is Professor Ali Mohraz at the University of California - Irvine.Bijels (bicontinuous interfacially jammed emulsion gels) were discovered in 2007 at the University of Edinburgh. These materials feature a tubular, bicontinuous arrangement of two fluid phases separated by a monolayer of jammed colloidal particles at the interface.Because of their unique morphological characteristics, bijels hold significant promise as next-generation materials for energy and biotechnology applications. But in order to fully realize their potential, their physics and mechanical properties must be better understood. The mechanical properties and stability of bijels is mediated by an interplay between interfacial forces that impart elasticity to the system, and external stresses. Unfortunately, the interfacial forces are inherently coupled with density differences and cannot be studied systematically in the presence of gravity.

Mohraz, Ali↗
NASA NTRS2019

Mechanical Design and Configuration of Penetrations for the Europa Clipper Avionics Vault Structure

The main purpose of the Avionics Vault is to shield radiation sensitive electronics for the Europa Clipper Spacecraft. The vault is a box structure made out of aluminum panels. The panels are roughly 10 mm thick in order to shield the electronics from the orbital total ionizing radiation around Jupiter. The vault requires an electromagnetic interference (EMI) shielding effectiveness (SE) of at least 70 dB in order to mitigate EMI with the spacecraft radar receiver. Overall, the vault accommodates four main types of penetrations: receptacle connectors, pass-through cables, fluid lines, and vent holes. More than 150 cables penetrate the vault panels to connect to electronic boxes inside. Fluid pipes enter and exit the vault to transfer heat to the rest of the spacecraft. Vent holes provide a path for air to escape from the vault during launch. Several novel penetrations designs were created to meet EMI and radiation shielding requirements. Receptacle connectors interface to the vault panels using 1.3 mm thick Ta10W plates. Pass-through cables penetrate the vault using aluminum clamshells after being wrapped with Teflon cushion tape, Kapton tape, and copper tape. Vent hole penetrations consist of a copper mesh for EMI shielding and an aluminum radiation shield bracket to direct air out of the vault during launch. Fluid lines terminate at the vault wall using mechanical fittings that resemble a nut and bolt interface. In addition, most mechanical seams and penetrations utilize EMI gaskets to ensure proper EMI shielding. To reduce risk and confirm that the vault penetration designs were appropriate for EMI shielding, an EMI chamber at the Jet Propulsion Laboratory (JPL) was used to test a mock-up vault panel with multiple variations of all four main types of vault penetrations. This EMI SE test also incorporated different methods for bundling pass-through cables, and a comparison of flange mounted connectors versus jam nut connectors. A low noise preamplifier and a Rohde & Schwarz spectrum analyzer measured E-field levels transmitting through the mock-up vault panel. The results showed a shielding effectiveness of 77 dB for the mock-up vault panel, which exceeds the 70 dB target for Europa Clipper. Both the flange mounted connectors and jam nut connectors exhibited similar EMI SE results at the measured frequencies, and all variations of vault penetrations showed favorable EMI SE levels. Since the flight panels will be much larger and include many more penetrations, there will be testing of the flight vault to confirm its EMI SE is compliant with environmental requirements.

Giersch, Louis↗
NASA NTRS2020

Design and Development of a Robust Chuck Mechanism for the Mars2020 Coring Drill

The Sampling and Caching Subsystem (SCS) onboard the Mars2020 rover includes a coring drill that can perform coring, abrasion, and regolith collection operations. The coring drill requires a chuck mechanism to allow for the changing of the bits needed to perform sampling. The chuck mechanism must be capable of securely connecting a bit under drilling, rover slip, and pullout loads, but also readily release a bit after application of these loads. The Mars2020 chuck consists of a ball lock mechanism that allows for robust engagement and release of bit assemblies that is preloaded to ensure a secure, stiff connection between the bit assembly and the rest of the corer. To prevent jamming, the chuck incorporates rollers to preload the ball lock. The rollers are mounted onto a flexured cam that minimizes changes in internal mechanism loads that result from thermally induced dimensional changes, further mitigating the potential for jamming. The chuck mechanism is moved between engaged, disengaged, and loose chuck positions by rotating the cam with a gearmotor that incorporates a magnetic detent brake that prevents inadvertent mechanism motion under design loads. Ongoing testing is occurring on the qualification model in a dirty environment while coring and abrading rocks in a Mars representative environment.

