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At least 163 records · Page 9

High-toughness graphite/epoxy composite material experiment

The experiment was designed to measure the effect of near-space exposure on mechanical properties of specially toughened 5208/T300 graphite-epoxy composites. The properties measured are elastic modulus, strength, and fracture toughness. Specimens were mounted on an external frame during the time of the LDEF mission. Specimen variables include angle of adjacent plies and fraction of interlaminar contact, which is controlled by the fraction of finely spaced holes in Mylar film placed between the prepreg monolayers of the composite.

Felbeck, David K.↗

Mechanical properties of triaxially braided composites: Experimental and analytical results

This paper investigates the unnotched tensile properties of two-dimensional triaxial braid reinforced composites from both an experimental and analytical viewpoint. The materials are graphite fibers in an epoxy matrix. Three different reinforcing fiber architectures were considered. Specimens were cut from resin transfer molded (RTM) composite panels made from each braid. There were considerable differences in the observed elastic constants from different size strain gage and extensometer readings. Larger strain gages gave more consistent results and correlated better with the extensometer readings. Experimental strains correlated reasonably well with analytical predictions in the longitudinal, zero degree, fiber direction but not in the transverse direction. Tensile strength results were not always predictable even in reinforcing directions. Minor changes in braid geometry led to disproportionate strength variations. The unit cell structure of the triaxial braid was discussed with the assistence of computer analysis of the microgeometry. Photomicrographs of the braid geometry were used to improve upon the computer graphics representations of unit cells. These unit cells were used to predict the elastic moduli with various degrees of sophistication. The simple and the complex analyses were generally in agreement but none adequately matched the experimental results for all the braids.

Masters, John E.↗

Effect of space environment on composite materials and thermal coatings (A0138-9)

This paper presents an experiment within the FRECOPA project on composite materials, adhesives, and thermal coatings. The aging of the specimens was limited because of the canister closing, the location on the trailing edge and the arrangement of the specimens inside the canister. The results show no evidence of change for several graphite fiber reinforced epoxy matrix composite materials as well as for two adhesives. Minor changes can be found on some second surface mirrors.

Parcelier, Michel↗

Mechanical properties of triaxially braided composites: Experimental and analytical results

The unnotched tensile properties of 2-D triaxial braid reinforced composites from both an experimental and an analytical viewpoint are studied. The materials are graphite fibers in an epoxy matrix. Three different reinforcing fiber architectures were considered. Specimens were cut from resin transfer molded (RTM) composite panels made from each braid. There were considerable differences in the observed elastic constants from different size strain gage and extensometer reading. Larger strain gages gave more consistent results and correlated better with the extensometer reading. Experimental strains correlated reasonably well with analytical predictions in the longitudinal, 0 degrees, fiber direction but not in the transverse direction. Tensile strength results were not always predictable even in reinforcing directions. Minor changes in braid geometry led to disproportionate strength variations. The unit cell structure of the triaxial braid was discussed with the assistance of computer analysis of the microgeometry. Photomicrographs of braid geometry were used to improve upon the computer graphics representations of unit cells. These unit cells were used to predict the elastic moduli with various degrees of sophistication. The simple and the complex analyses were generally in agreement but none adequately matched the experimental results for all the braids.

Masters, John E.↗

Graphite fiber reinforced thermoplastic resins

The results of a program designed to optimize the fabrication procedures for graphite thermoplastic composites are described. The properties of the composites as a function of temperature were measured and graphite thermoplastic fan exit guide vanes were fabricated and tested. Three thermoplastics were included in the investigation: polysulfone, polyethersulfone, and polyarylsulfone. Type HMS graphite was used as the reinforcement. Bending fatigue tests of HMS graphite/polyethersulfone demonstrated a gradual shear failure mode which resulted in a loss of stiffness in the specimens. Preliminary curves were generated to show the loss in stiffness as a function of stress and number of cycles. Fan exit guide vanes of HMS graphite polyethersulfone were satisfactorily fabricated in the final phase of the program. These were found to have stiffness and better fatigue behavior than graphite epoxy vanes which were formerly bill of material.

Navak, R. C.↗

Measurement of damping of graphite epoxy materials

Work on a damping measurement test apparatus is discussed. The device is designed to excite tube specimens in a vacuum chamber. Also some experiments were conducted on a tube specimen to confirm previously reported results. A table of data showing the results of forced vibration tests using a half ring and a free-free boundary is given. The main purpose was to study the effect of the frequency resolution on the damping ratio measurements.

Crocker, M. J.↗

Effect of temperature on composite sandwich structures subjected to low velocity impact

The effect of low velocity projectile impact on sandwich-type structural components was investigated. The materials used in the fabrication of the impact surface were graphite-, Kevlar-, and boron-fibers with appropriate epoxy matrices. The testing of the specimens was performed at moderately low- and high-temperatures as well as at room temperature to assess the impact-initiated strength degradation of the laminates. Eleven laminates with different stacking sequences, orientations, and thicknesses were tested. The low energy projectile impact is considered to simulate the damage caused by runway debris, the dropping of the hand tools during servicing, etc., on the secondary aircraft structures fabricated with the composite materials. The results show the preload and the impact energy combinations necessary to cause catastrophic failure in the laminates tested. A set of faired curves indicating the failure thresholds is shown separately for the tension-and compression-loaded laminates. The specific-strengths and -modulii for the various laminates tested are also given.

Sharma, A. V.↗

Impact-initiated damage thresholds in composites

An experimental investigation was conducted to study the effect of low velocity projectile impact on the sandwich-type structural components. The materials used in the fabrication of the impact surface were graphite-, Kevlar-, and boron-fibers with appropriate epoxy matrices. The testing of the specimens was performed at moderately low- and high-temperatures as well as at room temperature to assess the impact-initiated strength degradation of the laminates. Eleven laminates with different stacking sequences, orientations, and thicknesses were tested. The low energy projectile impact is considered to simulate the damage caused by runway debris, dropping of the hand tools during servicing, etc., on the secondary aircraft structures fabricated with the composite materials. The results show the preload and the impact energy combinations necessary to cause catastrophic failures in the laminates tested. A set of faired curves indicating the failure thresholds is shown separately for the tension- and compression-loaded laminates. The specific-strengths and -moduli for the various laminates tested are also given.

Sharma, A. V.↗

Local buckling and crippling of composite stiffener sections

Local buckling, postbuckling, and crippling (failure) of channel, zee, and I- and J-section stiffeners made of AS4/3502 graphite-epoxy unidirectional tape are studied by experiment and analysis. Thirty-six stiffener specimens were tested statically to failure in axial compression as intermediate length columns. Web width is 1.25 inches for all specimens, and the flange width-to-thickness ratio ranges from 7 to 28 for the specimens tested. The radius of the stiffener corners is either 0.125 or 0.250 inches. A sixteen-ply orthotropic layup, an eight-ply quasi-isotropic layup, and a sixteen-ply quasi-isotropic layup are examined. Geometrically nonlinear analyses of five specimens were performed with the STAGS finite element code. Analytical results are compared to experimental data. Inplane stresses from STAGS are used to conduct a plane stress failure analysis of these specimens. Also, the development of interlaminar stress equations from equilibrium for classical laminated plate theory is presented. An algorithm to compute high order displacement derivatives required by these equations based on the Discrete Fourier Transform (DFT) is discussed.

Bonanni, David L.↗

Measurement of damping of graphite epoxy composite materials and structural joints

The damping capacity of graphite epoxy materials and structural joints was evaluated. The damping ratio of different composite specimens and bonded joints were systematically evaluated under normal atmospheric conditions and in a vacuum environment. Free and forced vibration test methods were employed for measuring the damping ratios. The effect of edge support conditions on the damping value of a composite tube specimen was studied by using a series of experiments performed on the specimen with different edge supports. It was found that simulating a free-free boundary conditions by having no constraints at the ends gives the lowest value of the material damping of the composite. The accuracy of the estimation of the damping ratio value was improved by using a curve-fitting technique on the response data obtained through measurement. The effect of outgassing (moisture desorption) on the damping capacity was determined by measuring the damping ratio of the tube specimen in a vacuum environment before and after outgassing had occurred. The effects of high and low temperatures on the damping was also investigated by using a series of experiments on tube and beam specimens. An analytical model to study the vibrations of a bonded lap joint system was formulated. Numerical results were generated for different overlap ratios of the system. These were compared with experimental results. In order to determine the influence of bonded joints on the material damping capacity, experiments were conducted on bonded lap-jointed and double-butt-jointed specimens. These experimental results were compared with simple beam specimens with no joints.

Crocker, Malcolm J.↗

Static evaluation of surface coatings for compliant gas bearings in an oxidizing atmosphere to 650 C

Hard wear-resistant coatings and soft low shear strength coatings were developed for an air-lubricated compliant journal bearing for a future automotive gas turbine engine. The coatings were expected to function in either 540 or 650 C ambient. Soft lubricant coatings were generally limited in temperature. Therefore emphasis was on the hard wear-resistant coatings. The coating materials covered were TiC, B4C, Cr3C2, WC, SiC, CrB2, TiB2, Cr2O3, Al2O3, Si3N4, Tribaloy 800, CaF2, CaF2-BaF2 eutectic, Ni-Co, silver, CdO-graphite and proprietary compounds. The coatings on test coupons were subjected to static oven screening tests. The test consisted of exposure of material samples in an oven for 300 h at the maximum temperature (540 or 650 C) and ten temperature cycles from room temperature to the maximum service temperature. On the basis of the specimen examinations the following coatings were recommended for future wear tests: TiC (sputtered), Cr2O3 (sputtered), Si3N4 (sputtered), CdO and graphite (fused), Kaman DES (a proprietary coating), CrB2 (plasma sprayed), Cr3C2 (detonation gun) and NASA PS-106 (plasma sprayed).