Barletta, Anthony↗
DOE OSTI2017

Transmit-reference methods in software defined radio platforms for communication in harsh propagation environments and systems thereof

A method for adaptive Radio Frequency (RF) jamming according to one embodiment includes dynamically monitoring a RF spectrum; detecting any undesired signals in real time from the RF spectrum; and sending a directional countermeasure signal to jam the undesired signals. A method for adaptive Radio Frequency (RF) communications according to another embodiment includes transmitting a data pulse in a RF spectrum; and transmitting a reference pulse separated by a predetermined period of time from the data pulse; wherein the data pulse is modulated with data, wherein the reference pulse is unmodulated. A method for adaptive Radio Frequency (RF) communications according to yet another embodiment includes receiving a data pulse in a RF spectrum; and receiving a reference pulse separated in time from the data pulse, wherein the data pulse is modulated with data, wherein the reference pulse is unmodulated; and demodulating the pulses.

42 ENGINEERING↗
DOE OSTI2021

Computational Fluid Dynamics Simulation of Compressible Non-Newtonian Biomass in a Compression-Screw Feeder

Compression-screw feeders play a critical role in biorefineries to transport lignocellulosic biomass feedstocks from the feeding hoppers to biomass-conversion reactors in order to pretreat and convert biomass to hydrocarbon liquid biofuels and other power and energy resources. One of the main challenges in the operation of screw feeder is plugging and jamming of compressed biomass with high concentration of insoluble solids. The focus of this paper is to numerically investigate the screw feeder at these challenging operating conditions and help with the optimization of the screw feeder design to avoid operation failure. In this work a customized CFD model based on open-source OpenFOAM package [1] was developed to simulate the concentrated biomass as a highly viscous non-Newtonian fluid in the screw feeder. The biomass is modeled as a single-phase compressible Bingham fluid with a plastic viscosity as well as a density-dependent yield stress. The compressibility formulation (pressure-dependent density) and the density-dependent yield stress formulation in the governing equations follow the suggestions from a recent study by Duncan et al. [2]. A pilot-scale hopper/screw feeding system at NREL [3] is used to compare the experimental observations with our simulation results. The auger is 280 mm long and tapered with outer diameter changing from 80 mm to 35 mm. The auger rotates from 10 to 60 rpm in a conical throat which contains anti-rotational bars. The simulations predicted the required torque for the screw feeder and the pressure increase at the exit for biomass feedstocks with various fluid viscosity properties and auger rotating speeds. The analysis of the stress forces helped to identify the critical conditions were the screw feeder excessive wear or jamming could occur.

biofuels↗
DOE OSTI2023

Amphiphilic Heterografted Molecular Bottlebrushes with Tertiary Amine-Containing Side Chains as Efficient and Robust pH-Responsive Emulsifiers

Here, by combining the unique characteristics of molecular bottlebrushes (MBBs) and the properties of stimuli-responsive polymers, we show that MBBs with randomly grafted poly(n-butyl acrylate) and pH-responsive poly(2-(N,N-diethylamino)ethyl methacrylate) (PDEAEMA) side chains are efficient and robust pH-responsive emulsifiers. Water-in-toluene emulsions were formed at pH 4.0 and disrupted by increasing the pH to 10.0. The emulsion generation and disruption was reversible over the ten cycles investigated, and the bottlebrushes remained intact. The exceptional emulsion stability stemmed from the high interfacial binding energy of MBBs, imparted by their large molecular size and Janus architecture at the interface, as evidenced by the interfacial jamming and wrinkling of the assemblies upon reducing the interfacial area. At pH 10.0, PDEAEMA became water-insoluble, and the MBBs desorbed from the interface, causing de-emulsification. Consequently, we have shown that the judicious design of MBBs can generate properties of particle emulsifiers from their large size, while the responsiveness of the MBBs enables more potential applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Transient learning degrees of freedom for introducing function in materials

Significance Many protocols used in material design and training have a common theme: they introduce new degrees of freedom, often by relaxing away existing constraints, and then evolve these degrees of freedom based on a rule that leads the material to a desired state at which point these new degrees of freedom are frozen out. By creating a unifying framework for these protocols, we can now understand that some protocols work better than others because the choice of new degrees of freedom matters. For instance, introducing particle sizes as degrees of freedom to the minimization of a jammed particle packing can lead to a highly stable state, whereas particle stiffnesses do not have nearly the same impact.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Open millifluidics based on powder-encased channels

Millifluidics, the manipulation of liquid flow in millimeter-sized channels, has been a revolutionary concept in chemical processing and engineering. The solid channels that contain the liquids, though, are not flexible in their design and modification, and prevent contact with the external environment. All-liquid constructs, on the other hand, while flexible and open, are imbedded in a liquid environment. Here, we provide a route to circumvent these limitations by encasing the liquids in a hydrophobic powder in air that jams on the surface, containing and isolating flowing fluids, offering flexibility and adaptability in design, as manifest in the ability to reconfigure, graft, and segment the constructs. Along with the open nature of these powder-contained channels that allow arbitrary connections/disconnections and substance addition/extraction, numerous applications can be opened in the biological, chemical, and material arenas.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Aerobijels: Ultralight Carbon Monoliths from Cocontinuous Emulsions