Bhushan, B.↗

Erosion of graphite surface exposed to hot supersonic hydrogen gas

A theoretical model based on laminar boundary layer flow equations was developed to predict the erosion rate of a graphite (AGCarb-101) surface exposed to a hot supersonic stream of hydrogen gas. The supersonic flow in the nozzle outside the boundary layer formed over the surface of the specimen was determined by assuming one-dimensional isentropic conditions. An overall surface reaction rate expression based on experimental studies was used to describe the interaction of hydrogen with graphite. A satisfactory agreement was found between the results of the computation, and the available experimental data. Some shortcomings of the model and further possible improvements are discussed.

Sharma, O. P.↗

Deformation measurements of composite multi-span beam shear specimens by Moire interferometry

Experimental analyses were performed for determination of in plane deformations and shear strains in unidirectional and quasi-isotropic graphite-epoxy beams. Forty-eight ply beams were subjected to 5 point and 3 point flexure. Whole field measurements were recorded at load levels from about 20% to more than 90% of failure loads. Contour maps of U and W displacement fields were obtained by moire interferometry, using reference gratings of 2400 lines/mm. Clearly defined fringes with fringe orders exceeding 1000 were obtained. Whole field contour maps of shear strains were obtained by a method developed for these tests. Various anomalous effects were detected in the displacement fields. Their analysis indicated excess shear strains in resin rich zones in regions of shear tractions; free edge shear strains in quasi-isotropic specimens in regions of normal stresses; and shear stresses associated with cyclic shear compliances of quasi-isotropic plies in regions of shear tractions. Their contributions could occur independently or in superposition. Qualitative analyses addressed questions of relaxation; influence of contact stress distribution; specimen failure; effect of specimen overhang; nonlinearity; and qualities of 5 and 3 point flexure tests.

Post, D.↗

Scaling effects in angle-ply laminates

The effect of specimen size upon the response and strength of +/- 45 degree angle-ply laminates was investigated for two graphite fiber reinforced plastic systems and several stacking sequences. The first material system was a brittle epoxy based system, AS4 fibers in 3502 epoxy, and the second was a tough thermoplastic based system, AS4 fibers in PEEK matrix. For the epoxy based system, two generic +/- 45 degree lay-ups were studied: (+45 degrees sub n/-45 degrees sub n) sub 2S (blocked plies), and (+45 degrees/-45 degrees) sub 2nS, for n=1 and 2. The in-plane dimensions of the specimens were varied such that the width/length relationship was 12.7 x n/127 x n mm, for m=1, 2, 3, or 4. It is shown that the stress/strain response and the ultimate strength of these angle-ply laminates depends on the laminate thickness and the type of generic lay-up used. Furthermore, it is shown that first ply failure occurs in the surface plies as a result of normal rather than shear stresses. The implications of the experimental findings upon the validity of the +/- 45 degree tensile test which is used to determine the in-plane shear response of unidirectional composites are discussed.

Kellas, Sotiris↗

A method for determining structural properties of RCC thermal protection material

A method was developed for evaluation and prediction of effects of oxidation of the graphitic substrate on structural properties of Reinforced Carbon-Carbon (RCC) thermal protection material. Test specimens of RCC material were exposed to successive periods of convective heating in a plasma-jet facility to simulate the chemical reactions of Shuttle atmospheric entry. After each period of testing, the test specimen mass loss and performance in a nondestructive flexure test were determined. A computational model of the RCC specimen was developed for the NASA Structural Analysis (NASTRAN) program and validated by comparison of calculated and experimental results of flexure tests. The elastic moduli and ultimate loads in tension and compression were then computed for various levels of substrate oxidation.

Wakefield, R. M.↗

An investigation of the Iosipescu and Asymmetrical Four-Point Bend tests for composite materials

The results of an extensive analytical and experimental investigation of the Iosipescu and Asymmetrical Four-Point Bend (AFPB) test methods are summarized. Finite element analyses were used to assess the influence of notch parameters and load locations on the stress state in the specimens. The shear moduli and shear strengths were experimentally measured for quasi-isotropic graphite-epoxy laminates using both the Iosipescu and the AFPB test methods with various combinations of notch parameters and load locations. The test results indicate that changes in the notch geometry and load locations aimed at improving the stress distribution in the test section result in unexpected changes in the failure mode.

Spigel, B. S.↗

The effect of processing on autohesive strength development in thermoplastic resins and composites

In the present investigation of processing effects on the autohesive bond strength of neat polysulfone resin and graphite-reinforced polysulfone-matrix composites measured resin bond strength development in precracked compact tension specimens 'healed' by heating over a contact period at a given temperature. The critical strain energy release rate of refractured composite specimens did not exhibit the strong time or temperature dependence of the neat resin tests; only 80-90 percent of the undamaged fracture energy is recoverable.

Howes, Jeremy C.↗