In this work, bijels are used to develop a new class of ultralight hierarchically porous aerogels exhibiting multimodal porosity across multiple length scales. Through in situ functionalization of a particle-laden liquid interface wherein binary liquid pairs are kinetically trapped out of equilibrium through interfacial jamming, monolithic and freestanding carbon electrodes are produced with prescribed bulk densities down to ≈2 mg cm -3 . Exemplary electrokinetic experiments indicate that the bicontinuity of the pore structure is essential for enhancing transport to and from the active electrode surfaces, demonstrating that these materials possess a superior ability to accumulate and transport charge when compared to analogous systems with restricted pore connectivity and fluid throughput. This approach offers a new synthetic route to bicontinuous and hierarchical aerogel materials with nested multimodal porosities. Furthermore, the flexibility of this scheme can address critical issues related to transport-limited behaviors that arise in many technological fields, ranging from energy and catalysis research to remediation and sensing applications.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Liquid Letters

Abstract Using the interfacial jamming of cellulose nanocrystal (CNC) surfactants, a new concept, termed all‐liquid molding, is introduced to produce all‐liquid objects that retain the shape and details of the mold with high fidelity, yet remain all liquid and are responsive to external stimuli. This simple process, where the viscosity of the CNC dispersion can range from that of water to a crosslinked gel, opens tremendous opportunities for encapsulation, delivery systems, and unique microfluidic devices. The process described is generally applicable to any functionalized nanoparticles dispersed in one liquid and polymer ligands having complementary functionality dissolved in a second immiscible liquid. Such sculpted liquids retain all the characteristics of the liquids but retain shape indefinitely, very much like a solid, and provide a new platform for next‐generation soft materials.

Shi, Shaowei↗
DOE OSTI2018

Reconfigurable Printed Liquids

Abstract Liquids lack the spatial order required for advanced functionality. Interfacial assemblies of colloids, however, can be used to shape liquids into complex, 3D objects, simultaneously forming 2D layers with novel magnetic, plasmonic, or structural properties. Fully exploiting all‐liquid systems that are structured by their interfaces would create a new class of biomimetic, reconfigurable, and responsive materials. Here, printed constructs of water in oil are presented. Both form and function are given to the system by the assembly and jamming of nanoparticle surfactants, formed from the interfacial interaction of nanoparticles and amphiphilic polymers that bear complementary functional groups. These yield dissipative constructs that exhibit a compartmentalized response to chemical cues. Potential applications include biphasic reaction vessels, liquid electronics, novel media for the encapsulation of cells and active matter, and dynamic constructs that both alter, and are altered by, their external environment.

Forth, Joe↗
DOE OSTI2023

Reconfigurable Magnetic Liquid Building Blocks for Constructing Artificial Spinal Column Tissues

All-liquid molding can be used to transform a liquid into free-form solid constructs, while maintaining internal fluidity. Traditional biological scaffolds, such as cured pre-gels, are normally processed in solid state, sacrificing flowability and permeability. However, it is essential to maintain the fluidity of the scaffold to truly mimic the complexity and heterogeneity of natural human tissues. Here, this work molds an aqueous biomaterial ink into liquid building blocks with rigid shapes while preserving internal fluidity. The molded ink blocks for bone-like vertebrae and cartilaginous-intervertebral-disc shapes, are magnetically manipulated to assemble into hierarchical structures as a scaffold for subsequent spinal column tissue growth. It is also possible to join separate ink blocks by interfacial coalescence, different from bridging solid blocks by interfacial fixation. Generally, aqueous biomaterial inks are molded into shapes with high fidelity by the interfacial jamming of alginate surfactants. The molded liquid blocks can be reconfigured using induced magnetic dipoles, that dictated the magnetic assembly behavior of liquid blocks. The implanted spinal column tissue exhibits a biocompatibility based on in vitro seeding and in vivo cultivating results, showing potential physiological function such as bending of the spinal column.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2020

Periodic Porous 3D Electrodes Mitigate Gas Bubble Traffic during Alkaline Water Electrolysis at High Current Densities

We report alkaline water electrolysis at high current densities is plagued by gas bubble generation and trapping in stochastic porous electrodes (e.g., Ni foams), which causes a significant reduction in the number of electrolyte accessible catalyst active sites. Here, 3D printed Ni (3DPNi) electrodes with highly controlled, periodic structures are reported that suppress gas bubble coalescence, jamming, and trapping and, hence, result in rapid bubble release. The 3DPNi electrodes decorated with carbon-doped NiO achieve a high current density of 1000 mA cm -2 in 1.0 m KOH electrolyte at hydrogen evolution reaction and oxygen evolution reaction overpotentials of 245 and 425 mV, respectively. This work demonstrates a new approach to the deterministic design of 3D electrodes to facilitate rapid bubble transport and release to enhance the total electrode catalytic activity at commercially relevant current densities.

08 HYDROGEN↗
DOE OSTI2019

Interfacial Activity of Amine‐Functionalized Polyhedral Oligomeric Silsesquioxanes (POSS): A Simple Strategy To Structure Liquids

Abstract Amine‐functionalized polyhedral oligomeric silsesquioxane (POSS), the smallest, monodisperse cage‐shaped silica cubic nanoparticle, is exceptionally interfacially active and can form assemblies that jam the toluene/water interface, locking in non‐equilibrium shapes of one liquid phase in another. The packing density of the amine‐functionalized POSS assembly at the water/toluene interface can be tuned by varying the concentration, the pH value, and the degree of POSS functionalization. Functionalized POSS gives a higher interface coverage, and hence a lower interfacial tension, than nanoparticle surfactants formed by interactions between functionalized nanoparticles and polymeric ligands. Hydrogen‐bonded POSS surfactants are more stable at the interface, offering some unique advantages for generating Pickering emulsions over typical micron‐sized colloidal particles and ligand‐stabilized nanoparticle surfactants.

Hou, Honghao↗
DOE OSTI2022

Polyoxometalate‐Surfactant Assemblies: Responsiveness to Orthogonal Stimuli

Abstract Integrating different types of supramolecular interactions opens the possibility to generate nanoparticle surfactants (NPSs) at the liquid–liquid interface that are responsive to multiple stimuli. Here we develop a covalently modified polyoxometalate/β‐cyclodextrin (POM/β‐CD) organic–inorganic hybrid, consisting of a negatively charged POM cluster with β‐CD host groups. The POM/β‐CD hybrid can be dispersed in water and interacts at a water/oil interface with ligands dissolved in an oil phase through electrostatic or host–guest interactions, thereby generating POM‐surfactants (POMSs) having pH, redox, and guest‐competitive responsiveness, respectively. By taking advantage of the jamming of POMSs at the interface, a reconfigurable all‐liquid system could be produced that is responsive to orthogonal changes in the external environment.

Xia, Zhiqin↗
DOE OSTI2023

Using Aggregation to Chaperone Nanoparticles Across Fluid Interfaces

Abstract Nanoparticles (NPs) transfer is usually induced by adding ligands to modify NP surfaces, but aggregation of NPs oftentimes hampers the transfer. Here, we show that aggregation during NP phase transfer does not necessarily result in transfer failure. Using a model system comprising gold NPs and amphiphilic polymers, we demonstrate an unusual mechanism by which NPs can undergo phase transfer from the aqueous phase to the organic phase via a single‐aggregation‐single pathway. Our discovery challenges the conventional idea that aggregation inhibits NP transfer and provides an unexpected pathway for transferring larger‐sized NPs (>20 nm). The charged amphiphilic polymers effectively act as chaperons for the NP transfer and offer a unique way to manipulate the dispersion and distribution of NPs in two immiscible liquids. Moreover, by intentionally jamming the NP‐polymer assembly at the liquid/liquid interface, the transfer process can be inhibited.

Fu, Yuchen↗
DOE OSTI2019

Interfacial Activity of Amine-Functionalized Polyhedral Oligomeric Silsesquioxanes (POSS): A Simple Strategy To Structure Liquids

Amine-functionalized polyhedral oligomeric silsesquioxane (POSS), the smallest, monodisperse cage-shaped silica cubic nanoparticle, is exceptionally interfacially active and can form assemblies that jam the toluene/water interface, locking in non-equilibrium shapes of one liquid phase in another. The packing density of the amine-functionalized POSS assembly at the water/toluene interface can be tuned by varying the concentration, the pH value, and the degree of POSS functionalization. Functionalized POSS gives a higher interface coverage, and hence a lower interfacial tension, than nanoparticle surfactants formed by interactions between functionalized nanoparticles and polymeric ligands. Here, hydrogen-bonded POSS surfactants are more stable at the interface, offering some unique advantages for generating Pickering emulsions over typical micron-sized colloidal particles and ligand-stabilized nanoparticle surfactants.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